A modular click ligand-directed approach to label endogenous dopamine D1 receptors in live cells

Abstract Most luminescence-based technologies to determine the pharmacological properties of G Protein-Coupled Receptors (GPCRs) rely on the overexpression of genetically modified receptors. However, it is essential to develop approaches allowing the specific labelling of native receptors. Here we r...

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Main Authors: Xavier Gómez-Santacana, Marin Boutonnet, Carles Martínez-Juvés, Marta Cimadevila, Juanlo Catena, Enora Moutin, Thomas Roux, Eric Trinquet, Laurent Lamarque, Julie Perroy, Laurent Prézeau, Jurriaan M. Zwier, Jean-Philippe Pin, Amadeu Llebaria
Format: Article
Language:English
Published: Nature Portfolio 2025-04-01
Series:Communications Chemistry
Online Access:https://doi.org/10.1038/s42004-025-01504-3
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author Xavier Gómez-Santacana
Marin Boutonnet
Carles Martínez-Juvés
Marta Cimadevila
Juanlo Catena
Enora Moutin
Thomas Roux
Eric Trinquet
Laurent Lamarque
Julie Perroy
Laurent Prézeau
Jurriaan M. Zwier
Jean-Philippe Pin
Amadeu Llebaria
author_facet Xavier Gómez-Santacana
Marin Boutonnet
Carles Martínez-Juvés
Marta Cimadevila
Juanlo Catena
Enora Moutin
Thomas Roux
Eric Trinquet
Laurent Lamarque
Julie Perroy
Laurent Prézeau
Jurriaan M. Zwier
Jean-Philippe Pin
Amadeu Llebaria
author_sort Xavier Gómez-Santacana
collection DOAJ
description Abstract Most luminescence-based technologies to determine the pharmacological properties of G Protein-Coupled Receptors (GPCRs) rely on the overexpression of genetically modified receptors. However, it is essential to develop approaches allowing the specific labelling of native receptors. Here we report an innovative approach based on the use of molecular modules to build fluorescent ligand-directed probes that can label aminergic GPCRs. Such probes are readily prepared with a click reaction between a ligand that may include nucleophilic groups and a fluorescent electrophilic linker. The rapidity of click reaction before receptor labelling prevents a side reaction between the nucleophilic ligand and the electrophile. This approach allowed us to label D1 receptor in transfected cells and native receptors in neural cell lines, leaving the receptor fully functional. This approach will pave the way to develop new reagents and assays with which to monitor endogenous GPCRs’ distribution, trafficking, activity or binding properties in their native environment.
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spelling doaj-art-475b92cf00574b8199be82a06d9eb1212025-08-20T02:16:56ZengNature PortfolioCommunications Chemistry2399-36692025-04-018111210.1038/s42004-025-01504-3A modular click ligand-directed approach to label endogenous dopamine D1 receptors in live cellsXavier Gómez-Santacana0Marin Boutonnet1Carles Martínez-Juvés2Marta Cimadevila3Juanlo Catena4Enora Moutin5Thomas Roux6Eric Trinquet7Laurent Lamarque8Julie Perroy9Laurent Prézeau10Jurriaan M. Zwier11Jean-Philippe Pin12Amadeu Llebaria13Institut de Génomique Fonctionnelle, Université de Montpellier, CNRS and INSERMInstitut de Génomique Fonctionnelle, Université de Montpellier, CNRS and INSERMMedicinal Chemistry & Synthesis, Institute for Advanced Chemistry of Catalonia (IQAC), Spanish Council for Scientific Research (CSIC)Institut de Génomique Fonctionnelle, Université de Montpellier, CNRS and INSERMMedicinal Chemistry & Synthesis, Institute for Advanced Chemistry of Catalonia (IQAC), Spanish Council for Scientific Research (CSIC)Institut de Génomique Fonctionnelle, Université de Montpellier, CNRS and INSERMRevvityRevvityRevvityInstitut de Génomique Fonctionnelle, Université de Montpellier, CNRS and INSERMInstitut de Génomique Fonctionnelle, Université de Montpellier, CNRS and INSERMRevvityInstitut de Génomique Fonctionnelle, Université de Montpellier, CNRS and INSERMMedicinal Chemistry & Synthesis, Institute for Advanced Chemistry of Catalonia (IQAC), Spanish Council for Scientific Research (CSIC)Abstract Most luminescence-based technologies to determine the pharmacological properties of G Protein-Coupled Receptors (GPCRs) rely on the overexpression of genetically modified receptors. However, it is essential to develop approaches allowing the specific labelling of native receptors. Here we report an innovative approach based on the use of molecular modules to build fluorescent ligand-directed probes that can label aminergic GPCRs. Such probes are readily prepared with a click reaction between a ligand that may include nucleophilic groups and a fluorescent electrophilic linker. The rapidity of click reaction before receptor labelling prevents a side reaction between the nucleophilic ligand and the electrophile. This approach allowed us to label D1 receptor in transfected cells and native receptors in neural cell lines, leaving the receptor fully functional. This approach will pave the way to develop new reagents and assays with which to monitor endogenous GPCRs’ distribution, trafficking, activity or binding properties in their native environment.https://doi.org/10.1038/s42004-025-01504-3
spellingShingle Xavier Gómez-Santacana
Marin Boutonnet
Carles Martínez-Juvés
Marta Cimadevila
Juanlo Catena
Enora Moutin
Thomas Roux
Eric Trinquet
Laurent Lamarque
Julie Perroy
Laurent Prézeau
Jurriaan M. Zwier
Jean-Philippe Pin
Amadeu Llebaria
A modular click ligand-directed approach to label endogenous dopamine D1 receptors in live cells
Communications Chemistry
title A modular click ligand-directed approach to label endogenous dopamine D1 receptors in live cells
title_full A modular click ligand-directed approach to label endogenous dopamine D1 receptors in live cells
title_fullStr A modular click ligand-directed approach to label endogenous dopamine D1 receptors in live cells
title_full_unstemmed A modular click ligand-directed approach to label endogenous dopamine D1 receptors in live cells
title_short A modular click ligand-directed approach to label endogenous dopamine D1 receptors in live cells
title_sort modular click ligand directed approach to label endogenous dopamine d1 receptors in live cells
url https://doi.org/10.1038/s42004-025-01504-3
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