-
121
Synthesis of TiO2/Pd and TiO2/PdO Hollow Spheres and Their Visible Light Photocatalytic Activity
Published 2020-01-01“…The structure and optical properties of the as-prepared samples were characterized by X-ray diffraction, field emission scanning electron microscopy, transmission electron microscopy, Brunauer-Emmett-Telleranalysis, Barrett-Joyner-Halenda measurement, and UV-Vis diffuse reflectance spectroscopy. The photocatalysis efficiencies of all samples were evaluated through the photocatalytic degradation of rhodamine B under visible light irradiation. …”
Get full text
Article -
122
Photocatalytic Degradation of Acid Red and Acid Black Dyes Using Mn-Doped SrTiO₃ Perovskite Nanostructures
Published 2025-08-01“…The substances have been synthesized thru the sol-gel path and comprehensively characterized using X-ray Diffraction (XRD), Scanning Electron Microscopy (SEM), Transmission Electron Microscopy (TEM), Ultraviolet–Visible Diffuse Reflectance Spectroscopy (UV-Vis/DRS), Brunauer–Emmett–Teller (BET) surface analysis, and Fourier Transform Infrared Spectroscopy (FTIR). surface analysis. …”
Get full text
Article -
123
Enhanced LED light driven photocatalytic degradation of Cefdinir using bismuth titanate nanoparticles
Published 2025-07-01“…Bismuth titanate nanoparticles were synthesized and characterized using transmission electron microscopy (TEM), X-ray diffraction (XRD), and diffuse reflectance spectroscopy (DRS). Factors affecting the degradation protocol were optimized using a central composite design model, and the degradation efficiency was assessed using a validated RP-HPLC method. …”
Get full text
Article -
124
Photocatalytic Reduction of CO2 to Methane on Pt/TiO2 Nanosheet Porous Film
Published 2014-01-01“…The Pt/TiO2 nanosheet porous film was characterized by means of X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscope (TEM), and ultraviolet-visible light diffuse reflectance spectra (UV-vis DRS). Moreover, the transient photocurrent-time curves showed that the Pt/TiO2 nanosheet porous film exhibited higher photocurrent, indicating that the higher separation efficiency of the photogenerated charge carriers was achieved.…”
Get full text
Article -
125
Blue to Yellow Photoluminescence Emission and Photocatalytic Activity of Nitrogen Doping in TiO2 Powders
Published 2015-01-01“…The resulting powders were characterized using field emission scanning electron microscopy, X-ray diffraction, diffuse reflectance spectroscopy, Raman spectroscopy, Fourier transformation infrared spectroscopy, and photoluminescence emission spectroscopy (PL). …”
Get full text
Article -
126
Automatic and Rapid Discrimination of Cotton Genotypes by Near Infrared Spectroscopy and Chemometrics
Published 2012-01-01“…This paper reports the application of near infrared (NIR) spectroscopy and pattern recognition methods to rapid and automatic discrimination of the genotypes (parent, transgenic, and parent-transgenic hybrid) of cotton plants. Diffuse reflectance NIR spectra of representative cotton seeds (n=120) and leaves (n=123) were measured in the range of 4000–12000 cm−1. …”
Get full text
Article -
127
The NaBH4 Reduction and pH Effects on the Optical Property of Bismuth Vanadate
Published 2025-01-01“…Optical absorption data using a UV-visible diffuse reflectance spectrophotometer showed that the reduction process increases the maximum absorption edge to 575 nm and reduces the band gap energy to 2.78 eV at high pH. …”
Get full text
Article -
128
Impregnation of ZnO onto a Vegetal Activated Carbon from Algerian Olive Waste: A Sustainable Photocatalyst for Degradation of Ethyl Violet Dye
Published 2019-01-01“…The synthesized AC-ZnO material was characterized using powder X-ray diffraction, BET surface area measurements, Raman microscopy, thermogravimetric analysis, UV-visible diffuse reflectance spectroscopy, and zeta potential measurements. …”
Get full text
Article -
129
Electrochemical and physical properties of magnesioferrite nanomaterial and photocatalytic degradation of methylene blue
Published 2025-01-01“…The optical characteristics and crystalline structure of the MgFe2O4 nanomaterials were analysed using photoluminescence, diffuse reflectance spectroscopy, and X-ray diffraction. …”
Get full text
Article -
130
Layered double hydroxides (ZnAl-NO3-LDH) to mixed metal oxides: A promising pathway for sustainable NOx abatement
Published 2025-10-01“…The resulting ZnO-based LDOs were characterized via X-ray diffraction (XRD), Fourier Transform Infrared spectroscopy (FTIR), thermogravimetric analysis (TGA), scanning electron microscopy (SEM-EDS), and diffuse reflectance spectroscopy. The photocatalysts demonstrated a conversion efficiency of 27–29 % for NO photocatalytic conversion, with a notable reduction in NO₂ release (3–4 %) and a high selectivity of up to 91 % under light intensities of 20 and 40 W/m². …”
Get full text
Article -
131
Improved activity of SnO for the photocatalytic oxygen evolution
Published 2018-01-01“…The forbidden band, determined from the diffuse reflectance is found to be 1.46 eV. The electrical conductivity occurs by polaron hopping and follows an Arrhenius type law with activation energy of 0.21 eV, the change in the slope at 526 K is attributed to the oxidation to SnO2. …”
Get full text
Article -
132
Tailoring Al-Doped ZnO Nanoparticles via Scalable High-Energy Ball Milling–Solid-State Reaction: Structural, Optical, and Dielectric Insights for Light-Activated Antimicrobial Defe...
