Investigation of Elastic Properties of Sc Doped AlN: A <i>First principles</i> and Experimental Approach

Aluminum Nitride (AlN) is a promising piezoelectric material for microelectromechanical systems owing to its attractive physical and chemical properties and CMOS compatibility. It has a moderate piezo response compared to its rival material bound to its wide application. This obstacle can be overcom...

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Main Authors: Jyothilakshmi Rudresh, N. V. Srihari, Suhas Kowshik, Sandeep, K. K. Nagaraja
Format: Article
Language:English
Published: MDPI AG 2023-12-01
Series:Engineering Proceedings
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Online Access:https://www.mdpi.com/2673-4591/59/1/86
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author Jyothilakshmi Rudresh
N. V. Srihari
Suhas Kowshik
Sandeep
K. K. Nagaraja
author_facet Jyothilakshmi Rudresh
N. V. Srihari
Suhas Kowshik
Sandeep
K. K. Nagaraja
author_sort Jyothilakshmi Rudresh
collection DOAJ
description Aluminum Nitride (AlN) is a promising piezoelectric material for microelectromechanical systems owing to its attractive physical and chemical properties and CMOS compatibility. It has a moderate piezo response compared to its rival material bound to its wide application. This obstacle can be overcome by doping or alloying. Sc alloying increases the piezo response of AlN up to four-fold; it also increases the electromechanical coupling coefficient, which is a prominent figure of merit for any MEMS device application. Sc doping induces elastic softening in wurtzite AlN, enhances polarization, and increases piezoelectric constants. However, the possibility of phase separation at higher Sc concentrations, and the wurtzite phase of AlN, which is responsible for piezoelectricity, becomes negligible. Therefore, knowing the optimum concentration of Sc for device applications is necessary. In this work, using density functional theory, we calculated the lattice parameter, band and density of states along with the physical properties such as Young’s modulus, the bulk modulus, Poisson’s ratio, and elastic constants of pristine AlN and Sc doped AlN. The DFT calculations show that the geometrical optimized lattice parameters agree with the literature. As a function of increased Sc concentration, the calculated Young’s modulus and elastic constants decrease, indicating a decrease in hardness and elastic softening, respectively. Meanwhile, the bulk modulus and Poisson’s ratio increase with an increase in Sc concentration, representing an increase in the crystal cell parameters and elastic deformation. AlN and AlScN thin films were grown on Si (111) substrate using magnetron sputtering to study the structural properties experimentally. The deposited films show the required c-axis (002) preferential crystallographic orientation. The XRD peaks of Sc doped AlN thin films have shifted to a lower angle than pristine AlN, indicating elastic softening/tensile stress in grown thin films. So, from our observation, we can conclude that Sc doping induces elastic softening in AlN and deposited films have a preferential crystallographic orientation that can be applied in MEMS devices.
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spelling doaj-art-e36d3864fc944cb99b0c4982b21fa4ba2025-08-20T02:42:38ZengMDPI AGEngineering Proceedings2673-45912023-12-015918610.3390/engproc2023059086Investigation of Elastic Properties of Sc Doped AlN: A <i>First principles</i> and Experimental ApproachJyothilakshmi Rudresh0N. V. Srihari1Suhas Kowshik2Sandeep3K. K. Nagaraja4Alternate Energy Materials Laboratory, Department of Physics, Manipal Institute of Technology, Manipal Academy of Higher Education, Manipal 576 104, Karnataka, IndiaAlternate Energy Materials Laboratory, Department of Physics, Manipal Institute of Technology, Manipal Academy of Higher Education, Manipal 576 104, Karnataka, IndiaDepartment of Mechanical and Industrial Engineering, Manipal Institute of Technology, Manipal Academy of Higher Education, Manipal 576 104, Karnataka, IndiaAlternate Energy Materials Laboratory, Department of Physics, Manipal Institute of Technology, Manipal Academy of Higher Education, Manipal 576 104, Karnataka, IndiaAlternate Energy Materials Laboratory, Department of Physics, Manipal Institute of Technology, Manipal Academy of Higher Education, Manipal 576 104, Karnataka, IndiaAluminum Nitride (AlN) is a promising piezoelectric material for microelectromechanical systems owing to its attractive physical and chemical properties and CMOS compatibility. It has a moderate piezo response compared to its rival material bound to its wide application. This obstacle can be overcome by doping or alloying. Sc alloying increases the piezo response of AlN up to four-fold; it also increases the electromechanical coupling coefficient, which is a prominent figure of merit for any MEMS device application. Sc doping induces elastic softening in wurtzite AlN, enhances polarization, and increases piezoelectric constants. However, the possibility of phase separation at higher Sc concentrations, and the wurtzite phase of AlN, which is responsible for piezoelectricity, becomes negligible. Therefore, knowing the optimum concentration of Sc for device applications is necessary. In this work, using density functional theory, we calculated the lattice parameter, band and density of states along with the physical properties such as Young’s modulus, the bulk modulus, Poisson’s ratio, and elastic constants of pristine AlN and Sc doped AlN. The DFT calculations show that the geometrical optimized lattice parameters agree with the literature. As a function of increased Sc concentration, the calculated Young’s modulus and elastic constants decrease, indicating a decrease in hardness and elastic softening, respectively. Meanwhile, the bulk modulus and Poisson’s ratio increase with an increase in Sc concentration, representing an increase in the crystal cell parameters and elastic deformation. AlN and AlScN thin films were grown on Si (111) substrate using magnetron sputtering to study the structural properties experimentally. The deposited films show the required c-axis (002) preferential crystallographic orientation. The XRD peaks of Sc doped AlN thin films have shifted to a lower angle than pristine AlN, indicating elastic softening/tensile stress in grown thin films. So, from our observation, we can conclude that Sc doping induces elastic softening in AlN and deposited films have a preferential crystallographic orientation that can be applied in MEMS devices.https://www.mdpi.com/2673-4591/59/1/86aluminum scandium nitridepiezoelectricitydensity functional theoryDFTmagnetron sputteringelastic softening
spellingShingle Jyothilakshmi Rudresh
N. V. Srihari
Suhas Kowshik
Sandeep
K. K. Nagaraja
Investigation of Elastic Properties of Sc Doped AlN: A <i>First principles</i> and Experimental Approach
Engineering Proceedings
aluminum scandium nitride
piezoelectricity
density functional theory
DFT
magnetron sputtering
elastic softening
title Investigation of Elastic Properties of Sc Doped AlN: A <i>First principles</i> and Experimental Approach
title_full Investigation of Elastic Properties of Sc Doped AlN: A <i>First principles</i> and Experimental Approach
title_fullStr Investigation of Elastic Properties of Sc Doped AlN: A <i>First principles</i> and Experimental Approach
title_full_unstemmed Investigation of Elastic Properties of Sc Doped AlN: A <i>First principles</i> and Experimental Approach
title_short Investigation of Elastic Properties of Sc Doped AlN: A <i>First principles</i> and Experimental Approach
title_sort investigation of elastic properties of sc doped aln a i first principles i and experimental approach
topic aluminum scandium nitride
piezoelectricity
density functional theory
DFT
magnetron sputtering
elastic softening
url https://www.mdpi.com/2673-4591/59/1/86
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AT suhaskowshik investigationofelasticpropertiesofscdopedalnaifirstprinciplesiandexperimentalapproach
AT sandeep investigationofelasticpropertiesofscdopedalnaifirstprinciplesiandexperimentalapproach
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