Advanced machine learning models for the prediction of ceramic tiles’ properties during the firing stage

The firing stage is a critical phase in ceramic tile production, where the interplay of raw material composition and thermal treatment determines essential properties such as water absorption (WA) and bending strength (BS). This study employs advanced machine learning (ML) models to accurately predi...

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Main Authors: V. Vasic, Milica, Awoyera, Paul O., Fadugba, Oladlu George, Barisic, Ivana, Nettinger Grubeša, Ivanka
Format: Article
Language:English
Published: Scientific Reports 2025
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Online Access:http://hdl.handle.net/20.500.12493/2952
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author V. Vasic, Milica
Awoyera, Paul O.
Fadugba, Oladlu George
Barisic, Ivana
Nettinger Grubeša, Ivanka
author_facet V. Vasic, Milica
Awoyera, Paul O.
Fadugba, Oladlu George
Barisic, Ivana
Nettinger Grubeša, Ivanka
author_sort V. Vasic, Milica
collection KAB-DR
description The firing stage is a critical phase in ceramic tile production, where the interplay of raw material composition and thermal treatment determines essential properties such as water absorption (WA) and bending strength (BS). This study employs advanced machine learning (ML) models to accurately predict these properties by capturing their complex nonlinear relationships. A robust dataset of 312 ceramic samples was analyzed, including variables such as particle size distribution, chemical and mineralogical composition, and firing temperatures ranging from 1000 to 1300 °C. Among the four ensemble ML models evaluated, CatBoost demonstrated the highest predictive performance. Model accuracy was assessed using multiple evaluation metrics, including the coefficient of determination (R²), root mean squared error (RMSE), mean absolute error (MAE), and mean absolute percentage error (MAPE). To enhance interpretability, SHapley Additive exPlanations (SHAP) were used, revealing that clay mineral content and SiO₂ concentration were the most influential factors for WA, contributing approximately 40% and 30%, respectively. For BS, firing temperature (35%) and Al₂O₃ content (25%) were identified as the key predictors. Partial dependence plots further illustrated critical thresholds, such as a significant drop in WA above 62% SiO₂ and optimal BS values near 1200 °C, findings that align with known ceramic processing principles while offering new, data-driven formulation insights. These results demonstrate the value of explainable artificial intelligence (AI) in enabling real-time process optimization, enhancing product consistency, and supporting energy-efficient ceramic manufacturing. Future work will focus on extending the dataset to include a wider variety of clay compositions and investigating hybrid modeling approaches to further improve predictive performance.
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spelling oai:idr.kab.ac.ug:20.500.12493-29522025-10-01T00:00:34Z Advanced machine learning models for the prediction of ceramic tiles’ properties during the firing stage V. Vasic, Milica Awoyera, Paul O. Fadugba, Oladlu George Barisic, Ivana Nettinger Grubeša, Ivanka Ceramic tiles Firing stage Machine learning Water absorption Bending strength SHAP analysis Process optimization The firing stage is a critical phase in ceramic tile production, where the interplay of raw material composition and thermal treatment determines essential properties such as water absorption (WA) and bending strength (BS). This study employs advanced machine learning (ML) models to accurately predict these properties by capturing their complex nonlinear relationships. A robust dataset of 312 ceramic samples was analyzed, including variables such as particle size distribution, chemical and mineralogical composition, and firing temperatures ranging from 1000 to 1300 °C. Among the four ensemble ML models evaluated, CatBoost demonstrated the highest predictive performance. Model accuracy was assessed using multiple evaluation metrics, including the coefficient of determination (R²), root mean squared error (RMSE), mean absolute error (MAE), and mean absolute percentage error (MAPE). To enhance interpretability, SHapley Additive exPlanations (SHAP) were used, revealing that clay mineral content and SiO₂ concentration were the most influential factors for WA, contributing approximately 40% and 30%, respectively. For BS, firing temperature (35%) and Al₂O₃ content (25%) were identified as the key predictors. Partial dependence plots further illustrated critical thresholds, such as a significant drop in WA above 62% SiO₂ and optimal BS values near 1200 °C, findings that align with known ceramic processing principles while offering new, data-driven formulation insights. These results demonstrate the value of explainable artificial intelligence (AI) in enabling real-time process optimization, enhancing product consistency, and supporting energy-efficient ceramic manufacturing. Future work will focus on extending the dataset to include a wider variety of clay compositions and investigating hybrid modeling approaches to further improve predictive performance. 2025-09-30T17:14:39Z 2025-09-30T17:14:39Z 2025 Article Vasić, Milica V., et al. "Advanced machine learning models for the prediction of ceramic tiles’ properties during the firing stage." Scientific Reports 15.1 (2025): 31397. https://doi.org/10.1038/s41598-025-12011-9 http://hdl.handle.net/20.500.12493/2952 en Attribution-NonCommercial-NoDerivs 3.0 United States http://creativecommons.org/licenses/by-nc-nd/3.0/us/ application/pdf Scientific Reports
spellingShingle Ceramic tiles
Firing stage
Machine learning
Water absorption
Bending strength
SHAP analysis
Process optimization
V. Vasic, Milica
Awoyera, Paul O.
Fadugba, Oladlu George
Barisic, Ivana
Nettinger Grubeša, Ivanka
Advanced machine learning models for the prediction of ceramic tiles’ properties during the firing stage
title Advanced machine learning models for the prediction of ceramic tiles’ properties during the firing stage
title_full Advanced machine learning models for the prediction of ceramic tiles’ properties during the firing stage
title_fullStr Advanced machine learning models for the prediction of ceramic tiles’ properties during the firing stage
title_full_unstemmed Advanced machine learning models for the prediction of ceramic tiles’ properties during the firing stage
title_short Advanced machine learning models for the prediction of ceramic tiles’ properties during the firing stage
title_sort advanced machine learning models for the prediction of ceramic tiles properties during the firing stage
topic Ceramic tiles
Firing stage
Machine learning
Water absorption
Bending strength
SHAP analysis
Process optimization
url http://hdl.handle.net/20.500.12493/2952
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