Development and multifunctional investigation of reduced graphene oxide decorated MgO hybrid nanocomposite

The current work reports magnesium oxide (MgO) nanoparticles were synthesized by solution combustion route and prepared MgO was incorporated on reduced graphene oxide (rGO) using simple reflux method. Here, XRD (X-ray Diffraction), XPS (X-ray photoelectron spectroscopy), SEM (Scanning electron micro...

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Main Authors: M. Mylarappa, S. Chandruvasan, K.N. Shravana Kumara, G. Krishnamurthy, A.S. Santhosh Kumar
Format: Article
Language:English
Published: Elsevier 2025-06-01
Series:Hybrid Advances
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Online Access:http://www.sciencedirect.com/science/article/pii/S2773207X25000211
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author M. Mylarappa
S. Chandruvasan
K.N. Shravana Kumara
G. Krishnamurthy
A.S. Santhosh Kumar
author_facet M. Mylarappa
S. Chandruvasan
K.N. Shravana Kumara
G. Krishnamurthy
A.S. Santhosh Kumar
author_sort M. Mylarappa
collection DOAJ
description The current work reports magnesium oxide (MgO) nanoparticles were synthesized by solution combustion route and prepared MgO was incorporated on reduced graphene oxide (rGO) using simple reflux method. Here, XRD (X-ray Diffraction), XPS (X-ray photoelectron spectroscopy), SEM (Scanning electron microscopy), EDAX (Energy dispersive X-ray analysis) and Raman spectra were employed to confirm the sample. The prepared rGO/MgO exhibited 83 % antioxidant activity with lower IC50 value 2609.23 mg/mL. The capacitance (Csp), diffusion coefficient (D) and sensing property were evaluated. From cyclic voltammetry analysis (CV), the capacitance values of rGO and rGO/MgO electrodes were found to be 91.26 and 173.05 F/g. The lesser value of reversibility (EO−ER=1.98×10−5) with greater proton diffusion coefficient (D=1.812×10−6) demonstrate enhanced electrochemical performance using 1 M KOH electrolyte. The selected malachite green dye was effectively degraded up to 93 % within 150 min by first-order kinetics. The prepared rGO/MgO electrode has been used for evaluating the sensing activity of ascorbic acid (BS-A), resorcinol (BS-R), and uric acid (BS–U). The findings obtained demonstrated a higher detecting oxidation potential.
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spelling doaj-art-f70a2435e6964a55b1d853a2be915b222025-02-10T04:35:33ZengElsevierHybrid Advances2773-207X2025-06-019100397Development and multifunctional investigation of reduced graphene oxide decorated MgO hybrid nanocompositeM. Mylarappa0S. Chandruvasan1K.N. Shravana Kumara2G. Krishnamurthy3A.S. Santhosh Kumar4Department of Studies in Chemistry, Bangalore University, Bengaluru-560056, Karnataka, India; Corresponding author.Department of Chemistry, KLE Society's S Nijalingappa College, Rajajinagar, Bengaluru, India-560009Department of Chemistry, Maharani Lakshmi Ammanni College for Women, Bengaluru, India, 560012Department of Studies in Chemistry, Bangalore University, Bengaluru-560056, Karnataka, IndiaDepartment of Studies in Chemistry, Bangalore University, Bengaluru-560056, Karnataka, IndiaThe current work reports magnesium oxide (MgO) nanoparticles were synthesized by solution combustion route and prepared MgO was incorporated on reduced graphene oxide (rGO) using simple reflux method. Here, XRD (X-ray Diffraction), XPS (X-ray photoelectron spectroscopy), SEM (Scanning electron microscopy), EDAX (Energy dispersive X-ray analysis) and Raman spectra were employed to confirm the sample. The prepared rGO/MgO exhibited 83 % antioxidant activity with lower IC50 value 2609.23 mg/mL. The capacitance (Csp), diffusion coefficient (D) and sensing property were evaluated. From cyclic voltammetry analysis (CV), the capacitance values of rGO and rGO/MgO electrodes were found to be 91.26 and 173.05 F/g. The lesser value of reversibility (EO−ER=1.98×10−5) with greater proton diffusion coefficient (D=1.812×10−6) demonstrate enhanced electrochemical performance using 1 M KOH electrolyte. The selected malachite green dye was effectively degraded up to 93 % within 150 min by first-order kinetics. The prepared rGO/MgO electrode has been used for evaluating the sensing activity of ascorbic acid (BS-A), resorcinol (BS-R), and uric acid (BS–U). The findings obtained demonstrated a higher detecting oxidation potential.http://www.sciencedirect.com/science/article/pii/S2773207X25000211rGO/MgOAntioxidantPhotodegradationElectrochemicalSensor
spellingShingle M. Mylarappa
S. Chandruvasan
K.N. Shravana Kumara
G. Krishnamurthy
A.S. Santhosh Kumar
Development and multifunctional investigation of reduced graphene oxide decorated MgO hybrid nanocomposite
Hybrid Advances
rGO/MgO
Antioxidant
Photodegradation
Electrochemical
Sensor
title Development and multifunctional investigation of reduced graphene oxide decorated MgO hybrid nanocomposite
title_full Development and multifunctional investigation of reduced graphene oxide decorated MgO hybrid nanocomposite
title_fullStr Development and multifunctional investigation of reduced graphene oxide decorated MgO hybrid nanocomposite
title_full_unstemmed Development and multifunctional investigation of reduced graphene oxide decorated MgO hybrid nanocomposite
title_short Development and multifunctional investigation of reduced graphene oxide decorated MgO hybrid nanocomposite
title_sort development and multifunctional investigation of reduced graphene oxide decorated mgo hybrid nanocomposite
topic rGO/MgO
Antioxidant
Photodegradation
Electrochemical
Sensor
url http://www.sciencedirect.com/science/article/pii/S2773207X25000211
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