Alumina Support for Cobalt Catalyst in a Methane Dry Reforming Reaction: The Role of Water Content in a Solvent Medium

This study aimed to synthesize alumina from an inorganic aluminum nitrate precursor in various binary solvent systems of ethanol and water using the sol-gel self-assembly (SSA) method, employing a triblock copolymer, pluronic P123, as the pore-directing agent. The resulting materials were implemente...

Full description

Saved in:
Bibliographic Details
Main Authors: My Hien Thi Bach, Ngoc Thang Tran, Thanh Nha Thi Tran, Van Cuong Nguyen, Hong Anh Thi Nguyen
Format: Article
Language:English
Published: Wiley 2021-01-01
Series:International Journal of Chemical Engineering
Online Access:http://dx.doi.org/10.1155/2021/6681796
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1850162970744586240
author My Hien Thi Bach
Ngoc Thang Tran
Thanh Nha Thi Tran
Van Cuong Nguyen
Hong Anh Thi Nguyen
author_facet My Hien Thi Bach
Ngoc Thang Tran
Thanh Nha Thi Tran
Van Cuong Nguyen
Hong Anh Thi Nguyen
author_sort My Hien Thi Bach
collection DOAJ
description This study aimed to synthesize alumina from an inorganic aluminum nitrate precursor in various binary solvent systems of ethanol and water using the sol-gel self-assembly (SSA) method, employing a triblock copolymer, pluronic P123, as the pore-directing agent. The resulting materials were implemented as a support for the cobalt (Co) catalyst in a methane dry reforming (MDR) reaction at 1073 K under 1 atm. Regardless of the water percentage used in the support synthesis, the methane dry reforming reaction over Co catalysts on alumina supports showed the negligible change in conversion during the 12 h reaction. Moreover, there was evidence of large quantities of amorphous carbon and graphitic carbon on the spent catalyst surface. However, the low oxidation temperature of these deposited carbons could help maintain the balance between the carbon formation and the carbon elimination processes on the catalyst surface during the reforming reaction, hence prolonging the lifetime of the catalyst. The high conversion of methane (CH4) from 64.6% to 82.8% and carbon dioxide (CO2) from 70.7% to 86.6% for the MDR reaction over the as-prepared alumina-supported Co catalyst demonstrated a significant improvement in catalyst production for the MDR reaction from the viewpoint of large-scale applications.
format Article
id doaj-art-eecbf9e4a8bb4982bc2cff6a977a7fc3
institution OA Journals
issn 1687-806X
1687-8078
language English
publishDate 2021-01-01
publisher Wiley
record_format Article
series International Journal of Chemical Engineering
spelling doaj-art-eecbf9e4a8bb4982bc2cff6a977a7fc32025-08-20T02:22:25ZengWileyInternational Journal of Chemical Engineering1687-806X1687-80782021-01-01202110.1155/2021/66817966681796Alumina Support for Cobalt Catalyst in a Methane Dry Reforming Reaction: The Role of Water Content in a Solvent MediumMy Hien Thi Bach0Ngoc Thang Tran1Thanh Nha Thi Tran2Van Cuong Nguyen3Hong Anh Thi Nguyen4Faculty of Chemical Engineering, Industrial University of Ho Chi Minh City, 12 Nguyen Van Bao St, Go Vap, Ho Chi Minh 70000, VietnamFaculty of Chemical Engineering, Industrial University of Ho Chi Minh City, 12 Nguyen Van Bao St, Go Vap, Ho Chi Minh 70000, VietnamFaculty of Chemical Engineering, Industrial University of Ho Chi Minh City, 12 Nguyen Van Bao St, Go Vap, Ho Chi Minh 70000, VietnamFaculty of Chemical Engineering, Industrial University of Ho Chi Minh City, 12 Nguyen Van Bao St, Go Vap, Ho Chi Minh 70000, VietnamFaculty of Chemical Engineering, Ho Chi Minh City University of Food Industry, 140 Le Trong Tan St, Ho Chi Minh 70000, VietnamThis study aimed to synthesize alumina from an inorganic aluminum nitrate precursor in various binary solvent systems of ethanol and water using the sol-gel self-assembly (SSA) method, employing a triblock copolymer, pluronic P123, as the pore-directing agent. The resulting materials were implemented as a support for the cobalt (Co) catalyst in a methane dry reforming (MDR) reaction at 1073 K under 1 atm. Regardless of the water percentage used in the support synthesis, the methane dry reforming reaction over Co catalysts on alumina supports showed the negligible change in conversion during the 12 h reaction. Moreover, there was evidence of large quantities of amorphous carbon and graphitic carbon on the spent catalyst surface. However, the low oxidation temperature of these deposited carbons could help maintain the balance between the carbon formation and the carbon elimination processes on the catalyst surface during the reforming reaction, hence prolonging the lifetime of the catalyst. The high conversion of methane (CH4) from 64.6% to 82.8% and carbon dioxide (CO2) from 70.7% to 86.6% for the MDR reaction over the as-prepared alumina-supported Co catalyst demonstrated a significant improvement in catalyst production for the MDR reaction from the viewpoint of large-scale applications.http://dx.doi.org/10.1155/2021/6681796
spellingShingle My Hien Thi Bach
Ngoc Thang Tran
Thanh Nha Thi Tran
Van Cuong Nguyen
Hong Anh Thi Nguyen
Alumina Support for Cobalt Catalyst in a Methane Dry Reforming Reaction: The Role of Water Content in a Solvent Medium
International Journal of Chemical Engineering
title Alumina Support for Cobalt Catalyst in a Methane Dry Reforming Reaction: The Role of Water Content in a Solvent Medium
title_full Alumina Support for Cobalt Catalyst in a Methane Dry Reforming Reaction: The Role of Water Content in a Solvent Medium
title_fullStr Alumina Support for Cobalt Catalyst in a Methane Dry Reforming Reaction: The Role of Water Content in a Solvent Medium
title_full_unstemmed Alumina Support for Cobalt Catalyst in a Methane Dry Reforming Reaction: The Role of Water Content in a Solvent Medium
title_short Alumina Support for Cobalt Catalyst in a Methane Dry Reforming Reaction: The Role of Water Content in a Solvent Medium
title_sort alumina support for cobalt catalyst in a methane dry reforming reaction the role of water content in a solvent medium
url http://dx.doi.org/10.1155/2021/6681796
work_keys_str_mv AT myhienthibach aluminasupportforcobaltcatalystinamethanedryreformingreactiontheroleofwatercontentinasolventmedium
AT ngocthangtran aluminasupportforcobaltcatalystinamethanedryreformingreactiontheroleofwatercontentinasolventmedium
AT thanhnhathitran aluminasupportforcobaltcatalystinamethanedryreformingreactiontheroleofwatercontentinasolventmedium
AT vancuongnguyen aluminasupportforcobaltcatalystinamethanedryreformingreactiontheroleofwatercontentinasolventmedium
AT honganhthinguyen aluminasupportforcobaltcatalystinamethanedryreformingreactiontheroleofwatercontentinasolventmedium