Insights into the effects of biomass feedstock and pyrolysis conditions on the energy storage capacity and durability of standard biochar-based phase-change composites by Dimberu G. Atinafu, Ji Yong Choi, Jihee Nam, Yujin Kang, Sumin Kim

“…The PCM adsorption ratio of biochars derived from rice husk (RH) and Miscanthus straw linearly correlated with the pyrolysis temperature (550–700 °C), while RH700 resulted in a composite with a high enthalpy per unit mass of hexadecane (HXD) in RH700/HXD (250.9 J g−1) owing to the high surface area of RH700 (74.66 m2 g−1). …”
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A versatile HPLC method collaborated with NaDES-ultrasound-assisted LLE and machine learning for purity testing and trace analysis of 1,4-benzodiazepines in crime scene evidence, h... by Walaa Nabil Abd-AlGhafar, Rasha Abo Shabana, Rania El-Shaheny, Manar M. Tolba

“…The method showed excellent linearity and a high sensitivity with detection limits of 0.34, 0.18, and 0.04 µg mL−1 for CDP, ALP, and DZP, respectively. …”
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Development of a superheated water chromatography method for the sustainable determination of preservatives in foods and cosmetics by Roberta La Tella, Danilo Donnarumma, Francesca Rigano, Paola Donato, Patrik Appelblad, Paola Dugo, Luigi Mondello, Alice Mondello

“…The method combined eco-sustainable sample preparation with high-temperature LC separation on a PGC column and was fully validated in terms of linearity, precision, accuracy and detection and quantification limits. …”
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Design, synthesis, SAR and ADMET analyses of the novel class of synthetic 7-amino[1,2,5]oxadiazolo[3,4-b]pyridine-6-carboxylate derivatives with vasorelaxant activity by Anatolii Varenyk, Roman Vydzhak, Svitlana Panchishin, Irina Ivanova, Victor Zhirnov, Volodymyr Brovarets

“…Moreover, in the series of compounds with n-alkyl and cycloalkyl substituents, the derivative activity decreased linearly as the number of carbon atoms diminished. …”
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Development and Validation of an HPLC-MS/MS Method for the Simultaneous Quantification of Vitexin and Isovitexin in Rabbit Plasma: Pharmacokinetic Insights on a Microcapsule Formul... by Duc Tuan Nguyen, Trung Nguyen Nguyen Le, Duc Kien Ngo, Hien Minh Khuu, Khang Thien Tran, Hoang Thanh Le, Hung Viet Tran, Truong-Thang Nguyen Phan, Vo Thi Kim Khuyen, Han Hoang Do, Nhu Huynh Mai, Quan Minh Le

“…An LC-MS/MS method was developed and validated for the simultaneous determination of vitexin and isovitexin in the plasma of treated rabbits, using salicylic acid as the internal standard. Raw rabbit plasma samples were deproteinized using acetonitrile as a precipitation agent. …”
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Electroencephalography estimates brain age in infants with high precision: Leveraging advanced machine learning in healthcare by Saeideh Davoudi, Gabriela Lopez Arango, Florence Deguire, Inga Sophie Knoth, Fanny Thebault-Dagher, Rebecca Reh, Laurel Trainor, Janet Werker, Sarah Lippé

“…Additionally, the developing brain follows a trajectory characterized by increased non-linearity and complexity in which alpha rhythm plays an important role. …”
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Agronomic performance of curly lettuce seedlings from mill compost substrate under organic cropping system by Luiz Fernando de Sousa Antunes, Adelson Paulo Araújo, Maria Elizabeth Fernandes Correia, Norma Gouvêa Rumjanek, José Guilherme Marinho Guerra

“…Fresh commercial weight, head diameter, and number of leaves of lettuce plants increased linearly as applied N levels increased. These traits were superior in plants from seedlings produced with millicompost than with commercial substrate. …”
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Joint effects of atrial fibrillation and prothrombotic genotypes on the risk of venous thromboembolism by Erin Mathiesen Hald, Maja–Lisa Løchen, Kristian Hveem, Mary Cushman, Sigrid K. Brækkan, John–Bjarne Hansen

“…In participants without AF, the VTE risk increased linearly with increasing genetic risk score. No such association was found for those with AF. …”
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Reprotoxicity of zinc oxide nanoparticles synthesized with Crataegus monogyna leaves extract: testis and sperm function by F. REMITA, A. TALBI, C. ABDENNOUR, K. KHELILI, Y. BEDOUH, F. HAMOUD, F. DUMAN, Z. BOUSLAMA, R. ROUABHI, M. R. DJEBAR

“…Epididymis sperm was collected for sperm parameters: concentration, live sperm, motility, velocity (VCL, VSL, and VAP), linearity (LIN), amplitude lateral head (ALH), and beat cross frequency (BCF). …”
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Quantification of Total and Unbound Selinexor Concentrations in Human Plasma by a Fully Validated Liquid Chromatography-Tandem Mass Spectrometry Method by Suhyun Lee, Seungwon Yang, Hyeonji Kim, Wang-Seob Shim, Eunseo Song, Seunghoon Han, Sung-Soo Park, Suein Choi, Sungpil Han, Sung Hwan Joo, Seok Jun Park, Beomjin Shin, Donghyun Kim, Hyeon Su Kim, Kyung-Tae Lee, Eun Kyoung Chung

