Measurement of protein non-covalent interactions in buffer and cells

Nuclear magnetic resonance (NMR) serves as a powerful tool for studying both the structure and dynamics of proteins. The NOE method, alongside residual dipolar; coupling, paramagnetic effects, J-coupling, and other related techniques, has reached a level of maturity that allows for the determination...

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Main Authors: Jingwen Li, Xiangfei Song, Lishan Yao
Format: Article
Language:English
Published: KeAi Communications Co. Ltd. 2025-05-01
Series:Magnetic Resonance Letters
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Online Access:http://www.sciencedirect.com/science/article/pii/S2772516224000809
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author Jingwen Li
Xiangfei Song
Lishan Yao
author_facet Jingwen Li
Xiangfei Song
Lishan Yao
author_sort Jingwen Li
collection DOAJ
description Nuclear magnetic resonance (NMR) serves as a powerful tool for studying both the structure and dynamics of proteins. The NOE method, alongside residual dipolar; coupling, paramagnetic effects, J-coupling, and other related techniques, has reached a level of maturity that allows for the determination of protein structures. Furthermore, NMR relaxation methods prove to be highly effective in characterizing protein dynamics across various timescales. The properties of protein systems are dictated by intra- and intermolecular interactions among atoms, which involve covalent bonds, hydrogen bonds (H-bonds), electrostatic interactions, and van der Waals forces. Multiple NMR approaches have been developed to measure noncovalent interactions, and this paper offers a concise overview of noncovalent interaction measurements using NMR, with a specific emphasis on the advancements accomplished in our laboratory.
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institution Kabale University
issn 2772-5162
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publishDate 2025-05-01
publisher KeAi Communications Co. Ltd.
record_format Article
series Magnetic Resonance Letters
spelling doaj-art-e68e726401bc46039b74c477cd444cad2025-08-20T03:26:20ZengKeAi Communications Co. Ltd.Magnetic Resonance Letters2772-51622025-05-015220017310.1016/j.mrl.2024.200173Measurement of protein non-covalent interactions in buffer and cellsJingwen Li0Xiangfei Song1Lishan Yao2College of Chemistry and Chemical Engineering, China University of Petroleum (East China), Qingdao, 266580, ChinaQingdao New Energy Shandong Laboratory, Qingdao Institute of Bioenergy and Bioprocess Technology, Chinese Academy of Sciences, Qingdao, 266101, China; Shandong Energy Institute, Qingdao, 266101, China; Corresponding author. Qingdao New Energy Shandong Laboratory, Qingdao Institute of Bioenergy and Bioprocess Technology, Chinese Academy of Sciences, Qingdao, 266101, China.Qingdao New Energy Shandong Laboratory, Qingdao Institute of Bioenergy and Bioprocess Technology, Chinese Academy of Sciences, Qingdao, 266101, China; Shandong Energy Institute, Qingdao, 266101, China; Corresponding author. Qingdao New Energy Shandong Laboratory, Qingdao Institute of Bioenergy and Bioprocess Technology, Chinese Academy of Sciences, Qingdao, 266101, China.Nuclear magnetic resonance (NMR) serves as a powerful tool for studying both the structure and dynamics of proteins. The NOE method, alongside residual dipolar; coupling, paramagnetic effects, J-coupling, and other related techniques, has reached a level of maturity that allows for the determination of protein structures. Furthermore, NMR relaxation methods prove to be highly effective in characterizing protein dynamics across various timescales. The properties of protein systems are dictated by intra- and intermolecular interactions among atoms, which involve covalent bonds, hydrogen bonds (H-bonds), electrostatic interactions, and van der Waals forces. Multiple NMR approaches have been developed to measure noncovalent interactions, and this paper offers a concise overview of noncovalent interaction measurements using NMR, with a specific emphasis on the advancements accomplished in our laboratory.http://www.sciencedirect.com/science/article/pii/S2772516224000809NMRH-bondCH/CH van der Waals interactionsQuinary interactionsElectrostatic interactionsCH/π and NH/π stacking interactions
spellingShingle Jingwen Li
Xiangfei Song
Lishan Yao
Measurement of protein non-covalent interactions in buffer and cells
Magnetic Resonance Letters
NMR
H-bond
CH/CH van der Waals interactions
Quinary interactions
Electrostatic interactions
CH/π and NH/π stacking interactions
title Measurement of protein non-covalent interactions in buffer and cells
title_full Measurement of protein non-covalent interactions in buffer and cells
title_fullStr Measurement of protein non-covalent interactions in buffer and cells
title_full_unstemmed Measurement of protein non-covalent interactions in buffer and cells
title_short Measurement of protein non-covalent interactions in buffer and cells
title_sort measurement of protein non covalent interactions in buffer and cells
topic NMR
H-bond
CH/CH van der Waals interactions
Quinary interactions
Electrostatic interactions
CH/π and NH/π stacking interactions
url http://www.sciencedirect.com/science/article/pii/S2772516224000809
work_keys_str_mv AT jingwenli measurementofproteinnoncovalentinteractionsinbufferandcells
AT xiangfeisong measurementofproteinnoncovalentinteractionsinbufferandcells
AT lishanyao measurementofproteinnoncovalentinteractionsinbufferandcells