Synthesis of <i>N</i>-<i>p</i>-Fluorothiosemicarbazone and of Bis(<i>N</i>-<i>p</i>-Fluorophenylthiourea): Crystal Structure and Conformational Analysis of <i>N,N</i>′-Bis(4-Fluorophenyl)Hydrazine-1,2-Bis(Carbothioamide)

Synthesis of <i>N</i>-<i>p</i>-Fluorothiosemicarbazone and of Bis(<i>N</i>-<i>p</i>-Fluorophenylthiourea): Crystal Structure and Conformational Analysis of <i>N,N</i>′-Bis(4-Fluorophenyl)Hydrazine-1,2-Bis(Carbothioamide)

The reaction of the phosphonated hydrazone (2-hydrazineylidenepropyl) diphenylphosphine oxide <b>1</b> with <i>p</i>-fluorophenyl-isothiocyanate yields as a major product the thiosemicarbazone Ph<sub>2</sub>P(=O)CH<sub>2</sub>{C=N-NH(C=S)-N(H)C<sub&...

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Bibliographic Details
Main Authors: Sirine Salhi, Dorra Kanzari-Mnallah, Isabelle Jourdain, Michael Knorr, Carsten Strohmann, Jan-Lukas Kirchhoff, Hédi Mrabet, Azaiez Ben Akacha
Format: Article
Language:English
Published: MDPI AG 2024-11-01
Series:Molbank
Subjects:
thiourea
thiosemicarbazone
crystal structure
conformational analysis
supramolecular network
Online Access:https://www.mdpi.com/1422-8599/2024/4/M1926
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