“…<b>Results:</b> Calibration curves showed excellent linearity over a range of 5–2000 ng/mL for total selinexor (r² ≥ 0.998) and 0.05–20 ng/mL for unbound selinexor (r² ≥ 0.995). …”
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Optimized Extraction Method for Neutral Cannabinoids Quantification Using UHPLC-HRMS/MS by João Victor Meirelles, Débora Cristina Diniz Estevam, Vanessa Farelo dos Santos, Henrique Marcelo Gualberto Pereira, Tatiana D. Saint Pierre, Valdir F. Veiga-Junior, Monica Costa Padilha

“…As a proof-of-concept, it enabled the efficient processing of 16 samples of commercial CHE within a three-hour timeframe, showcasing its practicality and reproducibility, and highlighting its potential for broader adoption in similar scenarios for both human and veterinary medicines.…”
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The effects of step-wise improvement of forage combination in total mixed rations on fatty acid profile in the rumen and milk of Holstein cows by Sarvvl BAI, Zhi-jun CAO, Xin JIN, Ya-jing WANG, Hong-jian YANG, Sheng-li LI

“…In response to the forage combination, ruminal concentration of C16:0, C18:2n-6 and C18:3n-3 linearly increased against their dietary intakes (P<0.10). …”
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Development of a transportable High-Performance Liquid Chromatograph with Ultraviolet detection and a method for the rapid analysis of 13 carbonyl compounds hydrazones by Audrey Grandjean, Anaïs Becker, Mathilde Mascles, Franck Amiet, Jean-Philippe Amiet, Damien Bazin, Stéphane Le Calvé

“…The system features a straightforward isocratic pump, ensuring reliability and ease of operation, while sample delivery is managed by a piston pump coupled to a multiplexing valve. …”
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Green RP-HPLC method for simultaneous quantification of epigallocatechin-3-gallate and rosmarinic acid in lipid-based nanocarriers and biological fluids: Quality by design-driven o... by Rahul Koli, V.S. Mannur

“…Recovery assays in lipid-based nanocarriers, plasma, and urine samples demonstrated excellent recoveries (96.2–102.1%). …”
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The Determination of Eight Biogenic Amines Using MSPE-UHPLC-MS/MS and Their Application in Regard to Changes in These Biogenic Amines in Traditional Chinese Dish-Pickled Swimming C... by Peipei Li, Yu Chen, Junlu Bai, Huicheng Yang, Pengfei He, Junjie Zeng

“…Method validation indicated that the developed method showed good linearity (R² > 0.995); the average recovery rates were 84.7% to 115%, with the intra-day and inter-day relative standard deviations (RSD, <i>n</i> = 6) ranging from 3.7% to 7.5% and 4.2% to 7.7%, respectively. …”
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Detection Methods for Asparagine and Glutamine Contents in Fruits and Vegetables and Recommendations for Dietary Intake of Fruits and Vegetables in Patients with Urea Cycle Disorde... by YE Xinyu, LI Ziying, TANG Shujun, SUN Liping, ZHAO Yunxia, XIAO Weimin, GU Yaping, KUANG Huiying, CHEN Xin, YANG Guowu, HUANG Yali

“…After enzymatic hydrolysis with Pronase E, samples were treated with butylated hydroxyanisole as an antioxidant. …”
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A Validated Trigonelline-Based Method for the Standardization and Quality Control of Trigonella foenum-graecum L. [version 3; peer review: 2 approved] by Rizwan Ahmad, Ali Alabduallah, Mohammed Aldholmi, Salma Hago

“…The UPLC-MS/MS method was developed and validated using a green mobile phase of H2O: EtOH, and an r2-value of 0.999 in the linearity range of 0.1-500 ppb was adopted. The method was validated with an accuracy of 98.6% for trace analysis of TG using a small amount (10 mg) of fenugreek samples from five different origins. …”
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Association between relative fat mass and sterility in women of reproductive age in the United States: results from the 2013–2018 NHANES by Mengmeng Sun, Mengmeng Sun, Yuxing Lu, Yuxing Lu, Xi Yang, Xiaogang Mao, Xiaogang Mao

“…Furthermore, RFM and sterility prevalence were found to be positively linearly correlated by RCS analysis, with sterility rates sharply increasing as RFM levels rose. …”
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LC-MS/MS-Based Determination and Optimization of Linoleic Acid Oxides in <i>Baijiu</i> and Their Variation with Storage Time by Cheng Fang, Xiaotong Zhuang, Zhanguo Li, Yongfang Zou, Jizhou Pu, Dong Wang, Yan Xu

“…Calibration curves exhibited excellent linearity (R² > 0.9990) across 1.0–100.0 ppb ranges. …”
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A pilot study on LC–MS/MS quantification of remifentanil, etomidate, and rocuronium in maternal and fetal serum microsamples by Hao Liu, Meng Cai, Yong Peng, Jing-kun Miao, Jin Yu

“…Method validation demonstrated excellent linearity (R2 > 0.99) for all compounds, with LLOQs of 0.15 ± 0.02 ng/mL (remifentanil), 16.87 ± 0.51 ng/mL (etomidate), and 106.73 ± 8.63 ng/mL (rocuronium). …”
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