Singlet fission in heterogeneous lycopene aggregates

Abstract We have prepared lycopene aggregates with low scattering in an acetone–water suspension. The aggregates exhibit highly distorted absorption, extending from the UV up to 568 nm, as a result of strong excitonic interactions. We have investigated the structural organization of these aggregates...

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Main Authors: Chloe Magne, Vasyl Veremeienko, Roxanne Bercy, Minh-Huong Ha-Thi, Ana A. Arteni, Andrew A. Pascal, Mikas Vengris, Thomas Pino, Bruno Robert, Manuel J. Llansola-Portoles
Format: Article
Language:English
Published: Nature Portfolio 2025-02-01
Series:Scientific Reports
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Online Access:https://doi.org/10.1038/s41598-025-88220-z
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author Chloe Magne
Vasyl Veremeienko
Roxanne Bercy
Minh-Huong Ha-Thi
Ana A. Arteni
Andrew A. Pascal
Mikas Vengris
Thomas Pino
Bruno Robert
Manuel J. Llansola-Portoles
author_facet Chloe Magne
Vasyl Veremeienko
Roxanne Bercy
Minh-Huong Ha-Thi
Ana A. Arteni
Andrew A. Pascal
Mikas Vengris
Thomas Pino
Bruno Robert
Manuel J. Llansola-Portoles
author_sort Chloe Magne
collection DOAJ
description Abstract We have prepared lycopene aggregates with low scattering in an acetone–water suspension. The aggregates exhibit highly distorted absorption, extending from the UV up to 568 nm, as a result of strong excitonic interactions. We have investigated the structural organization of these aggregates by resonance Raman and TEM, revealing that the lycopene aggregates are not homogeneous, containing at least four different aggregate species. Transient absorption measurements upon excitation at 355, 515, and 570 nm, to sub-select these different species, reveal significant differences in dynamics between each of the aggregate types. The strong excitonic interactions produce extremely distorted transient electronic signatures, which do not allow an unequivocal identification of the excited states at times shorter than 60 ps. However, these experiments demonstrate that all the lycopene aggregated species form long-living triplets via singlet fission.
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publishDate 2025-02-01
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spelling doaj-art-fa14b781998944a187ef7cbef9e1a0722025-08-20T02:48:27ZengNature PortfolioScientific Reports2045-23222025-02-0115111210.1038/s41598-025-88220-zSinglet fission in heterogeneous lycopene aggregatesChloe Magne0Vasyl Veremeienko1Roxanne Bercy2Minh-Huong Ha-Thi3Ana A. Arteni4Andrew A. Pascal5Mikas Vengris6Thomas Pino7Bruno Robert8Manuel J. Llansola-Portoles9CEA, CNRS, Institute for Integrative Biology of the Cell (I2BC), Université Paris-SaclayCEA, CNRS, Institute for Integrative Biology of the Cell (I2BC), Université Paris-SaclayCEA, CNRS, Institute for Integrative Biology of the Cell (I2BC), Université Paris-SaclayCNRS, Institut Des Sciences Moléculaires d’Orsay, Université Paris-SaclayCEA, CNRS, Institute for Integrative Biology of the Cell (I2BC), Université Paris-SaclayCEA, CNRS, Institute for Integrative Biology of the Cell (I2BC), Université Paris-SaclayLaser Research Center, Faculty of Physics, Vilnius UniversityCNRS, Institut Des Sciences Moléculaires d’Orsay, Université Paris-SaclayCEA, CNRS, Institute for Integrative Biology of the Cell (I2BC), Université Paris-SaclayCEA, CNRS, Institute for Integrative Biology of the Cell (I2BC), Université Paris-SaclayAbstract We have prepared lycopene aggregates with low scattering in an acetone–water suspension. The aggregates exhibit highly distorted absorption, extending from the UV up to 568 nm, as a result of strong excitonic interactions. We have investigated the structural organization of these aggregates by resonance Raman and TEM, revealing that the lycopene aggregates are not homogeneous, containing at least four different aggregate species. Transient absorption measurements upon excitation at 355, 515, and 570 nm, to sub-select these different species, reveal significant differences in dynamics between each of the aggregate types. The strong excitonic interactions produce extremely distorted transient electronic signatures, which do not allow an unequivocal identification of the excited states at times shorter than 60 ps. However, these experiments demonstrate that all the lycopene aggregated species form long-living triplets via singlet fission.https://doi.org/10.1038/s41598-025-88220-zSelf-assembled lycopeneSinglet exciton fissionResonance RamanTransient absorption
spellingShingle Chloe Magne
Vasyl Veremeienko
Roxanne Bercy
Minh-Huong Ha-Thi
Ana A. Arteni
Andrew A. Pascal
Mikas Vengris
Thomas Pino
Bruno Robert
Manuel J. Llansola-Portoles
Singlet fission in heterogeneous lycopene aggregates
Scientific Reports
Self-assembled lycopene
Singlet exciton fission
Resonance Raman
Transient absorption
title Singlet fission in heterogeneous lycopene aggregates
title_full Singlet fission in heterogeneous lycopene aggregates
title_fullStr Singlet fission in heterogeneous lycopene aggregates
title_full_unstemmed Singlet fission in heterogeneous lycopene aggregates
title_short Singlet fission in heterogeneous lycopene aggregates
title_sort singlet fission in heterogeneous lycopene aggregates
topic Self-assembled lycopene
Singlet exciton fission
Resonance Raman
Transient absorption
url https://doi.org/10.1038/s41598-025-88220-z
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