Elimination of Escherichia coli in a Packed Column Containing Jujube Seed Kernel Granular Activated Carbon Coated With Silver Nanoparticles (Ag-NPs/GAC)

This study aims to develop a filter material capable of inhibiting bacterial growth and eliminating microorganisms from filtered water. Granular activated carbon (GAC) was prepared from jujube seed kernels by a chemical activation method whereby the kernels were heated at 650°C for 3 h in the presen...

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Main Authors: Ngounou M. Kameni, Mengue Nsoe, Esegni V. Amba, Guillaume Kofa, Koungou S. Ndi, Guifo J. Kayem
Format: Article
Language:English
Published: Wiley 2025-01-01
Series:Journal of Chemistry
Online Access:http://dx.doi.org/10.1155/joch/2260823
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author Ngounou M. Kameni
Mengue Nsoe
Esegni V. Amba
Guillaume Kofa
Koungou S. Ndi
Guifo J. Kayem
author_facet Ngounou M. Kameni
Mengue Nsoe
Esegni V. Amba
Guillaume Kofa
Koungou S. Ndi
Guifo J. Kayem
author_sort Ngounou M. Kameni
collection DOAJ
description This study aims to develop a filter material capable of inhibiting bacterial growth and eliminating microorganisms from filtered water. Granular activated carbon (GAC) was prepared from jujube seed kernels by a chemical activation method whereby the kernels were heated at 650°C for 3 h in the presence of varied concentrations of phosphoric acid (H3PO4) (1, 2 and 3 M). Silver nanoparticles (Ag-NPs) were prepared using the polysaccharide reduction method with AgNO3 at two concentrations (2 and 4 mmol). The Ag-NPs obtained were characterised by a UV–visible spectrophotometer, optical microscope and microorganism inhibition test. GAC was coated with Ag-NPs by impregnating it with a fixed concentration of Ag-NPs in a supersaturated solution. The resulting GAC and Ag-NPs/GAC were characterised using several methods (pH, point zero charge and FTIR). The leakage of Ag fixed on GAC was evaluated. The antimicrobial properties of the synthesised Ag-NPs/GAC were investigated using inhibition zone, impregnation and column techniques against E. coli. The best nanoparticle shape with a large reactive surface was obtained after treatment with 2 mmol of AgNO3. There was no leaching of Ag ions in the treated water after passage through the bed. Except for the GAC not impregnated with Ag-NPs, no E. coli CFU/mL was found in the filtered water obtained from Ag-NPs/GAC beds at all tested pHs after 2–3 days of operation.
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spelling doaj-art-e8dd44748c694e16b8912e706fafcf9d2025-08-20T02:45:42ZengWileyJournal of Chemistry2090-90712025-01-01202510.1155/joch/2260823Elimination of Escherichia coli in a Packed Column Containing Jujube Seed Kernel Granular Activated Carbon Coated With Silver Nanoparticles (Ag-NPs/GAC)Ngounou M. Kameni0Mengue Nsoe1Esegni V. Amba2Guillaume Kofa3Koungou S. Ndi4Guifo J. Kayem5Department of Process EngineeringDepartment of Process EngineeringDepartment of Process EngineeringDepartment of Process EngineeringDepartment of Process EngineeringDepartment of Process EngineeringThis study aims to develop a filter material capable of inhibiting bacterial growth and eliminating microorganisms from filtered water. Granular activated carbon (GAC) was prepared from jujube seed kernels by a chemical activation method whereby the kernels were heated at 650°C for 3 h in the presence of varied concentrations of phosphoric acid (H3PO4) (1, 2 and 3 M). Silver nanoparticles (Ag-NPs) were prepared using the polysaccharide reduction method with AgNO3 at two concentrations (2 and 4 mmol). The Ag-NPs obtained were characterised by a UV–visible spectrophotometer, optical microscope and microorganism inhibition test. GAC was coated with Ag-NPs by impregnating it with a fixed concentration of Ag-NPs in a supersaturated solution. The resulting GAC and Ag-NPs/GAC were characterised using several methods (pH, point zero charge and FTIR). The leakage of Ag fixed on GAC was evaluated. The antimicrobial properties of the synthesised Ag-NPs/GAC were investigated using inhibition zone, impregnation and column techniques against E. coli. The best nanoparticle shape with a large reactive surface was obtained after treatment with 2 mmol of AgNO3. There was no leaching of Ag ions in the treated water after passage through the bed. Except for the GAC not impregnated with Ag-NPs, no E. coli CFU/mL was found in the filtered water obtained from Ag-NPs/GAC beds at all tested pHs after 2–3 days of operation.http://dx.doi.org/10.1155/joch/2260823
spellingShingle Ngounou M. Kameni
Mengue Nsoe
Esegni V. Amba
Guillaume Kofa
Koungou S. Ndi
Guifo J. Kayem
Elimination of Escherichia coli in a Packed Column Containing Jujube Seed Kernel Granular Activated Carbon Coated With Silver Nanoparticles (Ag-NPs/GAC)
Journal of Chemistry
title Elimination of Escherichia coli in a Packed Column Containing Jujube Seed Kernel Granular Activated Carbon Coated With Silver Nanoparticles (Ag-NPs/GAC)
title_full Elimination of Escherichia coli in a Packed Column Containing Jujube Seed Kernel Granular Activated Carbon Coated With Silver Nanoparticles (Ag-NPs/GAC)
title_fullStr Elimination of Escherichia coli in a Packed Column Containing Jujube Seed Kernel Granular Activated Carbon Coated With Silver Nanoparticles (Ag-NPs/GAC)
title_full_unstemmed Elimination of Escherichia coli in a Packed Column Containing Jujube Seed Kernel Granular Activated Carbon Coated With Silver Nanoparticles (Ag-NPs/GAC)
title_short Elimination of Escherichia coli in a Packed Column Containing Jujube Seed Kernel Granular Activated Carbon Coated With Silver Nanoparticles (Ag-NPs/GAC)
title_sort elimination of escherichia coli in a packed column containing jujube seed kernel granular activated carbon coated with silver nanoparticles ag nps gac
url http://dx.doi.org/10.1155/joch/2260823
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