Comparative Evaluation of Tooth Discoloration Induced by an Experimental Antibiotic Paste Modified with Nano Chitosan: An In Vitro Study

<b>Background/Objectives:</b> Tooth discoloration is a common concern associated with the use of intra-canal medicaments, particularly those containing antibiotics. This study aims to evaluate the tooth discoloration potential of an experimental antibiotic paste modified with Nano Chitos...

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Main Authors: Mohamed Ahmed Elsayed, Md Sofiqul Islam, Safiya Ali, Zainab Hussain, Muhammed Mustahsen Rahman, Okba Mahmoud
Format: Article
Language:English
Published: MDPI AG 2025-07-01
Series:Dentistry Journal
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Online Access:https://www.mdpi.com/2304-6767/13/7/307
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author Mohamed Ahmed Elsayed
Md Sofiqul Islam
Safiya Ali
Zainab Hussain
Muhammed Mustahsen Rahman
Okba Mahmoud
author_facet Mohamed Ahmed Elsayed
Md Sofiqul Islam
Safiya Ali
Zainab Hussain
Muhammed Mustahsen Rahman
Okba Mahmoud
author_sort Mohamed Ahmed Elsayed
collection DOAJ
description <b>Background/Objectives:</b> Tooth discoloration is a common concern associated with the use of intra-canal medicaments, particularly those containing antibiotics. This study aims to evaluate the tooth discoloration potential of an experimental antibiotic paste modified with Nano Chitosan (APNC) and compare it with two antibiotic pastes and two calcium hydroxide-based pastes over different time intervals. <b>Methods</b>: Fifty bovine incisors were standardized and prepared up to size 60. The teeth were randomly assigned into five groups based on the medicament applied: Metapaste, Metapex, modified Triple Antibiotic Paste (mTAP), Double Antibiotic Paste (DAP), and APNC. A digital spectrophotometer was used to measure the color parameters (L*, a*, and b*) at two zones, above and below the cemento-enamel junction (CEJ), across four-time points: before application (T0- baseline), immediately after application (T1), after two weeks (T2), and after one month (T3). The color changes (ΔE) were calculated and statistically analyzed using repeated-measure ANOVA. <b>Results</b>: Statistically significant differences in discoloration were observed between the tested medicaments after one month (<i>p</i> < 0.05). mTAP caused the highest ΔE values both above and below the CEJ at all time points, particularly after one month (<i>p</i> < 0.05). Conversely, APNC, Metapaste, and DAP demonstrated the least discoloration, with no significant differences among them. The degree of discoloration was time-dependent and more pronounced below the CEJ in all groups. <b>Conclusions</b>: After one month, the experimental APNC paste induced tooth discoloration comparable to that of Metapaste, indicating minimal esthetic compromise. APNC may be a promising alternative to traditional antibiotic pastes with minimal discoloration effects.
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spelling doaj-art-e698b8b3ad5c483fadda3689830497bb2025-08-20T03:08:05ZengMDPI AGDentistry Journal2304-67672025-07-0113730710.3390/dj13070307Comparative Evaluation of Tooth Discoloration Induced by an Experimental Antibiotic Paste Modified with Nano Chitosan: An In Vitro StudyMohamed Ahmed Elsayed0Md Sofiqul Islam1Safiya Ali2Zainab Hussain3Muhammed Mustahsen Rahman4Okba Mahmoud5Department of Endodontics, RAK College of Dental Sciences, RAK Medical and Health Sciences University, Ras Al-Khaimah P.O. Box 12973, United Arab EmiratesDepartment of Operative Dentistry, RAK College of Dental Sciences, RAK Medical and Health Sciences University, Ras Al-Khaimah P.O. Box 12973, United Arab EmiratesDepartment of Clinical Science, RAK College of Dental Sciences, RAK Medical and Health Sciences University, Ras Al-Khaimah P.O. Box 12973, United Arab EmiratesDepartment of Clinical Science, RAK College of Dental Sciences, RAK Medical and Health Sciences University, Ras Al-Khaimah P.O. Box 12973, United Arab EmiratesDepartment of Periodontology, RAK College of Dental Sciences, RAK Medical and Health Sciences University, Ras