Enrichment of patchouli alcohol in extracted patchouli oil from Pogostemon cablin benth leaves using supercritical carbon dioxide

Essential oil has been extensively applied in various industrial applications for different purposes. In this work, essential oil from the cultivated Pogostemon cablin Benth in Malang, Indonesia was extracted by supercritical carbon dioxide (CO2) method. The experiments were carried out in a semi ba...

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Main Authors: Wahyudiono, Ajeng Almira Tarisha Asri, Pramudya Riandana Bhayu Gautama, Sugeng Winardi, Tadafumi Adschiri, Motonobu Goto, Siti Machmudah
Format: Article
Language:English
Published: Elsevier 2025-06-01
Series:Case Studies in Chemical and Environmental Engineering
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Online Access:http://www.sciencedirect.com/science/article/pii/S2666016424004407
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author Wahyudiono
Ajeng Almira Tarisha Asri
Pramudya Riandana Bhayu Gautama
Sugeng Winardi
Tadafumi Adschiri
Motonobu Goto
Siti Machmudah
author_facet Wahyudiono
Ajeng Almira Tarisha Asri
Pramudya Riandana Bhayu Gautama
Sugeng Winardi
Tadafumi Adschiri
Motonobu Goto
Siti Machmudah
author_sort Wahyudiono
collection DOAJ
description Essential oil has been extensively applied in various industrial applications for different purposes. In this work, essential oil from the cultivated Pogostemon cablin Benth in Malang, Indonesia was extracted by supercritical carbon dioxide (CO2) method. The experiments were carried out in a semi batch-type process at various operating conditions (40−80 °C of temperatures and 10−20 MPa of pressures). The extraction time was 120 min, while the CO2 flow rates were 3–5 mL/min. The gas chromatography mass spectrometry (GC-MS) indicated that the extracted patchouli oil comprises patchouli alcohol as a main substance. The results indicated that the supercritical CO2 extraction method is to be superior compared with the hydrodistillation extraction method. By hydrodistillation extraction method, the extracted patchouli oil was around 0.52 %, while by supercritical CO2 extraction method, the extraction yield increased significantly to 3.04 %. Besides the high extraction yield, the supercritical CO2 extraction method also can give a high quality of patchouli oil extract.
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institution OA Journals
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publishDate 2025-06-01
publisher Elsevier
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series Case Studies in Chemical and Environmental Engineering
spelling doaj-art-fbd5df6f3edf4a1dab49db92482f49df2025-08-20T02:39:03ZengElsevierCase Studies in Chemical and Environmental Engineering2666-01642025-06-011110104610.1016/j.cscee.2024.101046Enrichment of patchouli alcohol in extracted patchouli oil from Pogostemon cablin benth leaves using supercritical carbon dioxide Wahyudiono0Ajeng Almira Tarisha Asri1Pramudya Riandana Bhayu Gautama2Sugeng Winardi3Tadafumi Adschiri4Motonobu Goto5Siti Machmudah6Department of Chemical Engineering, Institut Teknologi Sepuluh Nopember, Kampus ITS Sukolilo, Surabaya, 60111, IndonesiaDepartment of Chemical Engineering, Institut Teknologi Sepuluh Nopember, Kampus ITS Sukolilo, Surabaya, 60111, IndonesiaDepartment of Chemical Engineering, Institut Teknologi Sepuluh Nopember, Kampus ITS Sukolilo, Surabaya, 60111, IndonesiaDepartment of Chemical Engineering, Institut Teknologi Sepuluh Nopember, Kampus ITS Sukolilo, Surabaya, 60111, IndonesiaNew Industry Creation Hatchery Center, Tohoku University, 6-6-10 Aoba, Aramaki, Aoba-ku, Sendai, 980-8579, Japan; WPI – Advanced Institute for Materials Research, Tohoku University, 6-6-10 Aoba, Aramaki, Aoba-ku, Sendai, 980-8579, JapanDepartment of Materials Process Engineering, Nagoya University, Furo-cho, Chikusa-ku, Nagoya, 464-8063, Japan; Super Critical Technology Centre Co. Ltd., Kuwana, Mie, 511-0838, JapanDepartment of Chemical Engineering, Institut Teknologi Sepuluh Nopember, Kampus ITS Sukolilo, Surabaya, 60111, Indonesia; Corresponding author.Essential oil has been extensively applied in various industrial applications for different purposes. In this work, essential oil from the cultivated Pogostemon cablin Benth in Malang, Indonesia was extracted by supercritical carbon dioxide (CO2) method. The experiments were carried out in a semi batch-type process at various operating conditions (40−80 °C of temperatures and 10−20 MPa of pressures). The extraction time was 120 min, while the CO2 flow rates were 3–5 mL/min. The gas chromatography mass spectrometry (GC-MS) indicated that the extracted patchouli oil comprises patchouli alcohol as a main substance. The results indicated that the supercritical CO2 extraction method is to be superior compared with the hydrodistillation extraction method. By hydrodistillation extraction method, the extracted patchouli oil was around 0.52 %, while by supercritical CO2 extraction method, the extraction yield increased significantly to 3.04 %. Besides the high extraction yield, the supercritical CO2 extraction method also can give a high quality of patchouli oil extract.http://www.sciencedirect.com/science/article/pii/S2666016424004407Supercritical CO2EnrichmentExtractionPatchouli oilEssential oil
spellingShingle Wahyudiono
Ajeng Almira Tarisha Asri
Pramudya Riandana Bhayu Gautama
Sugeng Winardi
Tadafumi Adschiri
Motonobu Goto
Siti Machmudah
Enrichment of patchouli alcohol in extracted patchouli oil from Pogostemon cablin benth leaves using supercritical carbon dioxide
Case Studies in Chemical and Environmental Engineering
Supercritical CO2
Enrichment
Extraction
Patchouli oil
Essential oil
title Enrichment of patchouli alcohol in extracted patchouli oil from Pogostemon cablin benth leaves using supercritical carbon dioxide
title_full Enrichment of patchouli alcohol in extracted patchouli oil from Pogostemon cablin benth leaves using supercritical carbon dioxide
title_fullStr Enrichment of patchouli alcohol in extracted patchouli oil from Pogostemon cablin benth leaves using supercritical carbon dioxide
title_full_unstemmed Enrichment of patchouli alcohol in extracted patchouli oil from Pogostemon cablin benth leaves using supercritical carbon dioxide
title_short Enrichment of patchouli alcohol in extracted patchouli oil from Pogostemon cablin benth leaves using supercritical carbon dioxide
title_sort enrichment of patchouli alcohol in extracted patchouli oil from pogostemon cablin benth leaves using supercritical carbon dioxide
topic Supercritical CO2
Enrichment
Extraction
Patchouli oil
Essential oil
url http://www.sciencedirect.com/science/article/pii/S2666016424004407
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