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Development and Validation of a High‐Performance Liquid Chromatography Method for the Determination of Epoxyaurapten From Pomelo Peel
Published 2025-08-01“…The effects of extraction solvent, liquid‐to‐material ratio, ultrasonic time, and extraction cycles on the extraction of epoxyaurapten from pomelo peel were investigated, and the optimal sample pretreatment conditions were determined to ensure the extraction efficiency. The results indicated a high degree of precision with a linear correlation coefficient of 0.9999. …”
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487
Simultaneous Determination of Multiple Acid-Suppressing Drugs by UPLC-MS/MS Method and Application for Pharmacokinetics Study
Published 2025-02-01“…Precisely quantifying their plasma levels is crucial for clinical pharmacokinetic assessments and therapeutic drug monitoring.Aim: This study aimed to establish a generic and efficient ultra-performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS) assay for the determination of five PPIs (esomeprazole, rabeprazole, ilaprazole, lansoprazole, and pantoprazole) and the P-CAB (vonoprazan) in human plasma.Methods: The six analytes were extracted from human plasma via protein precipitation and a single dilution step. …”
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488
Continuous Flow Injection Analysis Method for the Determination of a Drug Diphenhydramine Hydrochloride by Using Phosphomolybdic Acid
Published 2024-08-01“… The study presented a new method for determining diphenhydramine hydrochloride (DPH) in its pure form and some pharmaceutical preparations, within CFIA technique. …”
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489
Determination of Crack Resistance of the Cover and Slide Glass by Indentation Method with the Visualization Using Atomic Force Microscopy
Published 2024-04-01“…Crack resistance was determined by the Vickers pyramid indentation method. …”
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490
Determination of morphine, codeine and 6-monoacetylmorphine in saliva of substance-abuse patients using HPLC/MS methods
Published 2012-01-01“…Saliva represents an alternative specimen for substances abuse determination in toxicology. Hence, the aim of this study was to optimize a method for saliva specimen preparation for heroin metabolites, morphine and 6-monoacetylmorphine (6-mam), and codeine determination by liquid chromatography-mass spectrometry (LC/MS), and to apply this method on saliva samples taken from the patients. …”
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491
A Validated RP HPLC-PAD Method for the Determination of Hederacoside C in Ivy-Thyme Cough Syrup
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Establishment of QuEChERS-UPLC-MS/MS method to determine three kinds of ochratoxins in coffee
Published 2023-12-01“…<b>Objective:</b> A new method was developed for the simultaneous determination of three kinds of ochratoxins in coffee by ultra-high performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS) combined with QuEChERS pretreatment. …”
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493
Analytical Methods for the Determination of the Distribution of Total Petroleum Hydrocarbons in the Water and Sediment of Aquatic Systems: A Review
Published 2017-01-01“…Several methods of extraction and analytical determination for total petroleum hydrocarbons (TPHCs) in aqueous and solid samples are reviewed. …”
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494
ALTERNATIVE METHOD FOR DETERMINING METAL UPTAKE FROM WATER BY ESCHERICHIA COLI K12 CD3
Published 2025-06-01“…By comparison, usual TEM-EDX analyzes show that the concentration was not qualitatively determined. At the same time, the ICP-M device was not as efficient in measuring cadmium concentrations. …”
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Determination of neutron spectrum parameters at IREN facility using the MCNP simulation and experimental validation
Published 2025-01-01“…Our revised equation for determination of a shape parameter by the method of cadmium-ratio for multi-monitor has been used, in which the correction coefficients of the epithermal neutron transmission for cadmium cover, the thermal and epithermal neutron self-shielding, were included for improvement of the accuracy. …”
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497
Energy Efficiency of Heat Pumps Heating Systems at Subsoil Waters for South-East Regions of Europe
Published 2020-12-01“…This article is devoted to the methods for increasing the operational efficiency of the single-stage and two-stage schemes of heat pump installations for heating systems, based on the energy saving principles. …”
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498
Estimation of Damage Degree of Buildings in Earthquakes by Statistical Modeling Method
Published 2024-09-01“…After transforming the elements of these databases, new statistical characteristics of damageability were obtained with variation coefficient values less than 0.30. The research results can be used to determine the seismic load calculation through the permissible damage coefficient.…”
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Estimation of Reverberation Time in Classrooms Using the Residual Minimization Method
Published 2017-11-01“…The objective of the residual minimization method is to determine a coefficient correcting the Sabine’s model. …”
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500
Common inaccuracies and errors in the application of statistical methods in soil science
Published 2020-07-01“…Any statement about the type of relationship between features based on the correlation coefficient (Pearson or Spearman) is meaningless without specifying the number of replicates, since it is the number of replicates that determines the significance of the difference between the correlation coefficient and zero. …”
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