A Novel Copper Ionophore Nanoshuttle (Winged Cu) for Inducing Cuproptosis in B16 Melanoma Cells

Cuproptosis, a newly discovered copper-dependent programmed cell death pathway, represents a promising approach for anticancer therapy. However, the efficacy of cuproptosis critically depends on intracellular copper accumulation. Traditional copper ionophores have limited therapeutic efficacy due to...

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Main Authors: Yuhuan Wu, Ziyao Chang, Wenhao Wang, Chuanbin Wu, Xin Pan, Zhengwei Huang
Format: Article
Language:English
Published: MDPI AG 2025-06-01
Series:Biomolecules
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Online Access:https://www.mdpi.com/2218-273X/15/6/895
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author Yuhuan Wu
Ziyao Chang
Wenhao Wang
Chuanbin Wu
Xin Pan
Zhengwei Huang
author_facet Yuhuan Wu
Ziyao Chang
Wenhao Wang
Chuanbin Wu
Xin Pan
Zhengwei Huang
author_sort Yuhuan Wu
collection DOAJ
description Cuproptosis, a newly discovered copper-dependent programmed cell death pathway, represents a promising approach for anticancer therapy. However, the efficacy of cuproptosis critically depends on intracellular copper accumulation. Traditional copper ionophores have limited therapeutic efficacy due to their reliance on serum copper levels. Therefore, the development of novel copper ionophores to enhance intracellular copper levels is urgently needed. In this study, we targeted a melanoma model and pioneered the application of Bis(2-hydroxyethyl)dithiocarbamic acid copper(II) [Cu(HEDTC)<sub>2</sub>] as a highly efficient copper ionophore for inducing cuproptosis in B16 melanoma cells. Compared to conventional copper ionophores, Cu(HEDTC)<sub>2</sub> exhibits superior intracellular copper delivery efficiency, thereby enhancing the induction of cuproptosis. We further constructed a Cu(HEDTC)<sub>2</sub>@Soluplus-nanomicelle (CS NM) system designed to disrupt copper ion homeostasis in tumor cells and amplify cuproptosis. In this system, Cu(HEDTC)<sub>2</sub>, as a novel copper ionophore, significantly enhanced the copper level in B16 melanoma cells. Upon cellular internalization, CS NM underwent degradation and released copper ions, which subsequently triggered cuproptosis by causing abnormal aggregation of mitochondrial lipoylated proteins. This study provides a new experimental foundation and potential therapeutic strategy for cuproptosis-based cancer treatment.
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spelling doaj-art-e612873124f144afb5e11ac603fd23622025-08-20T02:24:33ZengMDPI AGBiomolecules2218-273X2025-06-0115689510.3390/biom15060895A Novel Copper Ionophore Nanoshuttle (Winged Cu) for Inducing Cuproptosis in B16 Melanoma CellsYuhuan Wu0Ziyao Chang1Wenhao Wang2Chuanbin Wu3Xin Pan4Zhengwei Huang5School of Pharmaceutical Science, Sun Yat-Sen University, Guangzhou 510006, ChinaSchool of Pharmaceutical Science, Sun Yat-Sen University, Guangzhou 510006, ChinaSchool of Pharmaceutical Science, Sun Yat-Sen University, Guangzhou 510006, ChinaState Key Laboratory of Bioactive Molecules and Druggability Assessment, Guangdong Basic Research Center of Excellence for Natural Bioactive Molecules and Discovery of Innovative Drugs, College of Pharmacy, Jinan University, Guangzhou 510632, ChinaSchool of Pharmaceutical Science, Sun Yat-Sen University, Guangzhou 510006, ChinaState Key Laboratory of Bioactive Molecules and Druggability Assessment, Guangdong Basic Research Center of Excellence for Natural Bioactive Molecules and Discovery of Innovative Drugs, College of Pharmacy, Jinan University, Guangzhou 510632, ChinaCuproptosis, a newly discovered copper-dependent programmed cell death pathway, represents a promising approach for anticancer therapy. However, the efficacy of cuproptosis critically depends on intracellular copper accumulation. Traditional copper ionophores have limited therapeutic efficacy due to their reliance on serum copper levels. Therefore, the development of novel copper ionophores to enhance intracellular copper levels is urgently needed. In this study, we targeted a melanoma model and pioneered the application of Bis(2-hydroxyethyl)dithiocarbamic acid copper(II) [Cu(HEDTC)<sub>2</sub>] as a highly efficient copper ionophore for inducing cuproptosis in B16 melanoma cells. Compared to conventional copper ionophores, Cu(HEDTC)<sub>2</sub> exhibits superior intracellular copper delivery efficiency, thereby enhancing the induction of cuproptosis. We further constructed a Cu(HEDTC)<sub>2</sub>@Soluplus-nanomicelle (CS NM) system designed to disrupt copper ion homeostasis in tumor cells and amplify cuproptosis. In this system, Cu(HEDTC)<sub>2</sub>, as a novel copper ionophore, significantly enhanced the copper level in B16 melanoma cells. Upon cellular internalization, CS NM underwent degradation and released copper ions, which subsequently triggered cuproptosis by causing abnormal aggregation of mitochondrial lipoylated proteins. This study provides a new experimental foundation and potential therapeutic strategy for cuproptosis-based cancer treatment.https://www.mdpi.com/2218-273X/15/6/895cuproptosiscopper ionophoreintracellular copper accumulationnanoshuttleB16 melanoma cells
spellingShingle Yuhuan Wu
Ziyao Chang
Wenhao Wang
Chuanbin Wu
Xin Pan
Zhengwei Huang
A Novel Copper Ionophore Nanoshuttle (Winged Cu) for Inducing Cuproptosis in B16 Melanoma Cells
Biomolecules
cuproptosis
copper ionophore
intracellular copper accumulation
nanoshuttle
B16 melanoma cells
title A Novel Copper Ionophore Nanoshuttle (Winged Cu) for Inducing Cuproptosis in B16 Melanoma Cells
title_full A Novel Copper Ionophore Nanoshuttle (Winged Cu) for Inducing Cuproptosis in B16 Melanoma Cells
title_fullStr A Novel Copper Ionophore Nanoshuttle (Winged Cu) for Inducing Cuproptosis in B16 Melanoma Cells
title_full_unstemmed A Novel Copper Ionophore Nanoshuttle (Winged Cu) for Inducing Cuproptosis in B16 Melanoma Cells
title_short A Novel Copper Ionophore Nanoshuttle (Winged Cu) for Inducing Cuproptosis in B16 Melanoma Cells
title_sort novel copper ionophore nanoshuttle winged cu for inducing cuproptosis in b16 melanoma cells
topic cuproptosis
copper ionophore
intracellular copper accumulation
nanoshuttle
B16 melanoma cells
url https://www.mdpi.com/2218-273X/15/6/895
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