Sugar Alcohols as Crosslinking Delay Additives for Fracturing Fluids

The development of thermally stable fracturing fluids is essential for the effective stimulation of deep and low-permeability reservoirs. The stabilizing additives used in these fluids typically fall into three categories: crosslinking delay molecules, oxygen scavengers, and pH buffers. However, man...

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Main Authors: Tariq Almubarak, Mohammed I. Alabdrabalnabi, Abdualilah Albaiz, Mohammed Yami
Format: Article
Language:English
Published: MDPI AG 2025-06-01
Series:Gels
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Online Access:https://www.mdpi.com/2310-2861/11/6/457
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author Tariq Almubarak
Mohammed I. Alabdrabalnabi
Abdualilah Albaiz
Mohammed Yami
author_facet Tariq Almubarak
Mohammed I. Alabdrabalnabi
Abdualilah Albaiz
Mohammed Yami
author_sort Tariq Almubarak
collection DOAJ
description The development of thermally stable fracturing fluids is essential for the effective stimulation of deep and low-permeability reservoirs. The stabilizing additives used in these fluids typically fall into three categories: crosslinking delay molecules, oxygen scavengers, and pH buffers. However, many conventional additives raise toxicity and environmental concerns, prompting the search for safer alternatives. This study investigates the use of sugar alcohols, commonly used as low-calorie sweeteners, as environmentally responsible additives for high-temperature fracturing fluids. A guar-based fluid system was formulated at a pH of 10 and evaluated using a high-pressure high-temperature (HPHT) rheometer under simulated field pumping conditions at 300 °F for a 90 min period. The viscosity was measured at a shear rate of 100 s<sup>−1</sup>, with intermittent low-shear rates introduced to assess the structural recovery and fluid integrity. The effect of sugar alcohol concentration on crosslinking delay was examined across systems containing varying amounts of a zirconium-based crosslinker ranging from 1 to 4 gpt. The results demonstrated that sugar alcohols effectively delayed crosslinking, allowing for controlled viscosity development and improved stability at elevated temperatures. When optimized at concentrations of 2 ppt of the sugar alcohol with 4 gpt of the crosslinker, the fluid generated a peak viscosity of 600 cP after 2.5 min and maintained a viscosity above 300 cP throughout the 90 min test. Breaker results showed a controlled viscosity reduction, with final viscosity values reaching 10 cP. The proppant settling experiments confirmed the suspension of more than 95% of the proppant during the treatment window. These findings highlight the potential of sugar alcohols as effective and environmentally safer crosslinking delay additives for hydraulic fracturing applications.
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institution Kabale University
issn 2310-2861
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spelling doaj-art-463a5ca409c44bca993feb3bf19b80652025-08-20T03:27:25ZengMDPI AGGels2310-28612025-06-0111645710.3390/gels11060457Sugar Alcohols as Crosslinking Delay Additives for Fracturing FluidsTariq Almubarak0Mohammed I. Alabdrabalnabi1Abdualilah Albaiz2Mohammed Yami3EXPEC Advanced Research Center—Saudi Aramco, Dhahran 31311, Saudi ArabiaEXPEC Advanced Research Center—Saudi Aramco, Dhahran 31311, Saudi ArabiaEXPEC Advanced Research Center—Saudi Aramco, Dhahran 31311, Saudi ArabiaEXPEC Advanced Research Center—Saudi Aramco, Dhahran 31311, Saudi ArabiaThe development of thermally stable fracturing fluids is essential for the effective stimulation of deep and low-permeability reservoirs. The stabilizing additives used in these fluids typically fall into three categories: crosslinking delay molecules, oxygen scavengers, and pH buffers. However, many conventional additives raise toxicity and environmental concerns, prompting the search for safer alternatives. This study investigates the use of sugar alcohols, commonly used as low-calorie sweeteners, as environmentally responsible additives for high-temperature fracturing fluids. A guar-based fluid system was formulated at a pH of 10 and evaluated using a high-pressure high-temperature (HPHT) rheometer under simulated field pumping conditions at 300 °F for a 90 min period. The viscosity was measured at a shear rate of 100 s<sup>−1</sup>, with intermittent low-shear rates introduced to assess the structural recovery and fluid integrity. The effect of sugar alcohol concentration on crosslinking delay was examined across systems containing varying amounts of a zirconium-based crosslinker ranging from 1 to 4 gpt. The results demonstrated that sugar alcohols effectively delayed crosslinking, allowing for controlled viscosity development and improved stability at elevated temperatures. When optimized at concentrations of 2 ppt of the sugar alcohol with 4 gpt of the crosslinker, the fluid generated a peak viscosity of 600 cP after 2.5 min and maintained a viscosity above 300 cP throughout the 90 min test. Breaker results showed a controlled viscosity reduction, with final viscosity values reaching 10 cP. The proppant settling experiments confirmed the suspension of more than 95% of the proppant during the treatment window. These findings highlight the potential of sugar alcohols as effective and environmentally safer crosslinking delay additives for hydraulic fracturing applications.https://www.mdpi.com/2310-2861/11/6/457hydraulic fracturingrheologyviscosity controlproppant suspensionoxidizers breakersustainability
spellingShingle Tariq Almubarak
Mohammed I. Alabdrabalnabi
Abdualilah Albaiz
Mohammed Yami
Sugar Alcohols as Crosslinking Delay Additives for Fracturing Fluids
Gels
hydraulic fracturing
rheology
viscosity control
proppant suspension
oxidizers breaker
sustainability
title Sugar Alcohols as Crosslinking Delay Additives for Fracturing Fluids
title_full Sugar Alcohols as Crosslinking Delay Additives for Fracturing Fluids
title_fullStr Sugar Alcohols as Crosslinking Delay Additives for Fracturing Fluids
title_full_unstemmed Sugar Alcohols as Crosslinking Delay Additives for Fracturing Fluids
title_short Sugar Alcohols as Crosslinking Delay Additives for Fracturing Fluids
title_sort sugar alcohols as crosslinking delay additives for fracturing fluids
topic hydraulic fracturing
rheology
viscosity control
proppant suspension
oxidizers breaker
sustainability
url https://www.mdpi.com/2310-2861/11/6/457
work_keys_str_mv AT tariqalmubarak sugaralcoholsascrosslinkingdelayadditivesforfracturingfluids
AT mohammedialabdrabalnabi sugaralcoholsascrosslinkingdelayadditivesforfracturingfluids
AT abdualilahalbaiz sugaralcoholsascrosslinkingdelayadditivesforfracturingfluids
AT mohammedyami sugaralcoholsascrosslinkingdelayadditivesforfracturingfluids