Synthesis and Crystal Structure of 2-(Dichloromethyl)-2-(4-nitrophenyl)-1,3-dioxane

Synthesis and Crystal Structure of 2-(Dichloromethyl)-2-(4-nitrophenyl)-1,3-dioxane

A new compound, 2-dichloromethyl-2-p-nitrophenyl-1,3-dioxane, was synthesized and characterized. The crystal structure of the title compound (C11H11Cl2NO4, Mr=292.11) has been determined by single-crystal X-ray diffraction. The crystal is of monoclinic, space group P21/c with a=11.013(2) Å, b=14.653...

Full description

Saved in:

Bibliographic Details
Main Authors:	Fei Ye, Chang-Ying Sun, Ying Fu
Format:	Article
Language:	English
Published:	Wiley 2013-01-01
Series:	Journal of Chemistry
Online Access:	http://dx.doi.org/10.1155/2013/974174
Tags:	Add Tag No Tags, Be the first to tag this record!

Similar Items

Crystal structure of 2-(2-hydroxy-5-nitrophenyl)-5-methyl-1,3-dioxane-5-carboxylic acid, C12H13N1O7
by: Jia Guo-Kai, et al.
Published: (2022-08-01)

The crystal structure of (2-(4-chlorophenyl)-5-methyl-1,3-dioxan-5-yl)methanol, C12H15ClO3
by: Zou Long-Sheng, et al.
Published: (2021-09-01)

Crystal structure of (Z)-2-(1-bromo-2-phenylvinyl)-5-ethyl-2-methyl-1,3-dioxane-5-carboxylic acid, C15H17Br1O4
by: Jia Guo-Kai, et al.
Published: (2022-08-01)

Crystal structure of 4-chloro-N′-[(1E)-(2-nitrophenyl)methylidene]benzohydrazide, C14H10ClN3O3
by: Al-Wahaibi Lamya H., et al.
Published: (2023-08-01)

The crystal structure of the co-crystal 1,4-dioxane–4,6-bis(nitroimino)-1,3,5-triazinan-2-one(2/1), C11H19N7O9
by: Guannan Zhao, et al.
Published: (2023-10-01)

Synthesis of 3-Phenyl-4[4-(m-nitrophenyl)-N-2-(2’-arylureido / arylthioureido-4’-N-morpholino-s-triazin)-benzo-[6,7]-coumarins and their Applicatiions
by: J. P. Raval, et al.
Published: (2004-01-01)

Crystal structure of 1-(4–chlorophenyl)-4-benzoyl-3-methyl-1H-pyrazol-5-ol, C17H13ClN2O2
by: Xu Li-Ying, et al.
Published: (2023-10-01)

Synthesis and crystal structure of 1-(7-hydroxy-3-(4-hydroxy-3-nitrophenyl)-4-oxo-4H-chromen-8-yl)-N,N-dimethylmethanaminiumnitrate, C18H17N3O9
by: Chen Hai-Lin, et al.
Published: (2023-10-01)

Direct ring fluorination of 3-substituted 5-(1,3-dioxane) acetal isoxazoles: application to the formal synthesis of a bioactive fluorinated isoxazole
by: Bacheley, Lucas, et al.
Published: (2024-02-01)

Synthesis and crystal structure analysis of 1-ethyl-1,3-dihydro-2H-benzo[d]imidazole-2-thione
by: Atash V. Gurbanov, et al.
Published: (2025-02-01)

Crystal structure of 1,3-diisopropyl-4,5-dimethylimidazol-2-ylidene-N,N′-bis(1,3-bis(2,6-diisopropylphenyl)-1,3-dihydro-2H-1,3,2-diazaborol-2-yl)-l2-germenediamine, C63H94B2GeN8
by: Wang Bing, et al.
Published: (2023-10-01)

Synthesis and crystal structures of 4,4′-methylenebis(2,6-diethylaniline) and 4,4′-methylenebis(3-chloro-2,6-diethylaniline)
by: Daniil E. Smirnov, et al.
Published: (2025-02-01)

Synthesis, Crystal Structure, and DFT Study of N′-(2,4-Dinitrophenyl)-2-Fluorobenzohydrazide
by: Aamer Saeed, et al.
Published: (2013-01-01)

Synthesis, Crystal Structure, and Theoretical Studies of N-(4-((4-chlorobenzyl)oxy)phenyl)-4- (trifluoromethyl)pyrimidin-2-amine
by: Jian-Chang Jin, et al.
Published: (2013-01-01)

The crystal structure of dimethyl 2,2ʹ-((adamantane-1,3-diylbis(4,1-phenylene)) bis(oxy))diacetate, C28H32O6
by: Chen Xiao-Ming, et al.
Published: (2023-08-01)

Crystal structure of 4-(2,2-difluoroethyl)-2,4-dimethyl-6-(trifluoromethyl)isoquinoline-1,3(2H,4H)-dione, C14H12F5NO2
by: Liu Jianlian, et al.
Published: (2021-09-01)

Synthesis and crystal structure of [Sr(urea)(NO3)2]n
by: Aysanem Bektursinova, et al.
Published: (2025-02-01)

