Direct 4D printing of hydrogels driven by structural topology

Four-dimensional (4D) printing combines shape-morphing materials and three-dimensional (3D) printing technology, enabling efficient fabrication of complex shape-changing structures. However, 4D printing of hydrogels into structures with complex shapes suffers from poor printability, which limit thei...

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Main Authors: Huijun Li, Paulo Jorge Da Silva Bartolo, Kun Zhou
Format: Article
Language:English
Published: Taylor & Francis Group 2025-12-01
Series:Virtual and Physical Prototyping
Subjects:
Online Access:https://www.tandfonline.com/doi/10.1080/17452759.2025.2462962
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author Huijun Li
Paulo Jorge Da Silva Bartolo
Kun Zhou
author_facet Huijun Li
Paulo Jorge Da Silva Bartolo
Kun Zhou
author_sort Huijun Li
collection DOAJ
description Four-dimensional (4D) printing combines shape-morphing materials and three-dimensional (3D) printing technology, enabling efficient fabrication of complex shape-changing structures. However, 4D printing of hydrogels into structures with complex shapes suffers from poor printability, which limit their practical applications. Here, we present an efficient strategy for direct 4D printing of hydrogels, leveraging intricate structural designs and highly viscous hydrogels. This strategy facilitates programmable shape-morphing through precise control of filament spacing and orientation, resulting in gradient swelling behaviours when the structures are immersed in a Ca2+-ion solution. Our study also reveals the critical role of printability in improving shape-morphing performance. On this basis, we propose a practical solution to enhance the shape-morphing capability of hydrogels with limited inherent performance by improving their printability through the addition of viscous additives such as MC or PVA. Overall, this strategy expands the list of hydrogels suitable for 4D printing, demonstrating compatibility with both synthetic and natural hydrogels, including Alginate/Methylcellulose (ALG/MC), gelatin methacryloyl (GELMA), and ALG/polyvinyl alcohol (PVA). Various sophisticated plant-inspired shape-morphing behaviours can be achieved in 4D-printed hydrogels through precise control of structural topology. The combined strategy of employing highly viscous hydrogel with intricate structural design demonstrates vast potential for applications in biomimetic soft robotics.
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institution Kabale University
issn 1745-2759
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publishDate 2025-12-01
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series Virtual and Physical Prototyping
spelling doaj-art-0573f6ea8db047e88fd12be3fee1c7732025-08-20T03:48:14ZengTaylor & Francis GroupVirtual and Physical Prototyping1745-27591745-27672025-12-0120110.1080/17452759.2025.2462962Direct 4D printing of hydrogels driven by structural topologyHuijun Li0Paulo Jorge Da Silva Bartolo1Kun Zhou2Singapore Centre for 3D Printing, School of Mechanical and Aerospace Engineering, Nanyang Technological University, Singapore, SingaporeSingapore Centre for 3D Printing, School of Mechanical and Aerospace Engineering, Nanyang Technological University, Singapore, SingaporeSingapore Centre for 3D Printing, School of Mechanical and Aerospace Engineering, Nanyang Technological University, Singapore, SingaporeFour-dimensional (4D) printing combines shape-morphing materials and three-dimensional (3D) printing technology, enabling efficient fabrication of complex shape-changing structures. However, 4D printing of hydrogels into structures with complex shapes suffers from poor printability, which limit their practical applications. Here, we present an efficient strategy for direct 4D printing of hydrogels, leveraging intricate structural designs and highly viscous hydrogels. This strategy facilitates programmable shape-morphing through precise control of filament spacing and orientation, resulting in gradient swelling behaviours when the structures are immersed in a Ca2+-ion solution. Our study also reveals the critical role of printability in improving shape-morphing performance. On this basis, we propose a practical solution to enhance the shape-morphing capability of hydrogels with limited inherent performance by improving their printability through the addition of viscous additives such as MC or PVA. Overall, this strategy expands the list of hydrogels suitable for 4D printing, demonstrating compatibility with both synthetic and natural hydrogels, including Alginate/Methylcellulose (ALG/MC), gelatin methacryloyl (GELMA), and ALG/polyvinyl alcohol (PVA). Various sophisticated plant-inspired shape-morphing behaviours can be achieved in 4D-printed hydrogels through precise control of structural topology. The combined strategy of employing highly viscous hydrogel with intricate structural design demonstrates vast potential for applications in biomimetic soft robotics.https://www.tandfonline.com/doi/10.1080/17452759.2025.2462962Programmable shape-morphing4D printinghydrogelsoft robotic
spellingShingle Huijun Li
Paulo Jorge Da Silva Bartolo
Kun Zhou
Direct 4D printing of hydrogels driven by structural topology
Virtual and Physical Prototyping
Programmable shape-morphing
4D printing
hydrogel
soft robotic
title Direct 4D printing of hydrogels driven by structural topology
title_full Direct 4D printing of hydrogels driven by structural topology
title_fullStr Direct 4D printing of hydrogels driven by structural topology
title_full_unstemmed Direct 4D printing of hydrogels driven by structural topology
title_short Direct 4D printing of hydrogels driven by structural topology
title_sort direct 4d printing of hydrogels driven by structural topology
topic Programmable shape-morphing
4D printing
hydrogel
soft robotic
url https://www.tandfonline.com/doi/10.1080/17452759.2025.2462962
work_keys_str_mv AT huijunli direct4dprintingofhydrogelsdrivenbystructuraltopology
AT paulojorgedasilvabartolo direct4dprintingofhydrogelsdrivenbystructuraltopology
AT kunzhou direct4dprintingofhydrogelsdrivenbystructuraltopology