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7701
EXPERIMENTAL SETUP FOR MODELING AND STUDY OF COMPLEX STRESS STATE IN FERROMAGNETIC MATERIALS
Published 2016-09-01“…The principle of operation of the device is based on the joint action at a sample of longitudinal extension and lateral bending. …”
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7702
Determination of the New Food Ingredient Pyrroloquinoline Quinone Disodium Salt in Foods by Centrifugal Ultrafiltration Coupled with High Performance Liquid Chromatography
Published 2025-04-01“…The limit of quantitation (LOQ) was 1.0 mg/kg for liquid samples and 4.0 mg/kg for soy sauce, semi-solid, and solid samples. …”
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7703
HPTLC-fluorescent densitometry for screening aflatoxin B1 in millet and buckwheat
Published 2025-05-01“…Apart from that, good linearity (0.999) was obtained within the range of 1−80 ng/band of AFB1. …”
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7704
Validation of Enzyme Immunoassay for Preclinical Pharmacokinetic Trials of Rituximab
Published 2019-06-01“…The within-run and between-run precision of the assay did not exceed 7.4 %, the total error of the method did not exceed 20.1 %. The linearity of dilution makes it possible to use the assay for the analysis of biological samples with a wide range of rituximab concentrations. …”
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7705
Validation of a method for the quantitative determination of narcotic and psychotropic substances in urine by UHPLC–MS/MS
Published 2022-07-01“…Selectivity, linearity, limits of qualitative determination, limit of quantitative determination (established under the contract with the customer firm), matrix effect, and measurement uncertainty were defined. …”
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7706
Study of closing time pattern and type of valve on water hammer phenomenon in water conveyance line
Published 2024-06-01“…In the third sample problem that the valve closure was exponential, hammer software estimate pressure head with 12 percent lower than AFT Impulse. …”
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7707
Development and validation of a QuEChERS-UPLC-MS/MS method for multi-class pesticide residue analysis in dairy products
Published 2025-12-01“…All pesticides showed excellent linearity (0.001–0.50 mg/L, R² > 0.99), with LOQs of 0.002 mg/kg. …”
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7708
Development and Validation of Pomalidomide Determination in Human Plasma by HPLC-MS/MS Method
Published 2020-11-01“…The method of the determination of pomalidomide in human plasma was developed and validated by HPLC-MS/MS. The linearity in plasma sample was achieved in the concentration range of 1,00 – 500,00 ng/ml. …”
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7709
Highly selective solid phase extraction of clonazepam from water using a urea modified MOF prior to HPLC analysis
Published 2025-07-01“…The developed method was successfully applied to real environmental water samples, confirming its practicality for environmental monitoring. …”
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7710
Green analytical protocol for the liquid chromatographic determination of ketoprofen in human urine after microextraction using Carbowax 20 M – modified cellulose membrane
Published 2025-05-01“…A Carbowax 20 M – modified cellulose membrane was utilized for the fabric sorptive phase extraction of ketoprofen from human urine samples followed by liquid chromatographic analysis. …”
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7711
Quantitative Determination of Ivermectin in Polymer Microspheres
Published 2022-02-01“…As a result of the development, the conditions for the analysis were selected, which allow us to evaluate the quantitative content of ivermectin in the sample. The method was validated for the parameters specificity, analytical area, linearity, trueness, repeatability, intermediate precision.…”
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7712
Residue determination of thiamethoxam and its metabolite clothianidin in okra using the modified QuEChERS method with d-SPE clean-up coupled with LC-MS/MS
Published 2024-12-01“…The developed method coupled with LC-MS/MS was applied to determine the residue amount in the collected samples. In 43 % of the samples, TMX residues were found in the range of 0.0051- 0.214 mg/Kg. …”
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7713
End-to-end Standardization of Original Medicines when Determining Related Impurities
Published 2023-12-01“…Column C18 250×4.6 mm, mobile phase 0.1% phosphoric acid and acetonitrile (gradient elution), flow rate 1 ml/min, sample volume 10 µl, UV detector (270 nm). They were validated in terms of specificity, linearity, detection limit, precision, robustness, and solution stability. …”
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7714
Comparison of inductively coupled plasma mass spectrometry and molybdenum blue colorimetry for total phosphorus determination in freshwater invertebrates.
Published 2025-01-01“…Total P in invertebrates determined using the two methods was strongly linearly correlated (r = 0.96) with a slope of 1.01. …”
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7715
Method Validation and Measurement Uncertainty Estimation for Determination of Multiclass Pesticide Residues in Tomato by Liquid Chromatography-Tandem Mass Spectrometry (LC-MS/MS)
Published 2024-01-01“…The calibration curves for all pesticides exhibited excellent linearities, with correlation coefficients exceeding 0.99. …”
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7716
Smartphone-Assisted Thin-Layer Chromatography for Rapid Quality Screening of Metformin
Published 2025-01-01“…The smartphone application, TLC Analyzer, accurately calculated the Rf values (0.604) consistent with those obtained using ImageJ software. The linearity of the method was 0.5–4 mg/mL. After optimization, the TLC Analyzer method was used to analyze metformin samples (n = 16) collected from local pharmacies. …”
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7717
Quantification of Rafoxanide Drug Residue from Sheep Meat in Sulaymaniyah Province/Iraq Using High-Performance Liquid Chromatography Hplc-Uv
Published 2023-09-01“…None of the testers were greater than Maximum Residual Limits (MRLs) legally established by the European Union (EU). 13 (26%) (n=50) samples were below MRLs, and 37 (74%) (n=50) samples were below the LOD.…”
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7718
ORDER IN THE CHAOS IN SPORTS ORGANIZATIONS
Published 2014-08-01“…Results: Results of this study, which have got through a single-sample t-test, show that sport organizations have six characteristics of welcoming to innovation, coherence, uncertainty, non-linearity, unpredictability, and ugly structure. …”
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7719
A straightforward Py-GC/MS methodology for quantification of microplastics in tap water
Published 2025-06-01“…Application to tap water samples revealed consistent detection of PS, ranging from 2.532 to 2.571 ng/L in morning samples and 0.867 to 1.540 ng/L in afternoon samples, with polypropylene and PE below the limit of quantification (<LOQ). …”
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7720
First HPLC-UV method for the determination of homocysteine thiolactone in human urine after derivatization with 1-benzyl-2-chloropyridinium bromide
Published 2025-03-01“…The method was successfully applied to urine samples delivered by apparently healthy donors. The presence of HTL was confirmed in twelve of eighteen study samples. …”
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