RECOVERY OF FIBRINOLYTIC AND COLLAGENOLYTIC ENZYMES FROM FISH AND SHRIMP BYPRODUCTS: POTENTIAL SOURCE FOR BIOMEDICAL APPLICATIONS

Fish and shrimp industries generate a significant amount of by-products. These by-products can be used for the extraction of enzymes of biomedical interest, such as fibrinolytic and collagenolytic. Thus, this work aimed to perform a screening of fish and shrimp byproducts as sources of enzymes with...

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Main Authors: Vagne de Melo Oliveira, Caio Rodrigo Dias Assis, Jéssica Costa Silva, Quesia Jemima Silva, Ranilson de Souza Bezerra, Ana Lúcia Figueiredo Porto
Format: Article
Language:English
Published: Instituto de Pesca 2019-02-01
Series:Boletim do Instituto de Pesca
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Online Access:https://institutodepesca.org/index.php/bip/article/view/1340
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author Vagne de Melo Oliveira
Caio Rodrigo Dias Assis
Jéssica Costa Silva
Quesia Jemima Silva
Ranilson de Souza Bezerra
Ana Lúcia Figueiredo Porto
author_facet Vagne de Melo Oliveira
Caio Rodrigo Dias Assis
Jéssica Costa Silva
Quesia Jemima Silva
Ranilson de Souza Bezerra
Ana Lúcia Figueiredo Porto
author_sort Vagne de Melo Oliveira
collection DOAJ
description Fish and shrimp industries generate a significant amount of by-products. These by-products can be used for the extraction of enzymes of biomedical interest, such as fibrinolytic and collagenolytic. Thus, this work aimed to perform a screening of fish and shrimp byproducts as sources of enzymes with fibrinolytic and collagenolytic activities and to characterize the biochemical properties of crude extracts with collagenolytic activity from Cichla ocellaris residues. Fibrinolytic enzymes were recovered with activities between 5.51 ± 0.02 U.mL-1 (Caranx crysos) and 56.16 ± 0.42 U.mL-1 (Litopenaeus vannamei), while collagenolytic enzymes were detected in a range between 6.79 ± 0.00 U.mg-1 (Trachurus lathami) and 94.35 ± 0.02 U.mg-1 (C. ocellaris). After collagenolytic screening, the selected species was C. ocellaris, being subjected to a preheating, which culminated with an increase of enzymatic activity of 35.07% (up to 127.44 ± 0.09 U.mg-1). The optimal collagenolytic activity recovered from C. ocellaris byproducts was 55 °C (thermostable between 25 and 60 °C) and 7.5 (stable between 6.5 and 11.5) for temperature and pH evaluations, respectively. The kinetic parameters were determined, obtaining Km of 5.92 mM and Vmax of 294.40 U.mg-1. The recovered enzyme was sensitive to the Cu2+, Hg2 and Pb2+ ions, being partially inhibited by phenylmethylsulphonyl fluoride (PMSF), N-p-tosyl-L-lysin chloromethyl ketone (TLCK) and Benzamidine. Furthermore, it was able to cleave native type I collagen, the most important type for industry. Thus, the recovery of biomolecules, besides offering to the industry an alternative source of active molecules, contributes to the reduction of the environmental impact, adding value to the fish product and providing a new source of income.
