Zusammensetzung und Dichte der Harnstoffschmelze und der koexistierenden Gasphase

An experimental method for the determination of the composition and density of the coexisting phases in the vapour-liquid carbon dioxide/ammonia/water equilibrium system at high pressure and temperature is presented. Apart from the elemental analysis of the vapour phase, which required a specially...

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Main Authors: W. Durisch, A. Buck
Format: Article
Language:deu
Published: Swiss Chemical Society 1975-10-01
Series:CHIMIA
Online Access:https://www.chimia.ch/chimia/article/view/9248
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author W. Durisch
A. Buck
author_facet W. Durisch
A. Buck
author_sort W. Durisch
collection DOAJ
description An experimental method for the determination of the composition and density of the coexisting phases in the vapour-liquid carbon dioxide/ammonia/water equilibrium system at high pressure and temperature is presented. Apart from the elemental analysis of the vapour phase, which required a specially developed sampling procedure, the chemical analyses were carried out by ordinary analytical methods. For the measurement of the vapour phase density, a high pressure high temperature gas pycnometer from a high alloy stainless steel was used. Results, including the concentration of urea in the vapour phase and of ammonium carbamate in the liquid phase are given for a charge density of 0.53 g/cm3, at a temperature of 170 °C, and initial NH3:CO2 and H2O:CO2 molar ratios of 2 and 0, resp.
format Article
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2673-2424
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publishDate 1975-10-01
publisher Swiss Chemical Society
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series CHIMIA
spelling doaj-art-e82d15ee583b4a7ab327559bcafadddb2025-08-20T02:29:54ZdeuSwiss Chemical SocietyCHIMIA0009-42932673-24241975-10-01291010.2533/chimia.1975.436Zusammensetzung und Dichte der Harnstoffschmelze und der koexistierenden GasphaseW. Durisch0A. Buck1Institut für Verfahrens- und Kältetechnik an der ETH Zürich, Sonneggstraße 3, 8006 ZürichInstitut für Verfahrens- und Kältetechnik an der ETH Zürich, Sonneggstraße 3, 8006 Zürich An experimental method for the determination of the composition and density of the coexisting phases in the vapour-liquid carbon dioxide/ammonia/water equilibrium system at high pressure and temperature is presented. Apart from the elemental analysis of the vapour phase, which required a specially developed sampling procedure, the chemical analyses were carried out by ordinary analytical methods. For the measurement of the vapour phase density, a high pressure high temperature gas pycnometer from a high alloy stainless steel was used. Results, including the concentration of urea in the vapour phase and of ammonium carbamate in the liquid phase are given for a charge density of 0.53 g/cm3, at a temperature of 170 °C, and initial NH3:CO2 and H2O:CO2 molar ratios of 2 and 0, resp. https://www.chimia.ch/chimia/article/view/9248
spellingShingle W. Durisch
A. Buck
Zusammensetzung und Dichte der Harnstoffschmelze und der koexistierenden Gasphase
CHIMIA
title Zusammensetzung und Dichte der Harnstoffschmelze und der koexistierenden Gasphase
title_full Zusammensetzung und Dichte der Harnstoffschmelze und der koexistierenden Gasphase
title_fullStr Zusammensetzung und Dichte der Harnstoffschmelze und der koexistierenden Gasphase
title_full_unstemmed Zusammensetzung und Dichte der Harnstoffschmelze und der koexistierenden Gasphase
title_short Zusammensetzung und Dichte der Harnstoffschmelze und der koexistierenden Gasphase
title_sort zusammensetzung und dichte der harnstoffschmelze und der koexistierenden gasphase
url https://www.chimia.ch/chimia/article/view/9248
work_keys_str_mv AT wdurisch zusammensetzungunddichtederharnstoffschmelzeundderkoexistierendengasphase
AT abuck zusammensetzungunddichtederharnstoffschmelzeundderkoexistierendengasphase