Scintillation proximity assay for DNA binding by human p53

Many DNA binding proteins are known to regulate gene expression. When that binding is altered, a disease state can result. A common method for measuring DNA binding, namely electrophoretic mobility shift assay (EMSA) is often used but it is not amenable to rapid screening of many samples. As an alte...

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Main Authors: Susannah Gal, Jeffery R. Cook, Leighton Howells
Format: Article
Language:English
Published: Taylor & Francis Group 2006-09-01
Series:BioTechniques
Online Access:https://www.future-science.com/doi/10.2144/000112222
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author Susannah Gal
Jeffery R. Cook
Leighton Howells
author_facet Susannah Gal
Jeffery R. Cook
Leighton Howells
author_sort Susannah Gal
collection DOAJ
description Many DNA binding proteins are known to regulate gene expression. When that binding is altered, a disease state can result. A common method for measuring DNA binding, namely electrophoretic mobility shift assay (EMSA) is often used but it is not amenable to rapid screening of many samples. As an alternative method, we have developed a DNA binding assay for the tumor suppressor protein p53 in a 96-well microtiter plate format using scintillation proximity assay (SPA) beads. We have shown this assay to be sensitive (as little as 0.5 ng p53 can be detected), quick (assay completed in as little as 15 min), and easily quantitated using a microtiter plate scintillation counter. We also used the assay to analyze the kinetics of the DNA binding to p53. The specificity of this p53 DNA binding SPA was confirmed using competition by oligonucleotides either from the same gene or from mutated versions of this sequence. Thus, SPA is a good alternative to gel shift assays for DNA binding and may be useful for the analysis of multiple tumor cell samples or for high-throughput screens for compounds affecting DNA binding by proteins of interest.
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spelling doaj-art-3e1de05120af4d64ae491bafdf9c2c142025-08-20T02:25:54ZengTaylor & Francis GroupBioTechniques0736-62051940-98182006-09-0141330330810.2144/000112222Scintillation proximity assay for DNA binding by human p53Susannah Gal0Jeffery R. Cook1Leighton Howells21SUNY-Binghamton and BioLife Solutions, Binghamton, NY2Johnson & Johnson Pharmaceutical Research and Development, Raritan, NJ3GE Healthcare, Piscataway, NJ, USAMany DNA binding proteins are known to regulate gene expression. When that binding is altered, a disease state can result. A common method for measuring DNA binding, namely electrophoretic mobility shift assay (EMSA) is often used but it is not amenable to rapid screening of many samples. As an alternative method, we have developed a DNA binding assay for the tumor suppressor protein p53 in a 96-well microtiter plate format using scintillation proximity assay (SPA) beads. We have shown this assay to be sensitive (as little as 0.5 ng p53 can be detected), quick (assay completed in as little as 15 min), and easily quantitated using a microtiter plate scintillation counter. We also used the assay to analyze the kinetics of the DNA binding to p53. The specificity of this p53 DNA binding SPA was confirmed using competition by oligonucleotides either from the same gene or from mutated versions of this sequence. Thus, SPA is a good alternative to gel shift assays for DNA binding and may be useful for the analysis of multiple tumor cell samples or for high-throughput screens for compounds affecting DNA binding by proteins of interest.https://www.future-science.com/doi/10.2144/000112222
spellingShingle Susannah Gal
Jeffery R. Cook
Leighton Howells
Scintillation proximity assay for DNA binding by human p53
BioTechniques
title Scintillation proximity assay for DNA binding by human p53
title_full Scintillation proximity assay for DNA binding by human p53
title_fullStr Scintillation proximity assay for DNA binding by human p53
title_full_unstemmed Scintillation proximity assay for DNA binding by human p53
title_short Scintillation proximity assay for DNA binding by human p53
title_sort scintillation proximity assay for dna binding by human p53
url https://www.future-science.com/doi/10.2144/000112222
work_keys_str_mv AT susannahgal scintillationproximityassayfordnabindingbyhumanp53
AT jefferyrcook scintillationproximityassayfordnabindingbyhumanp53
AT leightonhowells scintillationproximityassayfordnabindingbyhumanp53