Antimicrobial Efficacy of Eugenol and Neem Oil Nanoemulsions Against Foodborne Pathogens and Food Spoilage Fungi

ABSTRACT Essential oils are widely recognized for their antimicrobial properties, making them promising natural alternatives for food preservation and spoilage prevention. However, practical challenges such as hydrophobicity, instability, and strong aroma have limited their applications. To overcome...

Full description

Saved in:
Bibliographic Details
Main Authors: L Susmita Devi, Avik Mukherjee, Manash R. Das, Santosh Kumar
Format: Article
Language:English
Published: Wiley 2025-03-01
Series:Food Bioengineering
Subjects:
Online Access:https://doi.org/10.1002/fbe2.70007
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1849698929731436544
author L Susmita Devi
Avik Mukherjee
Manash R. Das
Santosh Kumar
author_facet L Susmita Devi
Avik Mukherjee
Manash R. Das
Santosh Kumar
author_sort L Susmita Devi
collection DOAJ
description ABSTRACT Essential oils are widely recognized for their antimicrobial properties, making them promising natural alternatives for food preservation and spoilage prevention. However, practical challenges such as hydrophobicity, instability, and strong aroma have limited their applications. To overcome these challenges, this study aimed to prepare nanoemulsions of eugenol and neem oil using ultrasonication techniques and evaluating their antimicrobial efficacy, highlighting their potential for sustainable food preservation. The antimicrobial efficacy of these nanoemulsions was evaluated against four foodborne bacteria and spoilage fungi using well diffusion method. Nanoemulsions, formulated with oil concentrations of 5%–20%, exhibited particle sizes ranging from 135 to 373 d.nm for neem oil and 410 to 587 d.nm for eugenol, with polydispersity indices indicating variable size distribution (0.27–0.88 for neem oil and 0.13–0.60 for eugenol). Stability tests confirmed overall stability, although some eugenol‐based nanoemulsions exhibited minor precipitation due to turbidity. Both neem oil and eugenol nanoemulsions displayed significant antimicrobial activity, with eugenol being more effective even at lower concentrations. NNE‐20 showed the largest inhibition zones against Bacillus subtilis (17.83 mm), Escherichia coli (14.83 mm), and Enterobacter aerogenes (14.16 mm), while NNE‐15 was most effective against Staphylococcus aureus (14 mm). Eugenol nanoemulsions exhibited superior antibacterial activity, achieving inhibition zones of 18–23.5 mm with higher eugenol concentrations. For fungi, neem oil nanoemulsions inhibited Colletotrichum gloeosporioides, Rhizopus stolonifer and Aspergillus niger (15–20 mm), while eugenol nanoemulsions outperformed neem oil, showing zones of 24–26 mm (Aspergillus niger) and 20–24 mm (Saccharomyces cerevisiae). These findings highlight the potential of neem oil and eugenol nanoemulsions as stable, natural, and effective alternatives to synthetic preservatives for improving food safety and extending shelf life.
format Article
id doaj-art-a8286492d71f48e3861a633b747d1017
institution DOAJ
issn 2770-2081
language English
publishDate 2025-03-01
publisher Wiley
record_format Article
series Food Bioengineering
spelling doaj-art-a8286492d71f48e3861a633b747d10172025-08-20T03:18:45ZengWileyFood Bioengineering2770-20812025-03-014110111210.1002/fbe2.70007Antimicrobial Efficacy of Eugenol and Neem Oil Nanoemulsions Against Foodborne Pathogens and Food Spoilage FungiL Susmita Devi0Avik Mukherjee1Manash R. Das2Santosh Kumar3Department of Food Engineering and Technology Central Institute of Technology Kokrajhar Kokrajhar Assam IndiaDepartment of Food Engineering and Technology Central Institute of Technology Kokrajhar Kokrajhar Assam IndiaMaterials Sciences and Technology Division, CSIR North‐East Institute of Science and Technology Jorhat Assam IndiaDepartment of Food Engineering and Technology Central