Characterization, antioxidant capacity, and application of a microcapsule with essential oil from Campomanesia adamantium fruit residue in a cosmetic product

ABSTRACT Essential oils (EOs) are continuously explored from new sources, while encapsulation emerges as a promising strategy for their application in different fields. The aim of this study was to characterize microcapsules (MCs) containing EOs extracted from Campomanesia adamantium fruit residues,...

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Main Authors: Márcia Crestani Bin, Loyz Sousa Assis, Daniel Araujo Gonçalves, Claudia Andrea Lima Cardoso, Camila Panzetti Alonso, Adriana Mary Mestriner Felipe de Melo, Dênia Mendes de Sousa Valladão, Eliana Janet Sanjinez Argandoña
Format: Article
Language:English
Published: Universidade Federal de Lavras 2025-03-01
Series:Ciência e Agrotecnologia
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Online Access:http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1413-70542025000100213&lng=en&tlng=en
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author Márcia Crestani Bin
Loyz Sousa Assis
Daniel Araujo Gonçalves
Claudia Andrea Lima Cardoso
Camila Panzetti Alonso
Adriana Mary Mestriner Felipe de Melo
Dênia Mendes de Sousa Valladão
Eliana Janet Sanjinez Argandoña
author_facet Márcia Crestani Bin
Loyz Sousa Assis
Daniel Araujo Gonçalves
Claudia Andrea Lima Cardoso
Camila Panzetti Alonso
Adriana Mary Mestriner Felipe de Melo
Dênia Mendes de Sousa Valladão
Eliana Janet Sanjinez Argandoña
author_sort Márcia Crestani Bin
collection DOAJ
description ABSTRACT Essential oils (EOs) are continuously explored from new sources, while encapsulation emerges as a promising strategy for their application in different fields. The aim of this study was to characterize microcapsules (MCs) containing EOs extracted from Campomanesia adamantium fruit residues, evaluate their antioxidant capacity and incorporate them into a cosmetic formulation. Two microcapsules (MCs) containing EO were prepared by complex coacervation with gelatin (G) and gum arabic (GA) in two ratios: MC1 (G:GA 1:2) and MC2 (G:GA 2:1). The chemical composition, EO retention, encapsulation efficiency, morphological features, solubility, hygroscopicity, thermal properties, infrared spectroscopy, and antioxidant capacity were analyzed. EO and MC were incorporated into an anti-aging cosmetic formulation, and the organoleptic characteristics, stability (4, 25, and 45 °C), spreadability, and microbiological quality of the cream were evaluated for 90 days. MC1 exhibited superior properties due to the greater proportion of gum arabic, which provided thermal protection, better water solubility, lower hygroscopicity, and a less porous surface. The MC1 and MC2 antioxidant capacities were similar to those of free EO, consistent with the results of the retention rates and encapsulation efficiency. Infrared spectroscopy confirmed the encapsulation, maintaining the main constituents of EO (α-pinene, limonene, β-ocimene, and β-caryophyllene). Incorporating the MCs and EO into a cosmetic cream resulted in the formation of a stable emulsion with good spreadability and consistent organoleptic properties over 90 days, suggesting that C. adamantium residue can be used in cosmetic formulations.
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spelling doaj-art-e6f7eb66411c44c1af85bc471001bd972025-08-20T02:08:45ZengUniversidade Federal de LavrasCiência e Agrotecnologia1981-18292025-03-014910.1590/1413-7054202549021824Characterization, antioxidant capacity, and application of a microcapsule with essential oil from Campomanesia adamantium fruit residue in a cosmetic productMárcia Crestani Binhttps://orcid.org/0000-0002-9288-3634Loyz Sousa Assishttps://orcid.org/0000-0001-9640-0962Daniel Araujo Gonçalveshttps://orcid.org/0000-0002-0204-2779Claudia Andrea Lima Cardosohttps://orcid.org/0000-0002-4907-0056Camila Panzetti Alonsohttps://orcid.org/0009-0002-0308-6295Adriana Mary Mestriner Felipe de Melohttps://orcid.org/0000-0001-9643-7036Dênia Mendes de Sousa Valladãohttps://orcid.org/0000-0002-2643-1963Eliana Janet Sanjinez Argandoñahttps://orcid.org/0000-0001-9377-8839ABSTRACT Essential oils (EOs) are continuously explored from new sources, while encapsulation emerges as a promising strategy for their application in different fields. The aim of this study was to characterize microcapsules (MCs) containing EOs extracted from Campomanesia adamantium fruit residues, evaluate their antioxidant capacity and incorporate them into a cosmetic formulation. Two microcapsules (MCs) containing EO were prepared by complex coacervation with gelatin (G) and gum arabic (GA) in two ratios: MC1 (G:GA 1:2) and MC2 (G:GA 2:1). The chemical composition, EO retention, encapsulation efficiency, morphological features, solubility, hygroscopicity, thermal properties, infrared spectroscopy, and antioxidant capacity were analyzed. EO and MC were incorporated into an anti-aging cosmetic formulation, and the organoleptic characteristics, stability (4, 25, and 45 °C), spreadability, and microbiological quality of the cream were evaluated for 90 days. MC1 exhibited superior properties due to the greater proportion of gum arabic, which provided thermal protection, better water solubility, lower hygroscopicity, and a less porous surface. The MC1 and MC2 antioxidant capacities were similar to those of free EO, consistent with the results of the retention rates and encapsulation efficiency. Infrared spectroscopy confirmed the encapsulation, maintaining the main constituents of EO (α-pinene, limonene, β-ocimene, and β-caryophyllene). Incorporating the MCs and EO into a cosmetic cream resulted in the formation of a stable emulsion with good spreadability and consistent organoleptic properties over 90 days, suggesting that C. adamantium residue can be used in cosmetic formulations.http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1413-70542025000100213&lng=en&tlng=enAgrobiodiversitybioactive compoundsCerradoguaviravolatile oil
spellingShingle Márcia Crestani Bin
Loyz Sousa Assis
Daniel Araujo Gonçalves
Claudia Andrea Lima Cardoso
Camila Panzetti Alonso
Adriana Mary Mestriner Felipe de Melo
Dênia Mendes de Sousa Valladão
Eliana Janet Sanjinez Argandoña
Characterization, antioxidant capacity, and application of a microcapsule with essential oil from Campomanesia adamantium fruit residue in a cosmetic product
Ciência e Agrotecnologia
Agrobiodiversity
bioactive compounds
Cerrado
guavira
volatile oil
title Characterization, antioxidant capacity, and application of a microcapsule with essential oil from Campomanesia adamantium fruit residue in a cosmetic product
title_full Characterization, antioxidant capacity, and application of a microcapsule with essential oil from Campomanesia adamantium fruit residue in a cosmetic product
title_fullStr Characterization, antioxidant capacity, and application of a microcapsule with essential oil from Campomanesia adamantium fruit residue in a cosmetic product
title_full_unstemmed Characterization, antioxidant capacity, and application of a microcapsule with essential oil from Campomanesia adamantium fruit residue in a cosmetic product
title_short Characterization, antioxidant capacity, and application of a microcapsule with essential oil from Campomanesia adamantium fruit residue in a cosmetic product
title_sort characterization antioxidant capacity and application of a microcapsule with essential oil from campomanesia adamantium fruit residue in a cosmetic product
topic Agrobiodiversity
bioactive compounds
Cerrado
guavira
volatile oil
url http://www.scielo.br/scielo.php?script=sci_arttext&pid=S1413-70542025000100213&lng=en&tlng=en
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