Synthesis, Structure, and Characterization of Keggin-Type Germanate

A novel Keggin-type germanate, (NH4)9[Ge7O14F3]3·1.75H2O (I), is hydrothermally synthesized and structurally characterized by X-ray single-crystal diffraction, elemental analysis, XRD, and TG. (I) is tetragonal system with space group I4/mmm and unit cell: a=28.280 (4) Å, c=24.881(5) Å, V=19899(6) Å...

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Bibliographic Details
Main Authors: Ya-feng Li, Xiao-lin Qin, Yue Xu, Wen-yuan Gao, Yue Gao
Format: Article
Language:English
Published: Wiley 2013-01-01
Series:Journal of Chemistry
Online Access:http://dx.doi.org/10.1155/2013/639409
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