Published 2025-04-01“…This study reports the synthesis of aluminum-doped ZnO nanoparticles (Al-ZnO NPs) via a top-down mechanochemical solid-state reaction (SSR) approach using high-energy ball milling (HEBM) as a rapid, controllable, and efficient method. Al-ZnO samples were characterized using X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FT-IR), transmission electron microscopy (TEM), scanning electron microscopy (SEM), energy-dispersive spectroscopy (EDS), and UV-Vis diffuse reflectance spectroscopy. …”
Get full text
Article -
133
Design of AgI/BiVO4 heterostructures for photocatalytic antibiotic removal and antimicrobial action
Published 2025-01-01“…To examine their structural and optical properties, a suite of characterization methods, including energy-dispersive x-ray spectroscopy (EDX), Raman spectroscopy, transmission electron microscopy (TEM), field emission scanning electron microscopy (FE-SEM), x-ray diffraction (XRD), and diffuse reflectance spectroscopy (DRS), was utilized. …”
Get full text
Article -
134
Synthesis O-g-C<sub>3</sub>N<sub>4</sub>/TiO<sub>2</sub> rutile composite material for photocatalytic application
Published 2019-11-01“…Obtaining O-g-C3N4/TiO2 binary composite was confirmed through various analytical techniques including X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS) and ultraviolet-visible diffuse reflectance spectra (UV-Vis-DRS) methods. …”
Get full text
Article -
135
Synthesis and Application of Fe-Doped TiO2-Halloysite Nanotubes Composite and Their Potential Application in Water Treatment
Published 2019-01-01“…The photocatalyst-adsorbent composite (TiO2-Fe-HNTs) was synthesized by the hydrothermal method and characterized by X-ray diffraction, thermogravimetric analysis, Fourier-transform infrared spectroscopy, scanning electron microscopy-energy dispersive X-ray spectroscopy, and diffuse reflectance spectroscopy. The adsorption and photocatalysis mechanism by the TiO2-Fe-HNT composite were examined on methylene blue dye, rhodamine blue dye, naproxen sodium (pharmaceutical drug waste), and imidacloprid (pesticide). …”
Get full text
Article -
136
Preparation and Photocatalytic Dye Degradation Properties of CeO2 / BiOI Heterojunction
Published 2023-06-01“…X-ray powder diffraction ( XRD), scanning electron microscope ( SEM), ultraviolet-visible diffuse reflectance spectroscopy ( UV-Vis DRS) and electrochemistry were used to characterize the prepared samples, and the effects of CeO2 calcination temperatures and different mass ratios on the photocatalytic degradation efficiency were evaluated by the degradation experiments of rhodamine B ( RhB) . …”
Get full text
Article -
137
Enhancing cement-based inorganic coating performance through the integration of graphene-titanium dioxide composite nanofibers
Published 2025-07-01“…The 650 °C sample, on the other hand, contained 87.1 % of the anatase and 16.9 % rutile phases, with the lowest photocatalytic efficiency of 70 %. Photoluminescence (PL) and diffuse reflectance spectroscopy (DRS) tests revealed that the incorporation of graphene mitigated electron-hole recombination rates, resulting in a redshifted spectrum. …”
Get full text
Article -
138
Fe-TiO2 Nanoparticles Synthesized by Green Chemistry for Potential Application in Waste Water Photocatalytic Treatment
Published 2019-01-01“…The cathodoluminescence (CL) and photoluminescence (PL) studies of the doped and undoped nanoparticles show a luminescence signal attributed to surface oxygen vacancies (visible CL emission 380–700 nm and PL emission 350–800 nm); additionally, a decrease in emission intensity is observed due the inhibition of the recombination of the photogenerated electron-holes pairs; moreover, nanopowders were analyzed by UV-Vis spectrophotometry of diffuse reflectance, and the absorption edge of the Fe-TiO2 in comparison to undoped TiO2 is extended greatly toward the visible light. …”
Get full text
Article -
139
Surface and quantum chemical parameters of nickel oxide nanostructures suited for ultraviolet-assisted cationic dye degradation
Published 2024-04-01“…Fourier transform infrared spectroscopy and energy dispersive X-ray were employed to analyze the functional group and elemental composition of NiO NPs. The ultraviolet diffuse reflectance spectra indicated an optical band gap of 3.08 eV for synthesized NiO nanoparticles. …”
Get full text
Article -
140
Synthesis of Zinc Oxide-based nanocomposites for photocatalytic removal of contaminant
Published 2024-11-01“…The samples were characterized by X-ray diffraction (XRD), field emission scanning electron microscope (FESEM), Fourier transform infrared spectroscopy (FT-IR), and diffuse reflectance spectroscopy (DRS). The XRD results revealed that zinc oxide and graphite carbon nitride have a hexagonal wurtzite structure and a hexagonal structure, respectively. …”
Get full text
Article