-
241
Further investigation on microstructure refinement of internal crack initiation region in VHCF regime of high-strength steels
Published 2019-05-01“…The profile samples prepared by focused ion beam (FIB) in crack initiation region (CIR) and fish-eye (FiE) region of failed specimens subjected to rotary bending (RB) and ultrasonic axial (UL) fatigue testing with various stress ratios (R) were observed by transmission electron microscopy (TEM) with selected area electron diffraction (SAD) detection for two high-strength steels. …”
Get full text
Article -
242
Study on the degradation mechanism of mechanical properties of red sandstone under static and dynamic loading after different high temperatures
Published 2025-04-01“…Abstract To study the effect of high temperature on the mechanical properties of red sandstone, YNS600 electro-hydraulic servo universal testing machine and pneumatic separating Hopkinson press bar (SHPB) device were respectively used to conduct static and dynamic load loading tests on red sandstone after 500~1000 ℃ action, and X diffraction detection. The damage pattern and mechanical property index changes before and after high temperature action were compared, and the relationship between mineral composition, microstructure and mechanical parameters of the specimens and temperature was analyzed, and a theoretical model was constructed. …”
Get full text
Article -
243
Development of BaSrTiO3 nanomaterial based dispersive solid phase microextraction method for cadmium determination in thyme samples using flame atomic absorption spectrometry
Published 2025-07-01“…Characterization techniques including XRD (X-ray Diffraction), FTIR (Fourier transform infrared spectroscopy), and SEM (scanning electron microscopy) were utilized for characterizing the synthesized nanomaterial. …”
Get full text
Article -
244
Quercetin-conjugated magnetic nanoparticles inhibit Staphylococcus aureus growth and biofilm formation via downregulation of Coa and Hla genes
Published 2025-07-01“…Biofilm detection experiments showed that 95% of studied microorganisms had moderate-to-strong biofilm formation abilities. …”
Get full text
Article -
245
Poly(butylene adipate-co-terephthalate) (PBAT)/AgFe2O4 biopolymer nanocomposite-based flexible triboelectric nanogenerator as a self-powered touch sensor
Published 2025-07-01“…AgFe2O4 (AFO) nanoparticles, synthesized via combustion, were characterized using X-ray diffraction (XRD) and Fourier transform infrared (FTIR) spectroscopy. …”
Get full text
Article -
246
Monitoring ocular disease via optical nanostructures potentially applicable to corneal contact lens products
Published 2024-06-01“…The nanostructures produced a 4° diffraction angle difference in response to the environmental changes. …”
Get full text
Article -
247
Preparation of Magnetic Molecularly Imprinted Polymers for Selective Recognition and Determination of Clenbuterol in Pork Samples
Published 2020-01-01“…MMIPs were successfully applied as adsorbents to preconcentrated CLB in pork samples and detected by HPLC with UV. The limit of detection (LOD) and limit of quantification (LOQ) were 4.27 μg/L and 14.2 μg/L, respectively. …”
Get full text
Article -
248
Microstructural Evolution of UNS S32205 Duplex Stainless Steel During Cold Rolling and Subsequent Annealing
Published 2025-02-01“…Strain-induced martensite was not detected within this strain range by using X-ray diffraction and DC-magnetisation measurements. …”
Get full text
Article -
249
Synthesis and characterization of hematite nanomaterials imprinted with acetone, ethanol and methanol for AI-Based IoT gas sensor arrays
Published 2025-08-01“…Among the models, RF-GB exhibited the lowest limit of detection (LOD), while RF presented relatively higher LOD values. …”
Get full text
Article -
250
Effect of particle size on release of solid dispersed particles during the "Dissolution" test
Published 2025-06-01“…Amorphism was determined by X-ray powder diffraction and electron microscopy. The efficiency of disperse systems was compared based on the results of the "Dissolution" test of powders mechanically ground to the same particle size in the biological pH range. …”
Get full text
Article -
251
Spray-printed ZnO thin film for high-sensitivity NO2 gas sensing
Published 2025-06-01“…Abstract The controlling and precise detection of nitrogen dioxide (NO2) gas is important in many industrial processes such as medical, petrochemical, and agriculture. …”
Get full text
Article -
252
Antibacterial Efficacy of Solid-State Cu²⁺ Exchanged Clinoptilolite: Structural Characterization and Microbial Resistance
Published 2025-05-01“…The results revealed slight modifications in the crystalline structure of clinoptilolite, along with the detection of both Cu2+ ions and copper oxide after the ion exchange process. …”
Get full text
Article -
253
The Solid Phase Extraction of Some Metal Ions Using Palladium Nanoparticles Attached to Silica Gel Chemically Bonded by Silica-Bonded N-Propylmorpholine as New Sorbent prior to The...