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spelling doaj-art-edbeac7c34104f92b9a6b09fdc07aa562025-08-20T02:04:33ZengInstituto de PescaBoletim do Instituto de Pesca1678-23052019-02-0145110.20950/1678-2305.2019.45.1.389RECOVERY OF FIBRINOLYTIC AND COLLAGENOLYTIC ENZYMES FROM FISH AND SHRIMP BYPRODUCTS: POTENTIAL SOURCE FOR BIOMEDICAL APPLICATIONSVagne de Melo Oliveira0Caio Rodrigo Dias Assis1Jéssica Costa Silva2Quesia Jemima Silva3Ranilson de Souza Bezerra4Ana Lúcia Figueiredo Porto5Universidade Federal Rural de Pernambuco -  UFRPE, Laboratório de Tecnologia de Produtos Bioativos -  LABTECBIO, Departamento de Morfologia e Fisiologia Animal -  DMFA / Universidade Federal de Pernambuco -  UFPE, Laboratório de Enzimologia -  LABENZ, Departamento de Bioquí­­micaUniversidade Federal de Pernambuco -  UFPE, Laboratório de Enzimologia -  LABENZ, Departamento de Bioquí­­micaUniversidade Federal Rural de Pernambuco -  UFRPE, Laboratório de Tecnologia de Produtos Bioativos -  LABTECBIO, Departamento de Morfologia e Fisiologia Animal -  DMFAUniversidade Federal Rural de Pernambuco -  UFRPE, Laboratório de Tecnologia de Produtos Bioativos -  LABTECBIO, Departamento de Morfologia e Fisiologia Animal -  DMFAUniversidade Federal de Pernambuco -  UFPE, Laboratório de Enzimologia -  LABENZ, Departamento de Bioquí­­micaUniversidade Federal Rural de Pernambuco -  UFRPE, Laboratório de Tecnologia de Produtos Bioativos -  LABTECBIO, Departamento de Morfologia e Fisiologia Animal -  DMFA Fish and shrimp industries generate a significant amount of by-products. These by-products can be used for the extraction of enzymes of biomedical interest, such as fibrinolytic and collagenolytic. Thus, this work aimed to perform a screening of fish and shrimp byproducts as sources of enzymes with fibrinolytic and collagenolytic activities and to characterize the biochemical properties of crude extracts with collagenolytic activity from Cichla ocellaris residues. Fibrinolytic enzymes were recovered with activities between 5.51 ± 0.02 U.mL-1 (Caranx crysos) and 56.16 ± 0.42 U.mL-1 (Litopenaeus vannamei), while collagenolytic enzymes were detected in a range between 6.79 ± 0.00 U.mg-1 (Trachurus lathami) and 94.35 ± 0.02 U.mg-1 (C. ocellaris). After collagenolytic screening, the selected species was C. ocellaris, being subjected to a preheating, which culminated with an increase of enzymatic activity of 35.07% (up to 127.44 ± 0.09 U.mg-1). The optimal collagenolytic activity recovered from C. ocellaris byproducts was 55 °C (thermostable between 25 and 60 °C) and 7.5 (stable between 6.5 and 11.5) for temperature and pH evaluations, respectively. The kinetic parameters were determined, obtaining Km of 5.92 mM and Vmax of 294.40 U.mg-1. The recovered enzyme was sensitive to the Cu2+, Hg2 and Pb2+ ions, being partially inhibited by phenylmethylsulphonyl fluoride (PMSF), N-p-tosyl-L-lysin chloromethyl ketone (TLCK) and Benzamidine. Furthermore, it was able to cleave native type I collagen, the most important type for industry. Thus, the recovery of biomolecules, besides offering to the industry an alternative source of active molecules, contributes to the reduction of the environmental impact, adding value to the fish product and providing a new source of income. https://institutodepesca.org/index.php/bip/article/view/1340byproductscollagenasethrombolytic
spellingShingle Vagne de Melo Oliveira
Caio Rodrigo Dias Assis
Jéssica Costa Silva
Quesia Jemima Silva
Ranilson de Souza Bezerra
Ana Lúcia Figueiredo Porto
RECOVERY OF FIBRINOLYTIC AND COLLAGENOLYTIC ENZYMES FROM FISH AND SHRIMP BYPRODUCTS: POTENTIAL SOURCE FOR BIOMEDICAL APPLICATIONS
Boletim do Instituto de Pesca
byproducts
collagenase
thrombolytic
title RECOVERY OF FIBRINOLYTIC AND COLLAGENOLYTIC ENZYMES FROM FISH AND SHRIMP BYPRODUCTS: POTENTIAL SOURCE FOR BIOMEDICAL APPLICATIONS
title_full RECOVERY OF FIBRINOLYTIC AND COLLAGENOLYTIC ENZYMES FROM FISH AND SHRIMP BYPRODUCTS: POTENTIAL SOURCE FOR BIOMEDICAL APPLICATIONS
title_fullStr RECOVERY OF FIBRINOLYTIC AND COLLAGENOLYTIC ENZYMES FROM FISH AND SHRIMP BYPRODUCTS: POTENTIAL SOURCE FOR BIOMEDICAL APPLICATIONS
title_full_unstemmed RECOVERY OF FIBRINOLYTIC AND COLLAGENOLYTIC ENZYMES FROM FISH AND SHRIMP BYPRODUCTS: POTENTIAL SOURCE FOR BIOMEDICAL APPLICATIONS
title_short RECOVERY OF FIBRINOLYTIC AND COLLAGENOLYTIC ENZYMES FROM FISH AND SHRIMP BYPRODUCTS: POTENTIAL SOURCE FOR BIOMEDICAL APPLICATIONS
title_sort recovery of fibrinolytic and collagenolytic enzymes from fish and shrimp byproducts potential source for biomedical applications
topic byproducts
collagenase
thrombolytic
url https://institutodepesca.org/index.php/bip/article/view/1340
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