Influence of exposure to phosphoric and polyacrylic acids on selected microscopic and physical/chemical properties of calcium hydroxide cements

Purpose This study aimed to evaluate if the contact of calcium hydroxide cements with polyacrylic and phosphoric acids would alter selected microscopic and physical and chemical properties. Materials and Methods Chemically activated (Hydro C and Dycal Advanced Formula II) and resin-modified photoact...

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Main Authors: Isabela Dantas Torres De Araújo, Renato Barbosa Soares, Camila Pessoa Lopes, Isana Álvares Ferreira, Boniek Castillo Dutra Borges
Format: Article
Language:English
Published: Istanbul University 2020-05-01
Series:European Oral Research
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Online Access:https://cdn.istanbul.edu.tr/file/JTA6CLJ8T5/B48346EFEB134312854C706D2F240576
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author Isabela Dantas Torres De Araújo
Renato Barbosa Soares
Camila Pessoa Lopes
Isana Álvares Ferreira
Boniek Castillo Dutra Borges
author_facet Isabela Dantas Torres De Araújo
Renato Barbosa Soares
Camila Pessoa Lopes
Isana Álvares Ferreira
Boniek Castillo Dutra Borges
author_sort Isabela Dantas Torres De Araújo
collection DOAJ
description Purpose This study aimed to evaluate if the contact of calcium hydroxide cements with polyacrylic and phosphoric acids would alter selected microscopic and physical and chemical properties. Materials and Methods Chemically activated (Hydro C and Dycal Advanced Formula II) and resin-modified photoactivated (Ultra-blend Plus) calcium hydroxide cements were examined after exposure to the following different strategies: contact with no substance (control group); rinsing with water and drying; contact with polyacrylic acid, rinsing with water, and drying; and contact with phosphoric acid, rinsing with water, and drying. Surface morphology, determined by scanning electron microscopy (SEM), water sorption and solubility, and the release of hydroxyl ions were evaluated. Results SEM showed a greater impact of the conditioning acids on the surface of the chemically activated cements. Ultra-blend Plus obtained the highest value of sorption (516.8 μg/mm3 ) and solubility (381.1 μg/mm3 ) and Hydro C had the lowest values 251.9 μg/mm3 and 206.3 μg/mm3 respectively. Considering the release of hydroxyl ions in comparison with time, Hydro C and Ultra-blend Plus presented significant statistical difference for polyacrylic and phosphoric acid subgroups. Conclusion Hydro C and Dycal presented intensification of surface irregularities after contact with conditioning acids. The chemically activated materials suffered a decrease in sorption and solubility. The action of the conditioning acids promotes greater increase of the release of hydroxyl ions for Hydro C and Dycal.
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spelling doaj-art-e9640994893c4d47b5f8f09f055fa58f2025-08-20T01:48:11ZengIstanbul UniversityEuropean Oral Research2651-28232020-05-01542697610.26650/eor.20200057123456Influence of exposure to phosphoric and polyacrylic acids on selected microscopic and physical/chemical properties of calcium hydroxide cementsIsabela Dantas Torres De Araújo0https://orcid.org/0000-0002-3946-9303Renato Barbosa Soares1https://orcid.org/0000-0003-2990-1593Camila Pessoa Lopes2https://orcid.org/0000-0002-1494-0867Isana Álvares Ferreira3https://orcid.org/0000-0002-0301-5692Boniek Castillo Dutra Borges4https://orcid.org/0000-0003-4313-5776Federal University of Rio Grande do Norte, Rio-Grande, BrazilFederal University of Rio Grande do Norte, Rio-Grande, BrazilFederal University of Rio Grande do Norte, Rio-Grande, BrazilFederal University of Rio Grande do Norte, Rio-Grande, BrazilFederal University of Rio Grande do Norte, Rio-Grande, BrazilPurpose This study aimed to evaluate if the contact of calcium hydroxide cements with polyacrylic and phosphoric acids would alter selected microscopic and physical and chemical properties. Materials and Methods Chemically activated (Hydro C and Dycal Advanced Formula II) and resin-modified photoactivated (Ultra-blend Plus) calcium hydroxide cements were examined after exposure to the following different strategies: contact with no substance (control group); rinsing with water and drying; contact with polyacrylic acid, rinsing with water, and drying; and contact with phosphoric acid, rinsing with water, and drying. Surface morphology, determined by scanning electron microscopy (SEM), water sorption and solubility, and the release of hydroxyl ions were evaluated. Results SEM showed a greater impact of the conditioning acids on the surface of the chemically activated cements. Ultra-blend Plus obtained the highest value of sorption (516.8 μg/mm3 ) and solubility (381.1 μg/mm3 ) and Hydro C had the lowest values 251.9 μg/mm3 and 206.3 μg/mm3 respectively. Considering the release of hydroxyl ions in comparison with time, Hydro C and Ultra-blend Plus presented significant statistical difference for polyacrylic and phosphoric acid subgroups. Conclusion Hydro C and Dycal presented intensification of surface irregularities after contact with conditioning acids. The chemically activated materials suffered a decrease in sorption and solubility. The action of the conditioning acids promotes greater increase of the release of hydroxyl ions for Hydro C and Dycal.https://cdn.istanbul.edu.tr/file/JTA6CLJ8T5/B48346EFEB134312854C706D2F240576calcium hydroxidehydrogen ion concentrationsolubilitysurface morphologywater absorption
spellingShingle Isabela Dantas Torres De Araújo
Renato Barbosa Soares
Camila Pessoa Lopes
Isana Álvares Ferreira
Boniek Castillo Dutra Borges
Influence of exposure to phosphoric and polyacrylic acids on selected microscopic and physical/chemical properties of calcium hydroxide cements
European Oral Research
calcium hydroxide
hydrogen ion concentration
solubility
surface morphology
water absorption
title Influence of exposure to phosphoric and polyacrylic acids on selected microscopic and physical/chemical properties of calcium hydroxide cements
title_full Influence of exposure to phosphoric and polyacrylic acids on selected microscopic and physical/chemical properties of calcium hydroxide cements
title_fullStr Influence of exposure to phosphoric and polyacrylic acids on selected microscopic and physical/chemical properties of calcium hydroxide cements
title_full_unstemmed Influence of exposure to phosphoric and polyacrylic acids on selected microscopic and physical/chemical properties of calcium hydroxide cements
title_short Influence of exposure to phosphoric and polyacrylic acids on selected microscopic and physical/chemical properties of calcium hydroxide cements
title_sort influence of exposure to phosphoric and polyacrylic acids on selected microscopic and physical chemical properties of calcium hydroxide cements
topic calcium hydroxide
hydrogen ion concentration
solubility
surface morphology
water absorption
url https://cdn.istanbul.edu.tr/file/JTA6CLJ8T5/B48346EFEB134312854C706D2F240576
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