Published 2012-01-01“…In this research at first palladium nanoparticle attached to a new chemically bonded silica gel has been synthesized and has been characterized with different techniques such as X-ray diffraction (XRD), fourier transform infrared (FT-IR), transmission electron microscopy (TEM), and scanning electron microscopy (SEM). …”
Get full text
Article -
254
A surface-modified graphene – carbon-based composite sensor for the voltammetric assessment of pyridoxine in food and pharmaceutical samples
Published 2024-12-01“…Scanning electron microscopy (SEM), X-ray diffraction (XRD), Energy dispersive X-ray (EDX) and Electrochemical impedance spectroscopy (EIS) were employed to gain a deep insight into the surface modification and elemental analysis of the unmodified graphene carbon paste sensor (UGCPS) and PGMGCPS. …”
Get full text
Article -
255
Electrochemical Determination of Diclofenac by Using ZIF-67/g-C3N4 Modified Electrode
Published 2021-01-01“…The obtained materials were characterized by using X-ray diffraction, scanning electron microscopy (SEM), EDX-mapping, and nitrogen adsorption/desorption isotherms. …”
Get full text
Article -
256
Analytical Study of Zinc Sulphide Electrode Prepared from Nano material
Published 2023-02-01“…ZnS NPs electrode and ZnS Non- NPs electrode give linear range upon (10-5-10-2)M and (10-4-10-2)M, Nernstain slope of (30.35 mV/decade) and (30.84 mV/decade), correlation coefficient of (0.9999) and (0.9995), detection limit of (1.733x10-7)M and (2.486x10-6)M, quantitative limit of (5.77x10-7)M and (7.07x10-6)M, the response time of (9-39) second and (13-36) second, respectively. …”
Get full text
Article -
257
Revealing Resistive Switching of Phase Transitions in an Al‐Doped Single Crystal of VO2 by DC and Pulsed Electrical Measurements
Published 2025-02-01“…Under low‐current R(T) measurements, the T(M1 → M2) and IMT are the only once detected by X‐ray diffraction that show reproducible resistive switching (RS) and hysteresis typical of first‐order transitions. …”
Get full text
Article -
258
Laser-based 3D printing and optical characterization of optical micro-nanostructures inspired by nocturnal insects compound eyes
Published 2025-01-01“…For example, the development of 3D micro-nanostructures that mimic nocturnal insect eyes (optimized for night vision), emerges as promising technology for detection in IR spectral region. Here, we report a proof of principle concerning the design and laser 3D printing of all ultrastructural details of nocturnal moth Grapholita Funebrana eyes, for potential use as microlens arrays for IR detection systems. …”
Get full text
Article -
259
Tuning surface interactions with bentonite-graphite composite material for fouling-resistant electrochemical sensing of phenol in olive mill wastewater
Published 2025-07-01“…The sensor achieved a low limit of detection (LOD) of 0.015 μM and a quantification limit (LOQ) of 0.052 μM. …”
Get full text
Article -
260
Carbon Nano-Onions–Polyvinyl Alcohol Nanocomposite for Resistive Monitoring of Relative Humidity
Published 2025-05-01“…The composition and morphology of the sensing film are explored by means of scanning electron microscopy, Raman spectroscopy, atomic force microscopy, and X-ray diffraction. The manufactured sensor’s room temperature RH detection performance is examined by applying a continuous flow of the electric current between the interdigitated electrodes and measuring the voltage as the RH varies from 5% to 95%. …”
Get full text
Article