Synthesis of High-Thermal Stable Titanium Dioxide Nanoparticles
Nanosized crystals of anatase phase TiO2 with high-thermal stability was synthesized in the range of 15–17 nm via sol-gel method using titanium n-butoxide precursor. Synthesize was done at two different temperatures, that is, 200 and 300∘C and the final products were calcined at 400∘C. The final pro...
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| Format: | Article |
| Language: | English |
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Wiley
2008-01-01
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| Series: | International Journal of Photoenergy |
| Online Access: | http://dx.doi.org/10.1155/2008/245981 |
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| _version_ | 1832568043579899904 |
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| author | M. Rashidzadeh |
| author_facet | M. Rashidzadeh |
| author_sort | M. Rashidzadeh |
| collection | DOAJ |
| description | Nanosized crystals of anatase phase TiO2 with high-thermal stability was synthesized in the range of 15–17 nm via sol-gel method using titanium n-butoxide precursor. Synthesize was done at two different temperatures, that is, 200 and 300∘C and the final products were calcined at 400∘C. The final products were characterized by N2 adsorption, X-ray diffraction, FT-IR, and TEM and tested in a photoreactor using fluorescien as model molecule. For thermal stability investigation, the sample prepared at 300∘C was heated up to 800, 850, and 900∘C, the XRD results showed that the synthesized anatase phase was stable up to 850∘C. Photocatalytic activity of the prepared samples showed that the fluorescien degradation followed a pseudo-first-order kinetic. |
| format | Article |
| id | doaj-art-ee347c7922ce4385a751ed88a411b388 |
| institution | Kabale University |
| issn | 1110-662X 1687-529X |
| language | English |
| publishDate | 2008-01-01 |
| publisher | Wiley |
| record_format | Article |
| series | International Journal of Photoenergy |
| spelling | doaj-art-ee347c7922ce4385a751ed88a411b3882025-02-03T00:59:59ZengWileyInternational Journal of Photoenergy1110-662X1687-529X2008-01-01200810.1155/2008/245981245981Synthesis of High-Thermal Stable Titanium Dioxide NanoparticlesM. Rashidzadeh0Catalysis Research Center, Research Institute of Petroleum Industry, P.O. Box 14665-1998, Tehran 1485733111, IranNanosized crystals of anatase phase TiO2 with high-thermal stability was synthesized in the range of 15–17 nm via sol-gel method using titanium n-butoxide precursor. Synthesize was done at two different temperatures, that is, 200 and 300∘C and the final products were calcined at 400∘C. The final products were characterized by N2 adsorption, X-ray diffraction, FT-IR, and TEM and tested in a photoreactor using fluorescien as model molecule. For thermal stability investigation, the sample prepared at 300∘C was heated up to 800, 850, and 900∘C, the XRD results showed that the synthesized anatase phase was stable up to 850∘C. Photocatalytic activity of the prepared samples showed that the fluorescien degradation followed a pseudo-first-order kinetic.http://dx.doi.org/10.1155/2008/245981 |
| spellingShingle | M. Rashidzadeh Synthesis of High-Thermal Stable Titanium Dioxide Nanoparticles International Journal of Photoenergy |
| title | Synthesis of High-Thermal Stable Titanium Dioxide Nanoparticles |
| title_full | Synthesis of High-Thermal Stable Titanium Dioxide Nanoparticles |
| title_fullStr | Synthesis of High-Thermal Stable Titanium Dioxide Nanoparticles |
| title_full_unstemmed | Synthesis of High-Thermal Stable Titanium Dioxide Nanoparticles |
| title_short | Synthesis of High-Thermal Stable Titanium Dioxide Nanoparticles |
| title_sort | synthesis of high thermal stable titanium dioxide nanoparticles |
| url | http://dx.doi.org/10.1155/2008/245981 |
| work_keys_str_mv | AT mrashidzadeh synthesisofhighthermalstabletitaniumdioxidenanoparticles |