Synthesis of Alkyl α-Amino-benzylphosphinates by the Aza-Pudovik Reaction; The Preparation of the Butyl Phenyl-<i>H</i>-phosphinate Starting P-Reagent

Synthesis of Alkyl α-Amino-benzylphosphinates by the Aza-Pudovik Reaction; The Preparation of the Butyl Phenyl-<i>H</i>-phosphinate Starting P-Reagent

Butyl phenyl-<i>H</i>-phosphinate that is not available commercially was prepared from phenyl-<i>H</i>-phosphinic acid by three methods: by alkylating esterification (i), by microwave-assisted direct esterification (ii), and unexpectedly, by thermal esterification (iii). Cons...

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Bibliographic Details
Main Authors: Bence Bajusz, Dorka Nagy, Regina Tóth, Zsuzsanna Szalai, Ágnes Gömöry, Angéla Takács, László Kőhidai, György Keglevich
Format: Article
Language:English
Published: MDPI AG 2025-01-01
Series:Molecules
Subjects:
alkyl phenyl-<i>H</i>-phosphinates
aza-Pudovik reaction
Kabachnik–Fields reaction
α-aminophosphinates
microwave
cytotoxic activity
Online Access:https://www.mdpi.com/1420-3049/30/2/339
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