Tailoring Nanopore Geometry in Anodic Aluminum Oxide Membranes through Physical Stretching and Controlled Anodization

Abstract The fabrication and application of anodic aluminum oxide (AAO) membranes with tailored nanopore geometries have profound implications in materials science and engineering. This study introduces a refined physical stretching method combined with precisely controlled anodization conditions to...

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Main Authors: Yu‐Chun Liu, Yi‐Fan Chen, Yu‐Chun Lin, You‐Hao Zheng, Lin‐Ruei Lee, Ming‐Hsuan Chang, Jhih‐Hao Ho, Yu‐Liang Lin, Jiun‐Tai Chen
Format: Article
Language:English
Published: Wiley-VCH 2025-03-01
Series:Advanced Materials Interfaces
Subjects:
Online Access:https://doi.org/10.1002/admi.202400699
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author Yu‐Chun Liu
Yi‐Fan Chen
Yu‐Chun Lin
You‐Hao Zheng
Lin‐Ruei Lee
Ming‐Hsuan Chang
Jhih‐Hao Ho
Yu‐Liang Lin
Jiun‐Tai Chen
author_facet Yu‐Chun Liu
Yi‐Fan Chen
Yu‐Chun Lin
You‐Hao Zheng
Lin‐Ruei Lee
Ming‐Hsuan Chang
Jhih‐Hao Ho
Yu‐Liang Lin
Jiun‐Tai Chen
author_sort Yu‐Chun Liu
collection DOAJ
description Abstract The fabrication and application of anodic aluminum oxide (AAO) membranes with tailored nanopore geometries have profound implications in materials science and engineering. This study introduces a refined physical stretching method combined with precisely controlled anodization conditions to manipulate the anisotropy of nanopores in AAO membranes. By employing high‐purity aluminum sheets and varying electrolytes such as sulfuric acid, oxalic acid, and phosphoric acid, anisotropic shapes are carried out with aspect ratios varying based on the applied mechanical forces and electrolytic conditions. The capability to produce AAO membranes with non‐uniform pore distributions is also demonstrated by applying irregular stretching forces, revealing the potential for creating customized nanostructures. The anisotropic AAO membranes serve as effective templates for synthesizing polymer nanorods, indicating their utility in guiding the formation of advanced nanomaterials with specific directional properties. Our results showcase the role of mechanical and chemical parameters in tailoring nanoscale material properties. The versatility of horizontally anisotropic AAO membranes in nanofabrication enables better control of nanopore geometry for applications in nanoelectronics, drug delivery, and biosensing.
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institution DOAJ
issn 2196-7350
language English
publishDate 2025-03-01
publisher Wiley-VCH
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series Advanced Materials Interfaces
spelling doaj-art-e7a6b952bb3b49e2b7874ebb8b4593a32025-08-20T02:52:08ZengWiley-VCHAdvanced Materials Interfaces2196-73502025-03-01126n/an/a10.1002/admi.202400699Tailoring Nanopore Geometry in Anodic Aluminum Oxide Membranes through Physical Stretching and Controlled AnodizationYu‐Chun Liu0Yi‐Fan Chen1Yu‐Chun Lin2You‐Hao Zheng3Lin‐Ruei Lee4Ming‐Hsuan Chang5Jhih‐Hao Ho6Yu‐Liang Lin7Jiun‐Tai Chen8Department of Applied Chemistry National Yang Ming Chiao Tung University Hsinchu 300093 TaiwanDepartment of Applied Chemistry National Yang Ming Chiao Tung University Hsinchu 300093 TaiwanDepartment of Applied Chemistry National Yang Ming Chiao Tung University Hsinchu 300093 TaiwanDepartment of Applied Chemistry National Yang Ming Chiao Tung University Hsinchu 300093 TaiwanDepartment of Applied Chemistry National Yang Ming Chiao Tung University Hsinchu 300093 TaiwanDepartment of Applied Chemistry National Yang Ming Chiao Tung University Hsinchu 300093 TaiwanDepartment of Applied Chemistry National Yang Ming Chiao Tung University Hsinchu 300093 TaiwanDepartment of Applied Chemistry National Yang Ming Chiao Tung University Hsinchu 300093 TaiwanDepartment of Applied Chemistry National Yang Ming Chiao Tung University Hsinchu 300093 TaiwanAbstract The fabrication and application of anodic aluminum oxide (AAO) membranes with tailored nanopore geometries have profound implications in materials science and engineering. This study introduces a refined physical stretching method combined with precisely controlled anodization conditions to manipulate the anisotropy of nanopores in AAO membranes. By employing high‐purity aluminum sheets and varying electrolytes such as sulfuric acid, oxalic acid, and phosphoric acid, anisotropic shapes are carried out with aspect ratios varying based on the applied mechanical forces and electrolytic conditions. The capability to produce AAO membranes with non‐uniform pore distributions is also demonstrated by applying irregular stretching forces, revealing the potential for creating customized nanostructures. The anisotropic AAO membranes serve as effective templates for synthesizing polymer nanorods, indicating their utility in guiding the formation of advanced nanomaterials with specific directional properties. Our results showcase the role of mechanical and chemical parameters in tailoring nanoscale material properties. The versatility of horizontally anisotropic AAO membranes in nanofabrication enables better control of nanopore geometry for applications in nanoelectronics, drug delivery, and biosensing.https://doi.org/10.1002/admi.202400699anisotropicanodic aluminum oxideanodizationphysical stretching nanorods
spellingShingle Yu‐Chun Liu
Yi‐Fan Chen
Yu‐Chun Lin
You‐Hao Zheng
Lin‐Ruei Lee
Ming‐Hsuan Chang
Jhih‐Hao Ho
Yu‐Liang Lin
Jiun‐Tai Chen
Tailoring Nanopore Geometry in Anodic Aluminum Oxide Membranes through Physical Stretching and Controlled Anodization
Advanced Materials Interfaces
anisotropic
anodic aluminum oxide
anodization
physical stretching nanorods
title Tailoring Nanopore Geometry in Anodic Aluminum Oxide Membranes through Physical Stretching and Controlled Anodization
title_full Tailoring Nanopore Geometry in Anodic Aluminum Oxide Membranes through Physical Stretching and Controlled Anodization
title_fullStr Tailoring Nanopore Geometry in Anodic Aluminum Oxide Membranes through Physical Stretching and Controlled Anodization
title_full_unstemmed Tailoring Nanopore Geometry in Anodic Aluminum Oxide Membranes through Physical Stretching and Controlled Anodization
title_short Tailoring Nanopore Geometry in Anodic Aluminum Oxide Membranes through Physical Stretching and Controlled Anodization
title_sort tailoring nanopore geometry in anodic aluminum oxide membranes through physical stretching and controlled anodization
topic anisotropic
anodic aluminum oxide
anodization
physical stretching nanorods
url https://doi.org/10.1002/admi.202400699
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