Validation and measurement uncertainty estimation in food microbiology: differences between quantitative and qualitative methods

The aim of this research is to describe quality control procedures, procedures for validation and measurement uncertainty (MU) determination as an important element of quality assurance in food microbiology laboratory for qualitative and quantitative type of analysis. Accreditation is conducted acco...

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Main Authors: Vesna Režić Dereani, Marijana Matek Sarić
Format: Article
Language:English
Published: Croatian Dairy Union 2010-09-01
Series:Mljekarstvo
Subjects:
Online Access:http://hrcak.srce.hr/index.php?show=clanak&id_clanak_jezik=89064
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author Vesna Režić Dereani
Marijana Matek Sarić
author_facet Vesna Režić Dereani
Marijana Matek Sarić
author_sort Vesna Režić Dereani
collection DOAJ
description The aim of this research is to describe quality control procedures, procedures for validation and measurement uncertainty (MU) determination as an important element of quality assurance in food microbiology laboratory for qualitative and quantitative type of analysis. Accreditation is conducted according to the standard ISO 17025:2007. General requirements for the competence of testing and calibration laboratories, which guarantees the compliance with standard operating procedures and the technical competence of the staff involved in the tests, recently are widely introduced in food microbiology laboratories in Croatia. In addition to quality manual introduction, and a lot of general documents, some of the most demanding procedures in routine microbiology laboratories are measurement uncertainty (MU) procedures and validation experiment design establishment. Those procedures are not standardized yet even at international level, and they require practical microbiological knowledge, altogether with statistical competence. Differences between validation experiments design for quantitative and qualitative food microbiology analysis are discussed in this research, and practical solutions are shortly described. MU for quantitative determinations is more demanding issue than qualitative MU calculation. MU calculations are based on external proficiency testing data and internal validation data. In this paper, practical schematic descriptions for both procedures are shown.
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issn 0026-704X
1846-4025
language English
publishDate 2010-09-01
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series Mljekarstvo
spelling doaj-art-ebaf62d14d484a8daf9dc0e62d7891562025-08-20T02:22:20ZengCroatian Dairy UnionMljekarstvo0026-704X1846-40252010-09-01603207213Validation and measurement uncertainty estimation in food microbiology: differences between quantitative and qualitative methodsVesna Režić DereaniMarijana Matek SarićThe aim of this research is to describe quality control procedures, procedures for validation and measurement uncertainty (MU) determination as an important element of quality assurance in food microbiology laboratory for qualitative and quantitative type of analysis. Accreditation is conducted according to the standard ISO 17025:2007. General requirements for the competence of testing and calibration laboratories, which guarantees the compliance with standard operating procedures and the technical competence of the staff involved in the tests, recently are widely introduced in food microbiology laboratories in Croatia. In addition to quality manual introduction, and a lot of general documents, some of the most demanding procedures in routine microbiology laboratories are measurement uncertainty (MU) procedures and validation experiment design establishment. Those procedures are not standardized yet even at international level, and they require practical microbiological knowledge, altogether with statistical competence. Differences between validation experiments design for quantitative and qualitative food microbiology analysis are discussed in this research, and practical solutions are shortly described. MU for quantitative determinations is more demanding issue than qualitative MU calculation. MU calculations are based on external proficiency testing data and internal validation data. In this paper, practical schematic descriptions for both procedures are shown.http://hrcak.srce.hr/index.php?show=clanak&id_clanak_jezik=89064measurement uncertaintyvalidationfood microbiology laboratoryqualitative and quantitative measurement
spellingShingle Vesna Režić Dereani
Marijana Matek Sarić
Validation and measurement uncertainty estimation in food microbiology: differences between quantitative and qualitative methods
Mljekarstvo
measurement uncertainty
validation
food microbiology laboratory
qualitative and quantitative measurement
title Validation and measurement uncertainty estimation in food microbiology: differences between quantitative and qualitative methods
title_full Validation and measurement uncertainty estimation in food microbiology: differences between quantitative and qualitative methods
title_fullStr Validation and measurement uncertainty estimation in food microbiology: differences between quantitative and qualitative methods
title_full_unstemmed Validation and measurement uncertainty estimation in food microbiology: differences between quantitative and qualitative methods
title_short Validation and measurement uncertainty estimation in food microbiology: differences between quantitative and qualitative methods
title_sort validation and measurement uncertainty estimation in food microbiology differences between quantitative and qualitative methods
topic measurement uncertainty
validation
food microbiology laboratory
qualitative and quantitative measurement
url http://hrcak.srce.hr/index.php?show=clanak&id_clanak_jezik=89064
work_keys_str_mv AT vesnarezicdereani validationandmeasurementuncertaintyestimationinfoodmicrobiologydifferencesbetweenquantitativeandqualitativemethods
AT marijanamateksaric validationandmeasurementuncertaintyestimationinfoodmicrobiologydifferencesbetweenquantitativeandqualitativemethods