Synthesis and crystal structure (E)-1-(4-bromo-2-hydroxyphenyl)-3-(dimethylamino)prop-2-en-1-one, C11H12BrNO2
by: Dong Zhang-Chao, et al.
Published: (2023-08-01)

The crystal structure of 4-((6-fluoropyridin-2-yloxy)methyl)benzonitrile, C13H9FN2O
by: Lu Zhi-Qiang
Published: (2022-08-01)

Crystal structure of 2-[(4-bromobenzyl)thio]-5-(5-bromothiophen-2-yl)-1,3,4-oxadiazole, C13H8Br2N2OS2
by: Al-Omary Fatmah A. M., et al.
Published: (2023-10-01)

Crystal structure of methyl 3-(1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)propanoate, C16H13NO4
by: Wang Tiantian, et al.
Published: (2022-08-01)

Synthesis and crystal structure of di-tert-butyl 1″-acetyl-2,2″,9′-trioxo-4a′,9a′-dihydro-1′H,3′H,9′H-dispiro[indoline-3,2′-xanthene-4′,3″-indoline]-1,3′-dicarboxylate, C39H38N2O9
by: Li Wu-Wu, et al.
Published: (2021-09-01)

Crystal structure of methyl ((4-aminobenzyl)sulfonyl)-L-prolinate, C13H18N2O4S
by: Wang Zhen, et al.
Published: (2023-08-01)

Synthesis and crystal structure of 2,2,2-trichloroethyl N-{4-[6-(1-hydroxyethyl)-1,2,4,5-tetrazin-3-yl]benzyl}carbamate
by: J. Voss, et al.
Published: (2025-02-01)

Synthesis and crystal structure of (3E,5S,10S,13S,14S,17Z)-17-ethylidene-10,13-dimethylhexadecahydro-3H-cyclopenta[α] phenanthren-3-one O-(4-fluorobenzoyl) oxime, C28H36FNO2
by: Yue Lan, et al.
Published: (2023-10-01)

Synthesis and crystal structure of 3-methyl-2-(methylthio)-4H-chromen-4-one, C12H12O2S
by: Liu Feng, et al.
Published: (2023-08-01)

The crystal structure of 4-chloro-2-(quinolin-8-yl)isoindoline-1,3-dione, C17H9ClN2O2
by: Yang Fan, et al.
Published: (2021-09-01)

Synthesis of 2-(1-Benzofuran-2-yl)-4-(1,3-benzoxazol-2-yl/ 1,3-benzothiazol-2-yl) Quinolines as Blue Green Fluorescent Probes
by: Yadav D. Bodke, et al.
Published: (2013-01-01)

Synthesis and crystal structure of 1-((3R,10S,13S, 17S)-3-((2-methoxyphenyl)amino)-10,13-dimethylhexadecahydro-1H-cyclopenta[α]phenanthren-17-yl)ethan-1-one, C28H41NO2
by: Ye Jiang-Hai, et al.
Published: (2023-08-01)

Synthesis, Crystal Structure, and Spectra Properties of the Cadmium (II) Complex with Bis(N-allylbenzimidazol-2-ylmethyl)benzylamine
by: Huilu Wu, et al.
Published: (2011-01-01)

Crystal structure of (3R,3aS,6R,6aR)-6-hexyl-3-methyltetrahydrofuro[3,4-b]furan-2,4-dione, C13H20O4
by: Huang Yu-Xi, et al.
Published: (2023-08-01)

Synthesis, Crystal Structure, and DNA-Binding Studies of a Nickel(II) Complex with the Bis(2-benzimidazolymethyl)amine Ligand
by: Huilu Wu, et al.
Published: (2012-01-01)

Synthesis and crystal structure of 2-(2-oxo-2-(o-tolyl)ethyl)-4H-chromen-4-one, C18H14O3
by: Liu Yi, et al.
Published: (2023-08-01)

Crystal structure of 2-(thiazol-2-yl)hexahydro-1H-4,7-epoxyisoindole-1,3(2H)-dione, C11H10N2O3S
by: Wang Qinglong, et al.
Published: (2023-08-01)

Crystal structure of methyl 2-(1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)acetate, C15H11NO4
by: Peng Wei, et al.
Published: (2022-08-01)

Comparison of the photoactivities of two commercial titanium dioxide powders in the degradation of 1,4-dioxane
by: M. Mehrvar, et al.
Published: (2002-01-01)

The crystal structure of the co-crystal: 2-hydroxybenzoic acid – N′-(butan-2-ylidene)pyridine-4-carbohydrazide, C10H13N3O·C7H6O3
by: Setshedi Itumeleng B., et al.
Published: (2021-09-01)

The crystal structure of N-cyclopentyl-3-hydroxy-4-methoxybenzamide, C13H17NO3
by: Zhang Jingxiao, et al.
Published: (2022-08-01)

Hydrolysis Reactions of p-Nitrophenyl Trifluoroacetate and S-Ethyl Trifluorothioacetate
by: Jack B. Suggs, et al.
Published: (2025-01-01)

Crystal structure of N-(4′-chloro-[1,1′-biphenyl]-2-yl)formamide, C13H10ClNO
by: Du Mo, et al.
Published: (2023-10-01)