Phase Transformation of VO2 Nanoparticles Assisted by Microwave Heating
The microwave assisted synthesis nowadays attracts a great deal of attention. Monoclinic phase VO2 (M) was prepared from NH4VO3 and H2C2O4·2H2O by a rapid microwave assisted technique. The synthesis parameters, microwave irradiation time, microwave power, and calcinations temperature were systematic...
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| Format: | Article |
| Language: | English |
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Wiley
2014-01-01
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| Series: | The Scientific World Journal |
| Online Access: | http://dx.doi.org/10.1155/2014/841418 |
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| author | Phatcharee Phoempoon Lek. Sikong |
| author_facet | Phatcharee Phoempoon Lek. Sikong |
| author_sort | Phatcharee Phoempoon |
| collection | DOAJ |
| description | The microwave assisted synthesis nowadays attracts a great deal of attention. Monoclinic phase VO2 (M) was prepared from NH4VO3 and H2C2O4·2H2O by a rapid microwave assisted technique. The synthesis parameters, microwave irradiation time, microwave power, and calcinations temperature were systematically varied and their influences on the structure and morphology were evaluated. The microwave power level has been carried out in range 180–600 W. TEM analysis demonstrated nanosized samples. The structural and morphological properties were measured using XRD, TEM, and thermal analyses. The variations of vanadium phase led to thermochromic properties. |
| format | Article |
| id | doaj-art-fb71da23ea604dc3b78494fda790b719 |
| institution | OA Journals |
| issn | 2356-6140 1537-744X |
| language | English |
| publishDate | 2014-01-01 |
| publisher | Wiley |
| record_format | Article |
| series | The Scientific World Journal |
| spelling | doaj-art-fb71da23ea604dc3b78494fda790b7192025-08-20T02:22:56ZengWileyThe Scientific World Journal2356-61401537-744X2014-01-01201410.1155/2014/841418841418Phase Transformation of VO2 Nanoparticles Assisted by Microwave HeatingPhatcharee Phoempoon0Lek. Sikong1Department of Mining and Materials Engineering, Faculty of Engineering, Prince of Songkla University, Hat Yai 90112, ThailandDepartment of Mining and Materials Engineering, Faculty of Engineering, Prince of Songkla University, Hat Yai 90112, ThailandThe microwave assisted synthesis nowadays attracts a great deal of attention. Monoclinic phase VO2 (M) was prepared from NH4VO3 and H2C2O4·2H2O by a rapid microwave assisted technique. The synthesis parameters, microwave irradiation time, microwave power, and calcinations temperature were systematically varied and their influences on the structure and morphology were evaluated. The microwave power level has been carried out in range 180–600 W. TEM analysis demonstrated nanosized samples. The structural and morphological properties were measured using XRD, TEM, and thermal analyses. The variations of vanadium phase led to thermochromic properties.http://dx.doi.org/10.1155/2014/841418 |
| spellingShingle | Phatcharee Phoempoon Lek. Sikong Phase Transformation of VO2 Nanoparticles Assisted by Microwave Heating The Scientific World Journal |
| title | Phase Transformation of VO2 Nanoparticles Assisted by Microwave Heating |
| title_full | Phase Transformation of VO2 Nanoparticles Assisted by Microwave Heating |
| title_fullStr | Phase Transformation of VO2 Nanoparticles Assisted by Microwave Heating |
| title_full_unstemmed | Phase Transformation of VO2 Nanoparticles Assisted by Microwave Heating |
| title_short | Phase Transformation of VO2 Nanoparticles Assisted by Microwave Heating |
| title_sort | phase transformation of vo2 nanoparticles assisted by microwave heating |
| url | http://dx.doi.org/10.1155/2014/841418 |
| work_keys_str_mv | AT phatchareephoempoon phasetransformationofvo2nanoparticlesassistedbymicrowaveheating AT leksikong phasetransformationofvo2nanoparticlesassistedbymicrowaveheating |