SYNTHESIS, PHYSICO-CHEMICAL ANALYSIS AND PHARMACOLOGICAL ACTIVITY OF SOME DERIVATIVES OF WARFARIN

Methods of synthesis of 7 warfarin derivatives from which three are combined has been developed. Their structural features, physicochemical properties of synthesized compounds by modern and spectral methods (IR, NMR spectroscopy) were determined. Their anticoagulant activity in vivo were studied by...

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Main Authors: A. Z. Abyshev, I. K. Zhurkovich, D. Yu. Ivkin, C. B. Nguyen
Format: Article
Language:Russian
Published: LLC Center of Pharmaceutical Analytics (LLC «CPHA») 2019-01-01
Series:Разработка и регистрация лекарственных средств
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Online Access:https://www.pharmjournal.ru/jour/article/view/429
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author A. Z. Abyshev
I. K. Zhurkovich
D. Yu. Ivkin
C. B. Nguyen
author_facet A. Z. Abyshev
I. K. Zhurkovich
D. Yu. Ivkin
C. B. Nguyen
author_sort A. Z. Abyshev
collection DOAJ
description Methods of synthesis of 7 warfarin derivatives from which three are combined has been developed. Their structural features, physicochemical properties of synthesized compounds by modern and spectral methods (IR, NMR spectroscopy) were determined. Their anticoagulant activity in vivo were studied by determining prothrombin time (PT). The most pronounced activity was possessed by substances AZ-5 (conjugate warfarin with a fragment of the substance diumancal, 41,2±2,3 s) and AZ-9 (diumancal, 45,18±4,85 s), comparable with the reference drug warfarin (37,4±2,8 s).
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id doaj-art-50cc7c135d3c4ffabc7da1fe003b3d94
institution DOAJ
issn 2305-2066
2658-5049
language Russian
publishDate 2019-01-01
publisher LLC Center of Pharmaceutical Analytics (LLC «CPHA»)
record_format Article
series Разработка и регистрация лекарственных средств
spelling doaj-art-50cc7c135d3c4ffabc7da1fe003b3d942025-08-20T02:54:18ZrusLLC Center of Pharmaceutical Analytics (LLC «CPHA»)Разработка и регистрация лекарственных средств2305-20662658-50492019-01-0102192198429SYNTHESIS, PHYSICO-CHEMICAL ANALYSIS AND PHARMACOLOGICAL ACTIVITY OF SOME DERIVATIVES OF WARFARINA. Z. Abyshev0I. K. Zhurkovich1D. Yu. Ivkin2C. B. Nguyen3Saint-Petersburg State Chemical-Pharmaceutical Academy, Ministry of HealthcareInstitute of Toxicology FMBASaint-Petersburg State Chemical-Pharmaceutical Academy, Ministry of HealthcareSaint-Petersburg State Chemical-Pharmaceutical Academy, Ministry of HealthcareMethods of synthesis of 7 warfarin derivatives from which three are combined has been developed. Their structural features, physicochemical properties of synthesized compounds by modern and spectral methods (IR, NMR spectroscopy) were determined. Their anticoagulant activity in vivo were studied by determining prothrombin time (PT). The most pronounced activity was possessed by substances AZ-5 (conjugate warfarin with a fragment of the substance diumancal, 41,2±2,3 s) and AZ-9 (diumancal, 45,18±4,85 s), comparable with the reference drug warfarin (37,4±2,8 s).https://www.pharmjournal.ru/jour/article/view/429coumarinwarfarindiumancalanticoagulant activity
spellingShingle A. Z. Abyshev
I. K. Zhurkovich
D. Yu. Ivkin
C. B. Nguyen
SYNTHESIS, PHYSICO-CHEMICAL ANALYSIS AND PHARMACOLOGICAL ACTIVITY OF SOME DERIVATIVES OF WARFARIN
Разработка и регистрация лекарственных средств
coumarin
warfarin
diumancal
anticoagulant activity
title SYNTHESIS, PHYSICO-CHEMICAL ANALYSIS AND PHARMACOLOGICAL ACTIVITY OF SOME DERIVATIVES OF WARFARIN
title_full SYNTHESIS, PHYSICO-CHEMICAL ANALYSIS AND PHARMACOLOGICAL ACTIVITY OF SOME DERIVATIVES OF WARFARIN
title_fullStr SYNTHESIS, PHYSICO-CHEMICAL ANALYSIS AND PHARMACOLOGICAL ACTIVITY OF SOME DERIVATIVES OF WARFARIN
title_full_unstemmed SYNTHESIS, PHYSICO-CHEMICAL ANALYSIS AND PHARMACOLOGICAL ACTIVITY OF SOME DERIVATIVES OF WARFARIN
title_short SYNTHESIS, PHYSICO-CHEMICAL ANALYSIS AND PHARMACOLOGICAL ACTIVITY OF SOME DERIVATIVES OF WARFARIN
title_sort synthesis physico chemical analysis and pharmacological activity of some derivatives of warfarin
topic coumarin
warfarin
diumancal
anticoagulant activity
url https://www.pharmjournal.ru/jour/article/view/429
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AT ikzhurkovich synthesisphysicochemicalanalysisandpharmacologicalactivityofsomederivativesofwarfarin
AT dyuivkin synthesisphysicochemicalanalysisandpharmacologicalactivityofsomederivativesofwarfarin
AT cbnguyen synthesisphysicochemicalanalysisandpharmacologicalactivityofsomederivativesofwarfarin