Bisphenol and Phthalate Migration Test from Mexican Meat Packaging Using HPLC-DAD Technique
The objective of this work was to analyze the bisphenols’ and phthalates’ (PAEs) migration from meat packages (of sausages, Winnies, and ham found in Mexican markets) to a water simulant. The determination of these compounds was realized by high performance liquid chromatography (HPLC) and diode arr...
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| Main Authors: | , , , , , |
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| Format: | Article |
| Language: | English |
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Wiley
2022-01-01
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| Series: | Journal of Chemistry |
| Online Access: | http://dx.doi.org/10.1155/2022/2688236 |
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| author | Valeria Ceballos-Luna David Chávez-Flores Ibiza Martínez-Serrano Beatriz A. Rocha-Gutierrez Myrna C. Nevárez-Rodríguez Blanca G. Beltrán |
| author_facet | Valeria Ceballos-Luna David Chávez-Flores Ibiza Martínez-Serrano Beatriz A. Rocha-Gutierrez Myrna C. Nevárez-Rodríguez Blanca G. Beltrán |
| author_sort | Valeria Ceballos-Luna |
| collection | DOAJ |
| description | The objective of this work was to analyze the bisphenols’ and phthalates’ (PAEs) migration from meat packages (of sausages, Winnies, and ham found in Mexican markets) to a water simulant. The determination of these compounds was realized by high performance liquid chromatography (HPLC) and diode array detection (DAD) at a wavelength of 254 nm. The mobile phase utilized was a mixture of acetonitrile:H2O (70 : 30). Elution was performed isocratically at a temperature of 25°C and at a flow rate of 1 mL min−1. The LOQs obtained for BPA, DEP, BADGE, DBP, BisDMA, DHP, DOP, and PA in µg mL−1 were 0.53, 2.09, 0.85, 1.45, 5.81, 1.03, 3.12, and 29.6, respectively. Calibration curves exhibited an adequate determination coefficient for all compounds (R2 >0.999). Excellent accuracy and precision in measurements (% RSD) were achieved. The recovery study showed good applicability of the method (percentage recovery 80% to 106%). The BPA, BADGE, DBP, and DOP concentrations found in samples exceeded the simulant migration limits (SMLs) established by the European Union. The contribution of the current investigation was to provide information related to the presence of bisphenols and PAEs in the package of meat products, highlighting the health risks associated with their exposure. |
| format | Article |
| id | doaj-art-f182ea9ca5fa43689783d03f20675056 |
| institution | Kabale University |
| issn | 2090-9071 |
| language | English |
| publishDate | 2022-01-01 |
| publisher | Wiley |
| record_format | Article |
| series | Journal of Chemistry |
| spelling | doaj-art-f182ea9ca5fa43689783d03f206750562025-02-03T01:07:11ZengWileyJournal of Chemistry2090-90712022-01-01202210.1155/2022/2688236Bisphenol and Phthalate Migration Test from Mexican Meat Packaging Using HPLC-DAD TechniqueValeria Ceballos-Luna0David Chávez-Flores1Ibiza Martínez-Serrano2Beatriz A. Rocha-Gutierrez3Myrna C. Nevárez-Rodríguez4Blanca G. Beltrán5Museum of ZoologyFaculty of Chemical SciencesMuseum of ZoologyFaculty of Chemical SciencesFaculty of Agrotechnological SciencesFaculty of Nursing and NutriologyThe objective of this work was to analyze the bisphenols’ and phthalates’ (PAEs) migration from meat packages (of sausages, Winnies, and ham found in Mexican markets) to a water simulant. The determination of these compounds was realized by high performance liquid chromatography (HPLC) and diode array detection (DAD) at a wavelength of 254 nm. The mobile phase utilized was a mixture of acetonitrile:H2O (70 : 30). Elution was performed isocratically at a temperature of 25°C and at a flow rate of 1 mL min−1. The LOQs obtained for BPA, DEP, BADGE, DBP, BisDMA, DHP, DOP, and PA in µg mL−1 were 0.53, 2.09, 0.85, 1.45, 5.81, 1.03, 3.12, and 29.6, respectively. Calibration curves exhibited an adequate determination coefficient for all compounds (R2 >0.999). Excellent accuracy and precision in measurements (% RSD) were achieved. The recovery study showed good applicability of the method (percentage recovery 80% to 106%). The BPA, BADGE, DBP, and DOP concentrations found in samples exceeded the simulant migration limits (SMLs) established by the European Union. The contribution of the current investigation was to provide information related to the presence of bisphenols and PAEs in the package of meat products, highlighting the health risks associated with their exposure.http://dx.doi.org/10.1155/2022/2688236 |
| spellingShingle | Valeria Ceballos-Luna David Chávez-Flores Ibiza Martínez-Serrano Beatriz A. Rocha-Gutierrez Myrna C. Nevárez-Rodríguez Blanca G. Beltrán Bisphenol and Phthalate Migration Test from Mexican Meat Packaging Using HPLC-DAD Technique Journal of Chemistry |
| title | Bisphenol and Phthalate Migration Test from Mexican Meat Packaging Using HPLC-DAD Technique |
| title_full | Bisphenol and Phthalate Migration Test from Mexican Meat Packaging Using HPLC-DAD Technique |
| title_fullStr | Bisphenol and Phthalate Migration Test from Mexican Meat Packaging Using HPLC-DAD Technique |
| title_full_unstemmed | Bisphenol and Phthalate Migration Test from Mexican Meat Packaging Using HPLC-DAD Technique |
| title_short | Bisphenol and Phthalate Migration Test from Mexican Meat Packaging Using HPLC-DAD Technique |
| title_sort | bisphenol and phthalate migration test from mexican meat packaging using hplc dad technique |
| url | http://dx.doi.org/10.1155/2022/2688236 |
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