Efficient synthesis of Triazolo[4,5-d]pyrimidine-7-carbonitriles and Imidazole-4,5-dicarbonitriles using Triethylorthoalkylates and their structural characterisation by Single-crystal x-ray diffraction

Efficient synthesis of Triazolo[4,5-d]pyrimidine-7-carbonitriles and Imidazole-4,5-dicarbonitriles using Triethylorthoalkylates and their structural characterisation by Single-crystal x-ray diffraction

Abstract Cyclisation of 5-amino-1-(4-nitrophenyl)-1H-1,2,3-triazole-4-carbimidoyl cyanide and 3-amino-3-((Z)-2-cyano-2-phenylvinylamino) maleonitrile using either triethyl orthoformate or triethyl orthopropionate in dimethylformamide (DMF):1,4-dioxane (1:1 v/v) mixture under reflux conditions affo...

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Bibliographic Details
Main Authors: Amal Al-Azmi, Mickey Vinodh
Format: Article
Language:English
Published: Elsevier 2021-04-01
Series:Kuwait Journal of Science
Subjects:
triethylorthoalkylates
triazole
imidazole
pyrimidine
crystal structure
Hirshfeld surface analysis
Online Access:https://journalskuwait.org/kjs/index.php/KJS/article/view/9948
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