A novel approach to determine residual aldehyde content in conjugated polysaccharides with 3-methyl-2-benzothiazolinonehydrazon (MBTH) by colorimetric method, automation, and HP-SEC

Polysaccharide activation by periodate oxidation to form aldehydes, followed by conjugation with proteins via reductive amination is a general procedure to make polysaccharide-protein conjugate vaccines. Controlling the level of residue aldehyde content after conjugation is critical to ensure vaccin...

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Bibliographic Details
Main Authors: Weidong Tong, Mingxiang Lin, Ping Zhuang, Bukuru Anaclet, Castle Cooper
Format: Article
Language:English
Published: Elsevier 2023-12-01
Series:Journal of Pharmaceutical and Biomedical Analysis Open
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2949771X23000221
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