Measurement of 4-(2-thiazole azo) rososinol acidy constants by means of ultraviolet spectroscopy and chemometrics in water-acetonitrile and water-dioxane binary mixtures

In this paper, by combining ultraviolet spectroscopy and Chemometrics method, the acid dissociation constant of 4- (2-thiazole azo) rososinol was measured. The absorption spectra of the 4- (2-thiazole azo) rososinol solution have a large spectral overlap, so it will be difficult to determine its aci...

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Main Authors: Mansoor Namazian, Shahriar Jahanbani, Ali Benvidi
Format: Article
Language:English
Published: Semnan University 2024-06-01
Series:شیمی کاربردی روز
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Online Access:https://chemistry.semnan.ac.ir/article_8829_dd74c5bffad96ec7e96cffa4edf757a6.pdf
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author Mansoor Namazian
Shahriar Jahanbani
Ali Benvidi
author_facet Mansoor Namazian
Shahriar Jahanbani
Ali Benvidi
author_sort Mansoor Namazian
collection DOAJ
description In this paper, by combining ultraviolet spectroscopy and Chemometrics method, the acid dissociation constant of 4- (2-thiazole azo) rososinol was measured. The absorption spectra of the 4- (2-thiazole azo) rososinol solution have a large spectral overlap, so it will be difficult to determine its acid dissociation constant using conventional spectroscopy. Using ultraviolet-visible spectroscopy and two rank annihilation factor analysis (TRAFA), acid constants, number of species, molar fraction, relative standard deviation (RSD) and net species spectrum acid dissociation of 4- (2-thiazole azo) rososinol in 20 to 80% v/v of acetonitrile in water and dioxane in water was calculated. The results obtained by the two rank annihilation factor analysis method show the efficiency of this method in determining the solution with high spectral overlap. As the percentage of solvents increases, the acid constant becomes smaller, which can be explained by the fact that the solubility and dielectric constant of water, acetonitrile and dioxane are different. The value of these variables depends on the physical parameters (dielectric constant and induction number).
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publishDate 2024-06-01
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series شیمی کاربردی روز
spelling doaj-art-eaed65b6f279461eb27b42e187e1d2eb2025-08-20T02:30:37ZengSemnan Universityشیمی کاربردی روز2981-24372024-06-01197115116610.22075/chem.2024.25783.20398829Measurement of 4-(2-thiazole azo) rososinol acidy constants by means of ultraviolet spectroscopy and chemometrics in water-acetonitrile and water-dioxane binary mixturesMansoor Namazian0Shahriar Jahanbani1Ali Benvidi2Faculty of Chemistry, Yazd University, Yazd, IranFaculty of Chemistry, Yazd University, Yazd, IranFaculty of Chemistry, Yazd University, Yazd, IranIn this paper, by combining ultraviolet spectroscopy and Chemometrics method, the acid dissociation constant of 4- (2-thiazole azo) rososinol was measured. The absorption spectra of the 4- (2-thiazole azo) rososinol solution have a large spectral overlap, so it will be difficult to determine its acid dissociation constant using conventional spectroscopy. Using ultraviolet-visible spectroscopy and two rank annihilation factor analysis (TRAFA), acid constants, number of species, molar fraction, relative standard deviation (RSD) and net species spectrum acid dissociation of 4- (2-thiazole azo) rososinol in 20 to 80% v/v of acetonitrile in water and dioxane in water was calculated. The results obtained by the two rank annihilation factor analysis method show the efficiency of this method in determining the solution with high spectral overlap. As the percentage of solvents increases, the acid constant becomes smaller, which can be explained by the fact that the solubility and dielectric constant of water, acetonitrile and dioxane are different. The value of these variables depends on the physical parameters (dielectric constant and induction number).https://chemistry.semnan.ac.ir/article_8829_dd74c5bffad96ec7e96cffa4edf757a6.pdf‎4- (2-thiazole azo) rososinol ‎ultraviolet spectroscopy ‎two rank annihilation factor analysis ‎acid dissociation constant
spellingShingle Mansoor Namazian
Shahriar Jahanbani
Ali Benvidi
Measurement of 4-(2-thiazole azo) rososinol acidy constants by means of ultraviolet spectroscopy and chemometrics in water-acetonitrile and water-dioxane binary mixtures
شیمی کاربردی روز
‎4- (2-thiazole azo) rososinol ‎
ultraviolet spectroscopy ‎
two rank annihilation factor analysis ‎
acid dissociation constant
title Measurement of 4-(2-thiazole azo) rososinol acidy constants by means of ultraviolet spectroscopy and chemometrics in water-acetonitrile and water-dioxane binary mixtures
title_full Measurement of 4-(2-thiazole azo) rososinol acidy constants by means of ultraviolet spectroscopy and chemometrics in water-acetonitrile and water-dioxane binary mixtures
title_fullStr Measurement of 4-(2-thiazole azo) rososinol acidy constants by means of ultraviolet spectroscopy and chemometrics in water-acetonitrile and water-dioxane binary mixtures
title_full_unstemmed Measurement of 4-(2-thiazole azo) rososinol acidy constants by means of ultraviolet spectroscopy and chemometrics in water-acetonitrile and water-dioxane binary mixtures
title_short Measurement of 4-(2-thiazole azo) rososinol acidy constants by means of ultraviolet spectroscopy and chemometrics in water-acetonitrile and water-dioxane binary mixtures
title_sort measurement of 4 2 thiazole azo rososinol acidy constants by means of ultraviolet spectroscopy and chemometrics in water acetonitrile and water dioxane binary mixtures
topic ‎4- (2-thiazole azo) rososinol ‎
ultraviolet spectroscopy ‎
two rank annihilation factor analysis ‎
acid dissociation constant
url https://chemistry.semnan.ac.ir/article_8829_dd74c5bffad96ec7e96cffa4edf757a6.pdf
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