Al-Khaimah, P.O. Box 12973, United Arab EmiratesDepartment of Clinical Sciences, College of Dentistry, Ajman University, Ajman P.O. Box 346, United Arab Emirates<b>Background/Objectives:</b> Tooth discoloration is a common concern associated with the use of intra-canal medicaments, particularly those containing antibiotics. This study aims to evaluate the tooth discoloration potential of an experimental antibiotic paste modified with Nano Chitosan (APNC) and compare it with two antibiotic pastes and two calcium hydroxide-based pastes over different time intervals. <b>Methods</b>: Fifty bovine incisors were standardized and prepared up to size 60. The teeth were randomly assigned into five groups based on the medicament applied: Metapaste, Metapex, modified Triple Antibiotic Paste (mTAP), Double Antibiotic Paste (DAP), and APNC. A digital spectrophotometer was used to measure the color parameters (L*, a*, and b*) at two zones, above and below the cemento-enamel junction (CEJ), across four-time points: before application (T0- baseline), immediately after application (T1), after two weeks (T2), and after one month (T3). The color changes (ΔE) were calculated and statistically analyzed using repeated-measure ANOVA. <b>Results</b>: Statistically significant differences in discoloration were observed between the tested medicaments after one month (<i>p</i> < 0.05). mTAP caused the highest ΔE values both above and below the CEJ at all time points, particularly after one month (<i>p</i> < 0.05). Conversely, APNC, Metapaste, and DAP demonstrated the least discoloration, with no significant differences among them. The degree of discoloration was time-dependent and more pronounced below the CEJ in all groups. <b>Conclusions</b>: After one month, the experimental APNC paste induced tooth discoloration comparable to that of Metapaste, indicating minimal esthetic compromise. APNC may be a promising alternative to traditional antibiotic pastes with minimal discoloration effects.https://www.mdpi.com/2304-6767/13/7/307calcium hydroxideintracanal medicamentsnano chitosanspectrophotometric analysistriple antibiotic pastetooth discoloration
spellingShingle Mohamed Ahmed Elsayed
Md Sofiqul Islam
Safiya Ali
Zainab Hussain
Muhammed Mustahsen Rahman
Okba Mahmoud
Comparative Evaluation of Tooth Discoloration Induced by an Experimental Antibiotic Paste Modified with Nano Chitosan: An In Vitro Study
Dentistry Journal
calcium hydroxide
intracanal medicaments
nano chitosan
spectrophotometric analysis
triple antibiotic paste
tooth discoloration
title Comparative Evaluation of Tooth Discoloration Induced by an Experimental Antibiotic Paste Modified with Nano Chitosan: An In Vitro Study
title_full Comparative Evaluation of Tooth Discoloration Induced by an Experimental Antibiotic Paste Modified with Nano Chitosan: An In Vitro Study
title_fullStr Comparative Evaluation of Tooth Discoloration Induced by an Experimental Antibiotic Paste Modified with Nano Chitosan: An In Vitro Study
title_full_unstemmed Comparative Evaluation of Tooth Discoloration Induced by an Experimental Antibiotic Paste Modified with Nano Chitosan: An In Vitro Study
title_short Comparative Evaluation of Tooth Discoloration Induced by an Experimental Antibiotic Paste Modified with Nano Chitosan: An In Vitro Study
title_sort comparative evaluation of tooth discoloration induced by an experimental antibiotic paste modified with nano chitosan an in vitro study
topic calcium hydroxide
intracanal medicaments
nano chitosan
spectrophotometric analysis
triple antibiotic paste
tooth discoloration
url https://www.mdpi.com/2304-6767/13/7/307
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AT safiyaali comparativeevaluationoftoothdiscolorationinducedbyanexperimentalantibioticpastemodifiedwithnanochitosananinvitrostudy
AT zainabhussain comparativeevaluationoftoothdiscolorationinducedbyanexperimentalantibioticpastemodifiedwithnanochitosananinvitrostudy
AT muhammedmustahsenrahman comparativeevaluationoftoothdiscolorationinducedbyanexperimentalantibioticpastemodifiedwithnanochitosananinvitrostudy
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