Experimental and Kinetic Study of CO Oxidation Over LaFe1-xCuxO3 (x=0, 0.2, 0.4, 0.6) Perovskite-Type Oxides

In this paper, catalytic oxidation of CO over the LaFe1-xCuxO3 (x= 0, 0.2, 0.4, 0.6) perovskite-type oxides was investigated. The catalysts were synthesized by sol-gel method and characterized by XRD, BET, FT-IR, H2-TPR and SEM methods. The catalytic activity of catalysts was tested in catalytic oxi...

Full description

Saved in:
Bibliographic Details
Main Authors: P. Rashidi Zonouz, M.E. Masoumi, A. Niaei, A. Tarjomannejad
Format: Article
Language:English
Published: Iranian Association of Chemical Engineering (IAChE) 2018-05-01
Series:Iranian Journal of Chemical Engineering
Subjects:
Online Access:https://www.ijche.com/article_67304_327261b61d6e199fcc0013efb42a978c.pdf
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1850178468581474304
author P. Rashidi Zonouz
M.E. Masoumi
A. Niaei
A. Tarjomannejad
author_facet P. Rashidi Zonouz
M.E. Masoumi
A. Niaei
A. Tarjomannejad
author_sort P. Rashidi Zonouz
collection DOAJ
description In this paper, catalytic oxidation of CO over the LaFe1-xCuxO3 (x= 0, 0.2, 0.4, 0.6) perovskite-type oxides was investigated. The catalysts were synthesized by sol-gel method and characterized by XRD, BET, FT-IR, H2-TPR and SEM methods. The catalytic activity of catalysts was tested in catalytic oxidation of CO. XRD patterns confirmed the synthesized perovskites to be single-phase perovskite-type oxides. The synthesized perovskite catalysts show high activity in the range of reaction temperature (50 - 300 ºC). The substitution of Cu in B-site of the perovskite catalysts enhanced their catalytic activity for CO oxidation. Among different synthesized perovskite catalysts, LaFe0.6Cu0.4O3 has the highest activity: nearly complete elimination of CO was achieved at 275 ºC with this catalyst. Kinetic studies for CO oxidation were performed based on power law and Mars-van Krevelen mechanisms. According to kinetic calculations, the most probable mechanism is the MKV-D (dissociative adsorption of oxygen) which can predict the experimental data with correlation coefficient of R2 > 0.995.
format Article
id doaj-art-eaabcecd4d314e789841ff9ee1e6c31b
institution OA Journals
issn 1735-5397
2008-2355
language English
publishDate 2018-05-01
publisher Iranian Association of Chemical Engineering (IAChE)
record_format Article
series Iranian Journal of Chemical Engineering
spelling doaj-art-eaabcecd4d314e789841ff9ee1e6c31b2025-08-20T02:18:43ZengIranian Association of Chemical Engineering (IAChE)Iranian Journal of Chemical Engineering1735-53972008-23552018-05-011529110267304Experimental and Kinetic Study of CO Oxidation Over LaFe1-xCuxO3 (x=0, 0.2, 0.4, 0.6) Perovskite-Type OxidesP. Rashidi Zonouz0M.E. Masoumi1A. Niaei2A. Tarjomannejad3Faculty of Engineering, Tehran North Branch, Islamic Azad University, Tehran, IranFaculty of Engineering, Tehran North Branch, Islamic Azad University, Tehran, IranDepartment of chemical Engineering & Petroleum, University of Tabriz, Tabriz, IranDepartment of chemical Engineering & Petroleum, University of Tabriz, Tabriz, IranIn this paper, catalytic oxidation of CO over the LaFe1-xCuxO3 (x= 0, 0.2, 0.4, 0.6) perovskite-type oxides was investigated. The catalysts were synthesized by sol-gel method and characterized by XRD, BET, FT-IR, H2-TPR and SEM methods. The catalytic activity of catalysts was tested in catalytic oxidation of CO. XRD patterns confirmed the synthesized perovskites to be single-phase perovskite-type oxides. The synthesized perovskite catalysts show high activity in the range of reaction temperature (50 - 300 ºC). The substitution of Cu in B-site of the perovskite catalysts enhanced their catalytic activity for CO oxidation. Among different synthesized perovskite catalysts, LaFe0.6Cu0.4O3 has the highest activity: nearly complete elimination of CO was achieved at 275 ºC with this catalyst. Kinetic studies for CO oxidation were performed based on power law and Mars-van Krevelen mechanisms. According to kinetic calculations, the most probable mechanism is the MKV-D (dissociative adsorption of oxygen) which can predict the experimental data with correlation coefficient of R2 > 0.995.https://www.ijche.com/article_67304_327261b61d6e199fcc0013efb42a978c.pdfco oxidationperovskitelafe1-xcuxo3kineticmvk mechanism
spellingShingle P. Rashidi Zonouz
M.E. Masoumi
A. Niaei
A. Tarjomannejad
Experimental and Kinetic Study of CO Oxidation Over LaFe1-xCuxO3 (x=0, 0.2, 0.4, 0.6) Perovskite-Type Oxides
Iranian Journal of Chemical Engineering
co oxidation
perovskite
lafe1-xcuxo3
kinetic
mvk mechanism
title Experimental and Kinetic Study of CO Oxidation Over LaFe1-xCuxO3 (x=0, 0.2, 0.4, 0.6) Perovskite-Type Oxides
title_full Experimental and Kinetic Study of CO Oxidation Over LaFe1-xCuxO3 (x=0, 0.2, 0.4, 0.6) Perovskite-Type Oxides
title_fullStr Experimental and Kinetic Study of CO Oxidation Over LaFe1-xCuxO3 (x=0, 0.2, 0.4, 0.6) Perovskite-Type Oxides
title_full_unstemmed Experimental and Kinetic Study of CO Oxidation Over LaFe1-xCuxO3 (x=0, 0.2, 0.4, 0.6) Perovskite-Type Oxides
title_short Experimental and Kinetic Study of CO Oxidation Over LaFe1-xCuxO3 (x=0, 0.2, 0.4, 0.6) Perovskite-Type Oxides
title_sort experimental and kinetic study of co oxidation over lafe1 xcuxo3 x 0 0 2 0 4 0 6 perovskite type oxides
topic co oxidation
perovskite
lafe1-xcuxo3
kinetic
mvk mechanism
url https://www.ijche.com/article_67304_327261b61d6e199fcc0013efb42a978c.pdf
work_keys_str_mv AT prashidizonouz experimentalandkineticstudyofcooxidationoverlafe1xcuxo3x0020406perovskitetypeoxides
AT memasoumi experimentalandkineticstudyofcooxidationoverlafe1xcuxo3x0020406perovskitetypeoxides
AT aniaei experimentalandkineticstudyofcooxidationoverlafe1xcuxo3x0020406perovskitetypeoxides
AT atarjomannejad experimentalandkineticstudyofcooxidationoverlafe1xcuxo3x0020406perovskitetypeoxides