Methylene Blue Dye Photodegradation during Synthesis and Characterization of WO3 Nanoparticles

Semiconductor-based photocatalytic systems have found widespread use in environmental pollution cleanup and renewable energy production. In this study, we synthesized WO3 as a catalyst for the degradation of methylene blue, a thiazine dye, which was used in the previous work. The hydrothermal proces...

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Main Authors: Raviteja Surakasi, null Alimuddin, Yenda Srinivasa Rao, Ashitha K. Sanuj, Pravin P. Patil, A. Jayaganthan, Ramana Hechhu
Format: Article
Language:English
Published: SAGE Publishing 2022-01-01
Series:Adsorption Science & Technology
Online Access:http://dx.doi.org/10.1155/2022/2882048
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author Raviteja Surakasi
null Alimuddin
Yenda Srinivasa Rao
Ashitha K. Sanuj
Pravin P. Patil
A. Jayaganthan
Ramana Hechhu
author_facet Raviteja Surakasi
null Alimuddin
Yenda Srinivasa Rao
Ashitha K. Sanuj
Pravin P. Patil
A. Jayaganthan
Ramana Hechhu
author_sort Raviteja Surakasi
collection DOAJ
description Semiconductor-based photocatalytic systems have found widespread use in environmental pollution cleanup and renewable energy production. In this study, we synthesized WO3 as a catalyst for the degradation of methylene blue, a thiazine dye, which was used in the previous work. The hydrothermal process is used to create WO3 nanoparticles, which are made from sodium tungstate. When it comes to confirming the nanoparticles, many characterization techniques are employed, including X-ray diffraction (XRD), Fourier transform infrared (FTIR), UV-Vis diffuse reflectance spectrometer (DRS), X-ray photoelectron spectroscopy (XPS), and field emission–scanning electron microscope (FE-SEM). The existence of monoclinic crystalline structure is shown by XRD, with the average crystalline size being around 34 nm. FTIR confirms the presence of metal oxides. The pellucid absorption extremity in the UV-Vis region corresponds to the rudimentary absorption of the WO3 semiconductor. FE-SEM confirms square-shaped nanoplates with EDX address the occurrence of elemental tungsten. The photocatalytic activity of WO3 nanoparticles against methylene blue is taken for at different intervals of time that confirms MB’s degradation. Our present work suggests that prepared nanoparticles should be potential for photocatalysts using various industrial dyes.
format Article
id doaj-art-f3ed9620bdb143eb912905a5c56f5a77
institution Kabale University
issn 2048-4038
language English
publishDate 2022-01-01
publisher SAGE Publishing
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series Adsorption Science & Technology
spelling doaj-art-f3ed9620bdb143eb912905a5c56f5a772025-01-03T01:25:16ZengSAGE PublishingAdsorption Science & Technology2048-40382022-01-01202210.1155/2022/2882048Methylene Blue Dye Photodegradation during Synthesis and Characterization of WO3 NanoparticlesRaviteja Surakasi0null Alimuddin1Yenda Srinivasa Rao2Ashitha K. Sanuj3Pravin P. Patil4A. Jayaganthan5Ramana Hechhu6Department of Mechanical EngineeringPhysical Sciences SectionDepartment of Mechanical EngineeringDepartment of MicrobiologyMechanical Engineering DepartmentDepartment of Automobile EngineeringDepartment of Pharmaceutical ChemistrySemiconductor-based photocatalytic systems have found widespread use in environmental pollution cleanup and renewable energy production. In this study, we synthesized WO3 as a catalyst for the degradation of methylene blue, a thiazine dye, which was used in the previous work. The hydrothermal process is used to create WO3 nanoparticles, which are made from sodium tungstate. When it comes to confirming the nanoparticles, many characterization techniques are employed, including X-ray diffraction (XRD), Fourier transform infrared (FTIR), UV-Vis diffuse reflectance spectrometer (DRS), X-ray photoelectron spectroscopy (XPS), and field emission–scanning electron microscope (FE-SEM). The existence of monoclinic crystalline structure is shown by XRD, with the average crystalline size being around 34 nm. FTIR confirms the presence of metal oxides. The pellucid absorption extremity in the UV-Vis region corresponds to the rudimentary absorption of the WO3 semiconductor. FE-SEM confirms square-shaped nanoplates with EDX address the occurrence of elemental tungsten. The photocatalytic activity of WO3 nanoparticles against methylene blue is taken for at different intervals of time that confirms MB’s degradation. Our present work suggests that prepared nanoparticles should be potential for photocatalysts using various industrial dyes.http://dx.doi.org/10.1155/2022/2882048
spellingShingle Raviteja Surakasi
null Alimuddin
Yenda Srinivasa Rao
Ashitha K. Sanuj
Pravin P. Patil
A. Jayaganthan
Ramana Hechhu
Methylene Blue Dye Photodegradation during Synthesis and Characterization of WO3 Nanoparticles
Adsorption Science & Technology
title Methylene Blue Dye Photodegradation during Synthesis and Characterization of WO3 Nanoparticles
title_full Methylene Blue Dye Photodegradation during Synthesis and Characterization of WO3 Nanoparticles
title_fullStr Methylene Blue Dye Photodegradation during Synthesis and Characterization of WO3 Nanoparticles
title_full_unstemmed Methylene Blue Dye Photodegradation during Synthesis and Characterization of WO3 Nanoparticles
title_short Methylene Blue Dye Photodegradation during Synthesis and Characterization of WO3 Nanoparticles
title_sort methylene blue dye photodegradation during synthesis and characterization of wo3 nanoparticles
url http://dx.doi.org/10.1155/2022/2882048
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AT yendasrinivasarao methylenebluedyephotodegradationduringsynthesisandcharacterizationofwo3nanoparticles
AT ashithaksanuj methylenebluedyephotodegradationduringsynthesisandcharacterizationofwo3nanoparticles
AT pravinppatil methylenebluedyephotodegradationduringsynthesisandcharacterizationofwo3nanoparticles
AT ajayaganthan methylenebluedyephotodegradationduringsynthesisandcharacterizationofwo3nanoparticles
AT ramanahechhu methylenebluedyephotodegradationduringsynthesisandcharacterizationofwo3nanoparticles