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7641
A New Method of Extraction and Measurement of Paraquat using BN/SPE Method Using High-Performance Liquid Chromatography
Published 2024-10-01“…In this paper, a novel extraction technique termed needle tip-based solid phase nano extraction was developed that describes a rapid method for the quantitative analysis of paraquat from an environmental water sample. Under the optimum extraction conditions, the method showed good linearity in the range of 1–100 µg/mL, acceptable reproducibility (RSD: 0.9507, n =4), and limits of detection (0.1µg/mL).…”
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7642
Extraction Efficiency of Different Solvents and LC-UV Determination of Biogenic Amines in Tea Leaves and Infusions
Published 2016-01-01“…Different extraction solvents have been tested and TCA 5% showed better analytical performances in terms of linearity, recovery percentages, LOD, LOQ, and repeatability than HCl 0.1 M and HClO4 0.1 M and was finally exploited for the quantitative determination of BAs in all samples. …”
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7643
Simultaneous determination of 12 pyrazine compounds in sauce-flavor Baijiu of different aging years by UPLC-MS/MS
Published 2024-10-01“…The results showed that 12 pyrazine compounds had a good linearity in the range of 50-1 000 μg/L (R<sup>2</sup>>0.99). …”
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7644
Prepartum supplementation of Ascophyllum nodosum meal or ethylenediamine dihydroiodide: Effects on colostrum yield and growth and health of dairy calves
Published 2025-04-01“…Plasma glucose concentration on d 5 of life decreased linearly in response to incremental levels of ASCO meal. …”
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7645
Newly Developed System For The Analysis Of Micro Quantites Of Molybdenum (VI) Using Flow Injection Analysis
Published 2007-06-01“…New microphotometer was constructed in our Laboratory Which deals with the determination of Molybdenum (VI) through its Catalysis effect on Hydrogen peroxide and potasum iodide Reaction in acid medium H2SO4 0.01 mM. Linearity of 97.3% for the range 5- 100 ppm. The repeatability of result was better than 0.8 % 0.5 ppm was obtanined as L.U. …”
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7646
The influence of 3D printing mode on the chemical composition and structure of 30HGSA steel
Published 2024-09-01“…It was found that the degree of loss of C, Cr and Si increases almost linearly and is directly proportional to the surfacing heat input (Q, J/mm). …”
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7647
Rapid Quantification of Gene Expression by Competitive RT-PCR and Ion-Pair Reversed-Phase HPLC
Published 1996-02-01“…IPRP-HPLC appears to offer important advantages to quantitative measurements of gene expression. These include rapid sample analysis and column re-equilibration, reduced sample handling and opportunity for introduction of quantification error, avoidance of fluorescent or radioactive tracers, high detector sensitivity and linearity and excellent quantitative reliability.…”
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7648
Estimation of some Organophosphorus Pesticides Using Carbon Paste Electrode Coupled with Molecularly Imprinted Polymers
Published 2018-09-01“…The extraction efficiency of the imprinted polymers has been evaluated by various parameters affecting to optimize the selective pre-concentration of OPPs from aqueous samples. The extraction efficiency of the MIPs-OPPs from environmental water samples was evaluated using carbon paste electrode and analytical parameters of the method, the slopes, linearity and detection limits of the liquid electrodes were ranged from 24.8 – 31.3 mV/decade , (10-1 - 10-7 ) mg L-1and (2.2-8.2x10-6) mg L-1, respectively with correlation coefficient (r) (0.9991-0.9998) and repeatability were established. …”
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7649
Lithium ferrite (LiFe5O8)/polymethyl methacrylate (PMMA) nano-composite used in high dielectric constant capacitor and electromagnetic applications
Published 2019-12-01“…The (I-V) characteristic of these nano-composites are in very good agreement with the non-linearity predicted by Kaiser et al. model. The effective dielectric constant is studied through different proposed models. …”
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7650
Quantification of Sensitization in Aluminum–Magnesium Alloys Through Frequency-Dependent Ultrasonic Attenuation
Published 2025-06-01“…By identifying the frequency range within which the attenuation parameter is linearly proportional to the frequency, the slopes of the frequency-attenuation relationship were determined and correlated with the DoS values of the sample plates. …”
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7651
Variable Selection for Generalized Single-Index Varying-Coefficient Models with Applications to Synergistic G × E Interactions
Published 2025-01-01“…Additionally, we assess the performance of our method through finite-sample simulations with both continuous and discrete gene variables. …”
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7652
Experimental study on friction resistance test of ultra-high-speed fracturing fluid in the mine
Published 2023-09-01“…The drag reduction rate of low-viscosity fracturing fluid and medium viscosity fracturing fluid show 4 kinds of trend with the increase of flow rate: decreasing linearly, increasing linearly, increasing first and then decreasing, and decreasing first and then increasing. …”
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7653
Development of a Gas Chromatography-Mass Spectrometry Method for the Quantification of Glucaric Acid Derivatives in Beverage Substrates
Published 2014-01-01“…The proposed method presented excellent intraday precision (%RSD < 10) and linearity for GL calibration curves (correlation coefficients > 0.995) and acceptable linearity for DGuA calibration curves (correlation coefficients > 0.97). …”
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7654
Development and Validation of Targeted Metabolomics Methods Using Liquid Chromatography–Tandem Mass Spectrometry (LC-MS/MS) for the Quantification of 235 Plasma Metabolites
Published 2025-02-01“…Fast polarity switching and scheduled SRM enhance the metabolome coverage and throughput, enabling the analysis of one sample in about 40 min. A simple “dilute and shoot” sample preparation protocol was employed, with samples injected at two dilution levels to align metabolite concentrations within calibration curve ranges. …”
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7655
Bioanalytical method validation to quantify ketorolac in human vitreous and aqueous via surrogate matrix of human plasma
Published 2025-12-01“…The method met the acceptance criteria with respect to selectivity, specificity, precision, accuracy, linearity, dilution integrity, and stability.Conclusions The validated method can use plasma as a surrogate matrix for quantitation of ketorolac in aqueous and vitreous humor, thereby eliminating the need to procure human vitreous and aqueous samples for validation prior to initiation of a clinical trial.…”
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7656
Evaluation of the presence of emerging contaminants in wastewater and seawater using automated solid-phase extraction and ultra-high-performance liquid chromatography coupled to ta...
Published 2024-11-01“…Matrix-matched calibration showed good linearity with determination coefficients ≥ 0.990. …”
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7657
Spectroscopic Determination of Fluoride Using Eriochrome Black T (EBT) as a Spectrophotometric Reagent from Groundwater
Published 2021-01-01“…The calibration curve, resulting in good linearity (R2 = 0.9997), was considered during quantitative analysis of the samples and in the spiking analysis. …”
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7658
Error-corrected ultradeep next-generation sequencing for detection of clonal haematopoiesis and haematological neoplasms - sensitivity, specificity and accuracy.
Published 2025-01-01“…Sequencing blood samples from 383 community-dwelling adults (mean depth 3758×) revealed 2,190 somatic variants/sample, > 99.9% were < 0.02 VAF. …”
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7659
Effect of Temperature on Interface Characteristics between Compacted Recycled Asphalt Pavement and Geogrid
Published 2023-01-01“…The shear strength consistently increases linearly with the increase of applied normal stress for all RAP samples. …”
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7660
Morphological and Optical Characterization of High Density Au/PAA Nanoarrays
Published 2016-01-01“…Also, the reflected intensities are decreased linearly for the as-prepared sample and decreased exponentially for Au/PAA samples. …”
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