Unveiling synergistic antioxidant combinations for α-tocopherol in emulsions: A spectrophotometric-mathematical approach

This study presents a novel method based on a spectrophotometric assay coupled with mathematical modeling (Weibull interactions modeling CAT) to evaluate synergistic interactions of antioxidants in an oil-in-water model emulsion. The approach addresses a major limitation in current assays by elimina...

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Main Authors: Camille Robichon, Pierre Villeneuve, Philippe Bohuon, Bruno Baréa, Nathalie Barouh, Francis Courtois, Frédéric Fine, Erwann Durand
Format: Article
Language:English
Published: Elsevier 2025-01-01
Series:Current Research in Food Science
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Online Access:http://www.sciencedirect.com/science/article/pii/S2665927125001650
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author Camille Robichon
Pierre Villeneuve
Philippe Bohuon
Bruno Baréa
Nathalie Barouh
Francis Courtois
Frédéric Fine
Erwann Durand
author_facet Camille Robichon
Pierre Villeneuve
Philippe Bohuon
Bruno Baréa
Nathalie Barouh
Francis Courtois
Frédéric Fine
Erwann Durand
author_sort Camille Robichon
collection DOAJ
description This study presents a novel method based on a spectrophotometric assay coupled with mathematical modeling (Weibull interactions modeling CAT) to evaluate synergistic interactions of antioxidants in an oil-in-water model emulsion. The approach addresses a major limitation in current assays by eliminating interference from pro-/antioxidant pathways induced by exogenous radical initiators or buffers, allowing for a more accurate assessment of antioxidant efficacy. Using the Weibull equation, key kinetic parameters (LagP, α, β) were extracted to characterize the impact of antioxidant combinations on lipid oxidation. Results showed that certain combinations, such as α-tocopherol with carnosic acid, dieckol, and myricetin, exhibited concentration-dependent synergistic effects. Among these, carnosic acid in equimolar ratios demonstrated particularly promising interactions. In contrast, ascorbic acid revealed antagonistic behaviour when combined with α-tocopherol. Additionally, the presence of ferrous ions significantly influenced antioxidant interactions, highlighting their role in modulating underlying mechanisms. Overall, carnosic acid and dieckol emerged as strong candidates for use in combination with α-tocopherol under specific conditions. This method provides a refined approach for screening antioxidant synergies and contributes to the development of more effective antioxidant formulations in emulsified systems.
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issn 2665-9271
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publishDate 2025-01-01
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series Current Research in Food Science
spelling doaj-art-8d8905f120ec49c2b972d8885344d9392025-08-20T03:31:30ZengElsevierCurrent Research in Food Science2665-92712025-01-011110113410.1016/j.crfs.2025.101134Unveiling synergistic antioxidant combinations for α-tocopherol in emulsions: A spectrophotometric-mathematical approachCamille Robichon0Pierre Villeneuve1Philippe Bohuon2Bruno Baréa3Nathalie Barouh4Francis Courtois5Frédéric Fine6Erwann Durand7CIRAD, UMR QualiSud, F-34398, Montpellier, France; QUALISUD, Univ Montpellier, Avignon Université, CIRAD, Institut Agro, IRD, Université de La Réunion, Montpellier, FranceCIRAD, UMR QualiSud, F-34398, Montpellier, France; QUALISUD, Univ Montpellier, Avignon Université, CIRAD, Institut Agro, IRD, Université de La Réunion, Montpellier, FranceQUALISUD, Univ Montpellier, Avignon Université, CIRAD, Institut Agro, IRD, Université de La Réunion, Montpellier, FranceCIRAD, UMR QualiSud, F-34398, Montpellier, France; QUALISUD, Univ Montpellier, Avignon Université, CIRAD, Institut Agro, IRD, Université de La Réunion, Montpellier, FranceCIRAD, UMR QualiSud, F-34398, Montpellier, France; QUALISUD, Univ Montpellier, Avignon Université, CIRAD, Institut Agro, IRD, Université de La Réunion, Montpellier, FranceQUALISUD, Univ Montpellier, Avignon Université, CIRAD, Institut Agro, IRD, Université de La Réunion, Montpellier, FranceTERRES INOVIA, Parc Industriel – 11 Rue Monge, Pessac, 33600, FranceCIRAD, UMR QualiSud, F-34398, Montpellier, France; QUALISUD, Univ Montpellier, Avignon Université, CIRAD, Institut Agro, IRD, Université de La Réunion, Montpellier, France; Corresponding author. CIRAD, UMR Qualisud, Montpellier, France.This study presents a novel method based on a spectrophotometric assay coupled with mathematical modeling (Weibull interactions modeling CAT) to evaluate synergistic interactions of antioxidants in an oil-in-water model emulsion. The approach addresses a major limitation in current assays by eliminating interference from pro-/antioxidant pathways induced by exogenous radical initiators or buffers, allowing for a more accurate assessment of antioxidant efficacy. Using the Weibull equation, key kinetic parameters (LagP, α, β) were extracted to characterize the impact of antioxidant combinations on lipid oxidation. Results showed that certain combinations, such as α-tocopherol with carnosic acid, dieckol, and myricetin, exhibited concentration-dependent synergistic effects. Among these, carnosic acid in equimolar ratios demonstrated particularly promising interactions. In contrast, ascorbic acid revealed antagonistic behaviour when combined with α-tocopherol. Additionally, the presence of ferrous ions significantly influenced antioxidant interactions, highlighting their role in modulating underlying mechanisms. Overall, carnosic acid and dieckol emerged as strong candidates for use in combination with α-tocopherol under specific conditions. This method provides a refined approach for screening antioxidant synergies and contributes to the development of more effective antioxidant formulations in emulsified systems.http://www.sciencedirect.com/science/article/pii/S2665927125001650α-TocopherolAntioxidantsSynergyLipid oxidationEmulsionModeling
spellingShingle Camille Robichon
Pierre Villeneuve
Philippe Bohuon
Bruno Baréa
Nathalie Barouh
Francis Courtois
Frédéric Fine
Erwann Durand
Unveiling synergistic antioxidant combinations for α-tocopherol in emulsions: A spectrophotometric-mathematical approach
Current Research in Food Science
α-Tocopherol
Antioxidants
Synergy
Lipid oxidation
Emulsion
Modeling
title Unveiling synergistic antioxidant combinations for α-tocopherol in emulsions: A spectrophotometric-mathematical approach
title_full Unveiling synergistic antioxidant combinations for α-tocopherol in emulsions: A spectrophotometric-mathematical approach
title_fullStr Unveiling synergistic antioxidant combinations for α-tocopherol in emulsions: A spectrophotometric-mathematical approach
title_full_unstemmed Unveiling synergistic antioxidant combinations for α-tocopherol in emulsions: A spectrophotometric-mathematical approach
title_short Unveiling synergistic antioxidant combinations for α-tocopherol in emulsions: A spectrophotometric-mathematical approach
title_sort unveiling synergistic antioxidant combinations for α tocopherol in emulsions a spectrophotometric mathematical approach
topic α-Tocopherol
Antioxidants
Synergy
Lipid oxidation
Emulsion
Modeling
url http://www.sciencedirect.com/science/article/pii/S2665927125001650
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