Synthesis, Properties, and In Vitro Hydrolytic Degradation of Poly(d,l-lactide-co-glycolide-co-ε-caprolactone)

Random copolymers of poly(d,l-lactide-co-glycolide-co-ε-caprolactone) (PLGC) were synthesized by the ring-opening polymerization of d,l-lactide (DLLA), glycolide (GA), and ε-caprolactone (CL). The effects of CL on the copolymers were evaluated to prepare suitable copolymers with controlled propertie...

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Main Authors: Yixiu Liu, Xizhuang Bai, A. Liang
Format: Article
Language:English
Published: Wiley 2016-01-01
Series:International Journal of Polymer Science
Online Access:http://dx.doi.org/10.1155/2016/8082014
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author Yixiu Liu
Xizhuang Bai
A. Liang
author_facet Yixiu Liu
Xizhuang Bai
A. Liang
author_sort Yixiu Liu
collection DOAJ
description Random copolymers of poly(d,l-lactide-co-glycolide-co-ε-caprolactone) (PLGC) were synthesized by the ring-opening polymerization of d,l-lactide (DLLA), glycolide (GA), and ε-caprolactone (CL). The effects of CL on the copolymers were evaluated to prepare suitable copolymers with controlled properties. Our results showed that the CL content significantly influenced the thermal and mechanical properties of the copolymers and that the CL content in compositions could be altered to control properties of random copolymers. The in vitro hydrolytic degradation of the resulting implants showed that the degradation rate of PLGC was lower than that of PLGA, which could markedly reduce acidic degradation products. Finally, we demonstrated that higher CL contents in compositions slowed degradation rates.
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spelling doaj-art-ef68de48c8ea4d74a916d1fa0a77e8bc2025-08-20T02:22:24ZengWileyInternational Journal of Polymer Science1687-94221687-94302016-01-01201610.1155/2016/80820148082014Synthesis, Properties, and In Vitro Hydrolytic Degradation of Poly(d,l-lactide-co-glycolide-co-ε-caprolactone)Yixiu Liu0Xizhuang Bai1A. Liang2Department of Sports Medicine and Joint Surgery, The First Affiliated Hospital of China Medical University, Shenyang 110001, ChinaDepartment of Sports Medicine and Joint Surgery, The First Affiliated Hospital of China Medical University, Shenyang 110001, ChinaDepartment of Orthopaedics, The Central Hospital Affiliated to Shenyang Medical College, Shenyang 110024, ChinaRandom copolymers of poly(d,l-lactide-co-glycolide-co-ε-caprolactone) (PLGC) were synthesized by the ring-opening polymerization of d,l-lactide (DLLA), glycolide (GA), and ε-caprolactone (CL). The effects of CL on the copolymers were evaluated to prepare suitable copolymers with controlled properties. Our results showed that the CL content significantly influenced the thermal and mechanical properties of the copolymers and that the CL content in compositions could be altered to control properties of random copolymers. The in vitro hydrolytic degradation of the resulting implants showed that the degradation rate of PLGC was lower than that of PLGA, which could markedly reduce acidic degradation products. Finally, we demonstrated that higher CL contents in compositions slowed degradation rates.http://dx.doi.org/10.1155/2016/8082014
spellingShingle Yixiu Liu
Xizhuang Bai
A. Liang
Synthesis, Properties, and In Vitro Hydrolytic Degradation of Poly(d,l-lactide-co-glycolide-co-ε-caprolactone)
International Journal of Polymer Science
title Synthesis, Properties, and In Vitro Hydrolytic Degradation of Poly(d,l-lactide-co-glycolide-co-ε-caprolactone)
title_full Synthesis, Properties, and In Vitro Hydrolytic Degradation of Poly(d,l-lactide-co-glycolide-co-ε-caprolactone)
title_fullStr Synthesis, Properties, and In Vitro Hydrolytic Degradation of Poly(d,l-lactide-co-glycolide-co-ε-caprolactone)
title_full_unstemmed Synthesis, Properties, and In Vitro Hydrolytic Degradation of Poly(d,l-lactide-co-glycolide-co-ε-caprolactone)
title_short Synthesis, Properties, and In Vitro Hydrolytic Degradation of Poly(d,l-lactide-co-glycolide-co-ε-caprolactone)
title_sort synthesis properties and in vitro hydrolytic degradation of poly d l lactide co glycolide co ε caprolactone
url http://dx.doi.org/10.1155/2016/8082014
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AT xizhuangbai synthesispropertiesandinvitrohydrolyticdegradationofpolydllactidecoglycolidecoecaprolactone
AT aliang synthesispropertiesandinvitrohydrolyticdegradationofpolydllactidecoglycolidecoecaprolactone