Institute of Technology Kokrajhar Kokrajhar Assam IndiaABSTRACT Essential oils are widely recognized for their antimicrobial properties, making them promising natural alternatives for food preservation and spoilage prevention. However, practical challenges such as hydrophobicity, instability, and strong aroma have limited their applications. To overcome these challenges, this study aimed to prepare nanoemulsions of eugenol and neem oil using ultrasonication techniques and evaluating their antimicrobial efficacy, highlighting their potential for sustainable food preservation. The antimicrobial efficacy of these nanoemulsions was evaluated against four foodborne bacteria and spoilage fungi using well diffusion method. Nanoemulsions, formulated with oil concentrations of 5%–20%, exhibited particle sizes ranging from 135 to 373 d.nm for neem oil and 410 to 587 d.nm for eugenol, with polydispersity indices indicating variable size distribution (0.27–0.88 for neem oil and 0.13–0.60 for eugenol). Stability tests confirmed overall stability, although some eugenol‐based nanoemulsions exhibited minor precipitation due to turbidity. Both neem oil and eugenol nanoemulsions displayed significant antimicrobial activity, with eugenol being more effective even at lower concentrations. NNE‐20 showed the largest inhibition zones against Bacillus subtilis (17.83 mm), Escherichia coli (14.83 mm), and Enterobacter aerogenes (14.16 mm), while NNE‐15 was most effective against Staphylococcus aureus (14 mm). Eugenol nanoemulsions exhibited superior antibacterial activity, achieving inhibition zones of 18–23.5 mm with higher eugenol concentrations. For fungi, neem oil nanoemulsions inhibited Colletotrichum gloeosporioides, Rhizopus stolonifer and Aspergillus niger (15–20 mm), while eugenol nanoemulsions outperformed neem oil, showing zones of 24–26 mm (Aspergillus niger) and 20–24 mm (Saccharomyces cerevisiae). These findings highlight the potential of neem oil and eugenol nanoemulsions as stable, natural, and effective alternatives to synthetic preservatives for improving food safety and extending shelf life.https://doi.org/10.1002/fbe2.70007antibacterial activity, natural food preservativeessential oilfunctional agentnanoemulsion
spellingShingle L Susmita Devi
Avik Mukherjee
Manash R. Das
Santosh Kumar
Antimicrobial Efficacy of Eugenol and Neem Oil Nanoemulsions Against Foodborne Pathogens and Food Spoilage Fungi
Food Bioengineering
antibacterial activity, natural food preservative
essential oil
functional agent
nanoemulsion
title Antimicrobial Efficacy of Eugenol and Neem Oil Nanoemulsions Against Foodborne Pathogens and Food Spoilage Fungi
title_full Antimicrobial Efficacy of Eugenol and Neem Oil Nanoemulsions Against Foodborne Pathogens and Food Spoilage Fungi
title_fullStr Antimicrobial Efficacy of Eugenol and Neem Oil Nanoemulsions Against Foodborne Pathogens and Food Spoilage Fungi
title_full_unstemmed Antimicrobial Efficacy of Eugenol and Neem Oil Nanoemulsions Against Foodborne Pathogens and Food Spoilage Fungi
title_short Antimicrobial Efficacy of Eugenol and Neem Oil Nanoemulsions Against Foodborne Pathogens and Food Spoilage Fungi
title_sort antimicrobial efficacy of eugenol and neem oil nanoemulsions against foodborne pathogens and food spoilage fungi
topic antibacterial activity, natural food preservative
essential oil
functional agent
nanoemulsion
url https://doi.org/10.1002/fbe2.70007
work_keys_str_mv AT lsusmitadevi antimicrobialefficacyofeugenolandneemoilnanoemulsionsagainstfoodbornepathogensandfoodspoilagefungi
AT avikmukherjee antimicrobialefficacyofeugenolandneemoilnanoemulsionsagainstfoodbornepathogensandfoodspoilagefungi
AT manashrdas antimicrobialefficacyofeugenolandneemoilnanoemulsionsagainstfoodbornepathogensandfoodspoilagefungi
AT santoshkumar antimicrobialefficacyofeugenolandneemoilnanoemulsionsagainstfoodbornepathogensandfoodspoilagefungi