Highly Efficient Photocatalysis by Zinc Oxide-Reduced Graphene Oxide (ZnO-rGO) Composite Synthesized via One-Pot Room-Temperature Chemical Deposition Method

We synthesized zinc oxide-reduced graphene oxide (ZnO-rGO) composites using a one-pot chemical deposition method at room temperature. Zinc powder and graphene oxide (GO) of different mass ratios (1 : 1, 1 : 2, 1 : 5, 1 : 10, and 1 : 20 GO to Zn) were used as precursors in a mildly alkaline solution....

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Main Authors: Roselle T. Ngaloy, Aixeen M. Fontanilla, Ma. S. Rebecca Soriano, Chelo S. Pascua, Yoshitaka Matsushita, Ian Jasper A. Agulo
Format: Article
Language:English
Published: Wiley 2019-01-01
Series:Journal of Nanotechnology
Online Access:http://dx.doi.org/10.1155/2019/1895043
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author Roselle T. Ngaloy
Aixeen M. Fontanilla
Ma. S. Rebecca Soriano
Chelo S. Pascua
Yoshitaka Matsushita
Ian Jasper A. Agulo
author_facet Roselle T. Ngaloy
Aixeen M. Fontanilla
Ma. S. Rebecca Soriano
Chelo S. Pascua
Yoshitaka Matsushita
Ian Jasper A. Agulo
author_sort Roselle T. Ngaloy
collection DOAJ
description We synthesized zinc oxide-reduced graphene oxide (ZnO-rGO) composites using a one-pot chemical deposition method at room temperature. Zinc powder and graphene oxide (GO) of different mass ratios (1 : 1, 1 : 2, 1 : 5, 1 : 10, and 1 : 20 GO to Zn) were used as precursors in a mildly alkaline solution. UV-Vis spectroscopy was used to study the photocatalytic efficiency of the samples through the photodegradation of methylene blue (MB). UV-Vis measurements show the fast decomposition of methylene blue under UV light illumination with the best degradation efficiency of 97.7% within one hour, achieved with sample ZG2 (1 GO : 2 Zn mass ratio). The corresponding degradation rate was kZG2 = 0.1253 min−1, which is at least 5.5 times better than other existing works using hydrothermal methods. We argue that the excellent photodegradation of MB by ZG2 is due to the efficient charge separation brought about by the electronic interaction of the rGO with the ZnO and the formation of a Zn-O-C bond, as supported by XRD and Raman spectroscopy measurements.
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spelling doaj-art-eb71bb8ed1fa411691ba3cf29716fd1f2025-08-20T02:22:21ZengWileyJournal of Nanotechnology1687-95031687-95112019-01-01201910.1155/2019/18950431895043Highly Efficient Photocatalysis by Zinc Oxide-Reduced Graphene Oxide (ZnO-rGO) Composite Synthesized via One-Pot Room-Temperature Chemical Deposition MethodRoselle T. Ngaloy0Aixeen M. Fontanilla1Ma. S. Rebecca Soriano2Chelo S. Pascua3Yoshitaka Matsushita4Ian Jasper A. Agulo5Micro and Nano Innovations Laboratory, Department of Physical Sciences, College of Science, University of the Philippines Baguio, Baguio 2600, PhilippinesMicro and Nano Innovations Laboratory, Department of Physical Sciences, College of Science, University of the Philippines Baguio, Baguio 2600, PhilippinesMicro and Nano Innovations Laboratory, Department of Physical Sciences, College of Science, University of the Philippines Baguio, Baguio 2600, PhilippinesMicro and Nano Innovations Laboratory, Department of Physical Sciences, College of Science, University of the Philippines Baguio, Baguio 2600, PhilippinesMaterials Analysis Station, National Institute for Materials Science, Sengen, Tsukuba, Ibaraki 305-0047, JapanMicro and Nano Innovations Laboratory, Department of Physical Sciences, College of Science, University of the Philippines Baguio, Baguio 2600, PhilippinesWe synthesized zinc oxide-reduced graphene oxide (ZnO-rGO) composites using a one-pot chemical deposition method at room temperature. Zinc powder and graphene oxide (GO) of different mass ratios (1 : 1, 1 : 2, 1 : 5, 1 : 10, and 1 : 20 GO to Zn) were used as precursors in a mildly alkaline solution. UV-Vis spectroscopy was used to study the photocatalytic efficiency of the samples through the photodegradation of methylene blue (MB). UV-Vis measurements show the fast decomposition of methylene blue under UV light illumination with the best degradation efficiency of 97.7% within one hour, achieved with sample ZG2 (1 GO : 2 Zn mass ratio). The corresponding degradation rate was kZG2 = 0.1253 min−1, which is at least 5.5 times better than other existing works using hydrothermal methods. We argue that the excellent photodegradation of MB by ZG2 is due to the efficient charge separation brought about by the electronic interaction of the rGO with the ZnO and the formation of a Zn-O-C bond, as supported by XRD and Raman spectroscopy measurements.http://dx.doi.org/10.1155/2019/1895043
spellingShingle Roselle T. Ngaloy
Aixeen M. Fontanilla
Ma. S. Rebecca Soriano
Chelo S. Pascua
Yoshitaka Matsushita
Ian Jasper A. Agulo
Highly Efficient Photocatalysis by Zinc Oxide-Reduced Graphene Oxide (ZnO-rGO) Composite Synthesized via One-Pot Room-Temperature Chemical Deposition Method
Journal of Nanotechnology
title Highly Efficient Photocatalysis by Zinc Oxide-Reduced Graphene Oxide (ZnO-rGO) Composite Synthesized via One-Pot Room-Temperature Chemical Deposition Method
title_full Highly Efficient Photocatalysis by Zinc Oxide-Reduced Graphene Oxide (ZnO-rGO) Composite Synthesized via One-Pot Room-Temperature Chemical Deposition Method
title_fullStr Highly Efficient Photocatalysis by Zinc Oxide-Reduced Graphene Oxide (ZnO-rGO) Composite Synthesized via One-Pot Room-Temperature Chemical Deposition Method
title_full_unstemmed Highly Efficient Photocatalysis by Zinc Oxide-Reduced Graphene Oxide (ZnO-rGO) Composite Synthesized via One-Pot Room-Temperature Chemical Deposition Method
title_short Highly Efficient Photocatalysis by Zinc Oxide-Reduced Graphene Oxide (ZnO-rGO) Composite Synthesized via One-Pot Room-Temperature Chemical Deposition Method
title_sort highly efficient photocatalysis by zinc oxide reduced graphene oxide zno rgo composite synthesized via one pot room temperature chemical deposition method
url http://dx.doi.org/10.1155/2019/1895043
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