Single‐Atom Sites With Axial Ligand‐Induced d Orbital Rearrangement as Efficient Electrocatalysts for Lithium–Oxygen Batteries

ABSTRACT Understanding and regulating the electronic states of single‐atom sites near the Fermi energy level are essential for developing effective electrocatalysts for lithium–oxygen batteries (LOBs). In this study, we introduce an axial oxygen ligand at the metal center of cobalt porphyrin (CoPP)...

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Main Authors: Pengfei Liu, Chuan Wang, Chenrui Zeng, Shuhan Wang, Xudong Yu, Haoruo Xiao, Yan Huang, Yang Zhang, Ying Zeng, Chaozhu Shu, Zhenxing Liang
Format: Article
Language:English
Published: Wiley 2025-06-01
Series:SusMat
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Online Access:https://doi.org/10.1002/sus2.70007
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author Pengfei Liu
Chuan Wang
Chenrui Zeng
Shuhan Wang
Xudong Yu
Haoruo Xiao
Yan Huang
Yang Zhang
Ying Zeng
Chaozhu Shu
Zhenxing Liang
author_facet Pengfei Liu
Chuan Wang
Chenrui Zeng
Shuhan Wang
Xudong Yu
Haoruo Xiao
Yan Huang
Yang Zhang
Ying Zeng
Chaozhu Shu
Zhenxing Liang
author_sort Pengfei Liu
collection DOAJ
description ABSTRACT Understanding and regulating the electronic states of single‐atom sites near the Fermi energy level are essential for developing effective electrocatalysts for lithium–oxygen batteries (LOBs). In this study, we introduce an axial oxygen ligand at the metal center of cobalt porphyrin (CoPP) to adjust the electronic state of the Co center. Theoretical calculations and experimental findings show that this axial interaction disrupts the planar tetragonal crystal field of CoPP, resulting in enhanced spin polarization and electronic rearrangement. This rearrangement of d orbitals causes an upward shift in the frontier orbitals, which facilitates electron exchange during reactions. Additionally, the increased number of unpaired electrons in the d orbitals enhances the adsorption of CoPP‐O‐MXene to various oxygen species, promoting the formation of a thin film‐like Li2O2. These thin film‐like discharge products improve contact with the electrode surfaces, leading to easier decomposition during the charging process. Consequently, CoPP‐O‐MXene‐based LOBs demonstrate a high discharge capacity of 11035 mAh g−¹, a low overpotential of 0.76 V, and remarkable cycling stability (445 cycles).
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issn 2692-4552
language English
publishDate 2025-06-01
publisher Wiley
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spelling doaj-art-ec79be33aeb44aa49b6f2ac2d9aea5812025-08-20T02:36:27ZengWileySusMat2692-45522025-06-0153n/an/a10.1002/sus2.70007Single‐Atom Sites With Axial Ligand‐Induced d Orbital Rearrangement as Efficient Electrocatalysts for Lithium–Oxygen BatteriesPengfei Liu0Chuan Wang1Chenrui Zeng2Shuhan Wang3Xudong Yu4Haoruo Xiao5Yan Huang6Yang Zhang7Ying Zeng8Chaozhu Shu9Zhenxing Liang10College of Materials and Chemistry & Chemical Engineering Chengdu University of Technology Chengdu Sichuan ChinaCollege of Materials and Chemistry & Chemical Engineering Chengdu University of Technology Chengdu Sichuan ChinaCollege of Materials and Chemistry & Chemical Engineering Chengdu University of Technology Chengdu Sichuan ChinaCollege of Materials and Chemistry & Chemical Engineering Chengdu University of Technology Chengdu Sichuan ChinaCollege of Materials and Chemistry & Chemical Engineering Chengdu University of Technology Chengdu Sichuan ChinaCollege of Materials and Chemistry & Chemical Engineering Chengdu University of Technology Chengdu Sichuan ChinaCollege of Materials and Chemistry & Chemical Engineering Chengdu University of Technology Chengdu Sichuan ChinaCollege of Materials and Chemistry & Chemical Engineering Chengdu University of Technology Chengdu Sichuan ChinaCollege of Materials and Chemistry & Chemical Engineering Chengdu University of Technology Chengdu Sichuan ChinaCollege of Materials and Chemistry & Chemical Engineering Chengdu University of Technology Chengdu Sichuan ChinaGuangdong Provincial Key Laboratory of Fuel Cell Technology, School of Chemistry and Chemical Engineering South China University of Technology Guangzhou ChinaABSTRACT Understanding and regulating the electronic states of single‐atom sites near the Fermi energy level are essential for developing effective electrocatalysts for lithium–oxygen batteries (LOBs). In this study, we introduce an axial oxygen ligand at the metal center of cobalt porphyrin (CoPP) to adjust the electronic state of the Co center. Theoretical calculations and experimental findings show that this axial interaction disrupts the planar tetragonal crystal field of CoPP, resulting in enhanced spin polarization and electronic rearrangement. This rearrangement of d orbitals causes an upward shift in the frontier orbitals, which facilitates electron exchange during reactions. Additionally, the increased number of unpaired electrons in the d orbitals enhances the adsorption of CoPP‐O‐MXene to various oxygen species, promoting the formation of a thin film‐like Li2O2. These thin film‐like discharge products improve contact with the electrode surfaces, leading to easier decomposition during the charging process. Consequently, CoPP‐O‐MXene‐based LOBs demonstrate a high discharge capacity of 11035 mAh g−¹, a low overpotential of 0.76 V, and remarkable cycling stability (445 cycles).https://doi.org/10.1002/sus2.70007axial ligandselectrocatalystlithium–oxygen batteryoxygen electrode reactionsingle‐atom sites
spellingShingle Pengfei Liu
Chuan Wang
Chenrui Zeng
Shuhan Wang
Xudong Yu
Haoruo Xiao
Yan Huang
Yang Zhang
Ying Zeng
Chaozhu Shu
Zhenxing Liang
Single‐Atom Sites With Axial Ligand‐Induced d Orbital Rearrangement as Efficient Electrocatalysts for Lithium–Oxygen Batteries
SusMat
axial ligands
electrocatalyst
lithium–oxygen battery
oxygen electrode reaction
single‐atom sites
title Single‐Atom Sites With Axial Ligand‐Induced d Orbital Rearrangement as Efficient Electrocatalysts for Lithium–Oxygen Batteries
title_full Single‐Atom Sites With Axial Ligand‐Induced d Orbital Rearrangement as Efficient Electrocatalysts for Lithium–Oxygen Batteries
title_fullStr Single‐Atom Sites With Axial Ligand‐Induced d Orbital Rearrangement as Efficient Electrocatalysts for Lithium–Oxygen Batteries
title_full_unstemmed Single‐Atom Sites With Axial Ligand‐Induced d Orbital Rearrangement as Efficient Electrocatalysts for Lithium–Oxygen Batteries
title_short Single‐Atom Sites With Axial Ligand‐Induced d Orbital Rearrangement as Efficient Electrocatalysts for Lithium–Oxygen Batteries
title_sort single atom sites with axial ligand induced d orbital rearrangement as efficient electrocatalysts for lithium oxygen batteries
topic axial ligands
electrocatalyst
lithium–oxygen battery
oxygen electrode reaction
single‐atom sites
url https://doi.org/10.1002/sus2.70007
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