Construction of self-supporting heterobimetallic phosphides for oxygen evolution reaction

Electrocatalysts with heterobimetallic active sites are considered to be effective geometries for electrocatalytic oxygen evolution reaction (OER). However, MOF-derived heterobimetallic phosphides are uncontrollable and the addition of traditional binders is complicated. Here, we designed an efficie...

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Main Authors: Adjapong Linda Akua Agyapomaa, Chulong Jin, Qingqing Zhang, Xiaojun Zeng
Format: Article
Language:English
Published: Elsevier 2025-09-01
Series:Materials Today Catalysis
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Online Access:http://www.sciencedirect.com/science/article/pii/S2949754X25000274
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author Adjapong Linda Akua Agyapomaa
Chulong Jin
Qingqing Zhang
Xiaojun Zeng
author_facet Adjapong Linda Akua Agyapomaa
Chulong Jin
Qingqing Zhang
Xiaojun Zeng
author_sort Adjapong Linda Akua Agyapomaa
collection DOAJ
description Electrocatalysts with heterobimetallic active sites are considered to be effective geometries for electrocatalytic oxygen evolution reaction (OER). However, MOF-derived heterobimetallic phosphides are uncontrollable and the addition of traditional binders is complicated. Here, we designed an efficient defect-rich (NF/Ni2P-Fe2P@NC) heterostructure derived from NF/Fe-MOF, in which nickel foam (NF) provides a supporting role and Ni source to promote the formation of heterobimetallic phosphides (Ni2P, Fe2P). NF/Ni2P-Fe2P@NC inherits remarkable OER performance with ultralow overpotential of 123 mV at a current density of 10 mA cm−2 and Tafel slope of 51. 3 mV dec−1 in alkaline electrolyte. The experimental results unravel that the multi-components (Ni2P, Fe2P, NC), rich heterogeneous interfaces (Ni2P/Fe2P), and numerous defects in the heterostructure provide abundant active sites, optimize the electronic structure, and improve the exposure of active sites, thereby promoting the electrocatalytic OER process. Density functional theory (DFT) calculations confirm that the free energy barrier for the catalyst to generate *OOH intermediates is low. Our findings present a simple and economical approach to obtaining heterobimetallic phosphides with robust OER performance.
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spelling doaj-art-e6ee85f4fe1a4d07a16343816baabcc22025-08-20T03:41:36ZengElsevierMaterials Today Catalysis2949-754X2025-09-011010011410.1016/j.mtcata.2025.100114Construction of self-supporting heterobimetallic phosphides for oxygen evolution reactionAdjapong Linda Akua Agyapomaa0Chulong Jin1Qingqing Zhang2Xiaojun Zeng3School of Materials Science and Engineering, Jingdezhen Ceramic University, Jingdezhen 333403, ChinaSchool of Materials Science and Engineering, Jingdezhen Ceramic University, Jingdezhen 333403, ChinaSchool of Materials Science and Engineering, Jingdezhen Ceramic University, Jingdezhen 333403, ChinaCorresponding author.; School of Materials Science and Engineering, Jingdezhen Ceramic University, Jingdezhen 333403, ChinaElectrocatalysts with heterobimetallic active sites are considered to be effective geometries for electrocatalytic oxygen evolution reaction (OER). However, MOF-derived heterobimetallic phosphides are uncontrollable and the addition of traditional binders is complicated. Here, we designed an efficient defect-rich (NF/Ni2P-Fe2P@NC) heterostructure derived from NF/Fe-MOF, in which nickel foam (NF) provides a supporting role and Ni source to promote the formation of heterobimetallic phosphides (Ni2P, Fe2P). NF/Ni2P-Fe2P@NC inherits remarkable OER performance with ultralow overpotential of 123 mV at a current density of 10 mA cm−2 and Tafel slope of 51. 3 mV dec−1 in alkaline electrolyte. The experimental results unravel that the multi-components (Ni2P, Fe2P, NC), rich heterogeneous interfaces (Ni2P/Fe2P), and numerous defects in the heterostructure provide abundant active sites, optimize the electronic structure, and improve the exposure of active sites, thereby promoting the electrocatalytic OER process. Density functional theory (DFT) calculations confirm that the free energy barrier for the catalyst to generate *OOH intermediates is low. Our findings present a simple and economical approach to obtaining heterobimetallic phosphides with robust OER performance.http://www.sciencedirect.com/science/article/pii/S2949754X25000274Self-supportingHeterobimetallic phosphidesDefectsIon exchangeOxygen evolution reaction
spellingShingle Adjapong Linda Akua Agyapomaa
Chulong Jin
Qingqing Zhang
Xiaojun Zeng
Construction of self-supporting heterobimetallic phosphides for oxygen evolution reaction
Materials Today Catalysis
Self-supporting
Heterobimetallic phosphides
Defects
Ion exchange
Oxygen evolution reaction
title Construction of self-supporting heterobimetallic phosphides for oxygen evolution reaction
title_full Construction of self-supporting heterobimetallic phosphides for oxygen evolution reaction
title_fullStr Construction of self-supporting heterobimetallic phosphides for oxygen evolution reaction
title_full_unstemmed Construction of self-supporting heterobimetallic phosphides for oxygen evolution reaction
title_short Construction of self-supporting heterobimetallic phosphides for oxygen evolution reaction
title_sort construction of self supporting heterobimetallic phosphides for oxygen evolution reaction
topic Self-supporting
Heterobimetallic phosphides
Defects
Ion exchange
Oxygen evolution reaction
url http://www.sciencedirect.com/science/article/pii/S2949754X25000274
work_keys_str_mv AT adjaponglindaakuaagyapomaa constructionofselfsupportingheterobimetallicphosphidesforoxygenevolutionreaction
AT chulongjin constructionofselfsupportingheterobimetallicphosphidesforoxygenevolutionreaction
AT qingqingzhang constructionofselfsupportingheterobimetallicphosphidesforoxygenevolutionreaction
AT xiaojunzeng constructionofselfsupportingheterobimetallicphosphidesforoxygenevolutionreaction