Stereochemistry of the Carbon-Nitrogen Bond Cleavage by Chloroformate Esters

Nicotine reacts with chloroformic esters to give the chloro-carbamates resulting from the cleavage of the C2' –N1' bond. The reaction is shown to proceed with at least 96 to 98 % inversion of configuration. In the same way, (R)-(+)-N,N-dimethyl-α-phenethylamine gave (S)-(−)-α-phenethyl ch...

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Main Authors: C. Hootelé, J.P. Lenders
Format: Article
Language:deu
Published: Swiss Chemical Society 1974-11-01
Series:CHIMIA
Online Access:https://www.chimia.ch/chimia/article/view/9188
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author C. Hootelé
J.P. Lenders
author_facet C. Hootelé
J.P. Lenders
author_sort C. Hootelé
collection DOAJ
description Nicotine reacts with chloroformic esters to give the chloro-carbamates resulting from the cleavage of the C2' –N1' bond. The reaction is shown to proceed with at least 96 to 98 % inversion of configuration. In the same way, (R)-(+)-N,N-dimethyl-α-phenethylamine gave (S)-(−)-α-phenethyl chloride with inversion.
format Article
id doaj-art-183f4fcfd9fb404b963b4bb8cb936526
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language deu
publishDate 1974-11-01
publisher Swiss Chemical Society
record_format Article
series CHIMIA
spelling doaj-art-183f4fcfd9fb404b963b4bb8cb9365262025-08-20T02:20:27ZdeuSwiss Chemical SocietyCHIMIA0009-42932673-24241974-11-01281110.2533/chimia.1974.665Stereochemistry of the Carbon-Nitrogen Bond Cleavage by Chloroformate EstersC. Hootelé0J.P. Lenders1Service de Chimie Organique - Faculté des Sciences - Université Libre de Bruxelles, BelgiqueService de Chimie Organique - Faculté des Sciences - Université Libre de Bruxelles, Belgique Nicotine reacts with chloroformic esters to give the chloro-carbamates resulting from the cleavage of the C2' –N1' bond. The reaction is shown to proceed with at least 96 to 98 % inversion of configuration. In the same way, (R)-(+)-N,N-dimethyl-α-phenethylamine gave (S)-(−)-α-phenethyl chloride with inversion. https://www.chimia.ch/chimia/article/view/9188
spellingShingle C. Hootelé
J.P. Lenders
Stereochemistry of the Carbon-Nitrogen Bond Cleavage by Chloroformate Esters
CHIMIA
title Stereochemistry of the Carbon-Nitrogen Bond Cleavage by Chloroformate Esters
title_full Stereochemistry of the Carbon-Nitrogen Bond Cleavage by Chloroformate Esters
title_fullStr Stereochemistry of the Carbon-Nitrogen Bond Cleavage by Chloroformate Esters
title_full_unstemmed Stereochemistry of the Carbon-Nitrogen Bond Cleavage by Chloroformate Esters
title_short Stereochemistry of the Carbon-Nitrogen Bond Cleavage by Chloroformate Esters
title_sort stereochemistry of the carbon nitrogen bond cleavage by chloroformate esters
url https://www.chimia.ch/chimia/article/view/9188
work_keys_str_mv AT chootele stereochemistryofthecarbonnitrogenbondcleavagebychloroformateesters
AT jplenders stereochemistryofthecarbonnitrogenbondcleavagebychloroformateesters