ADSORPTION-PHOTOCATALYSIS SYNERGY OF BI4TI2.9FE0.1O12 FOR CIPROFLOXACIN REMOVAL

The triple-layer Aurivillius compound Bi4Ti2.9Fe0.1O12 has been reported to exhibit both adsorption and photocatalytic properties and, therefore, can be used to remove organic waste such as antibiotic residues. In this study, the Bi4Ti2.9Fe0.1O12 compound was synthesized using the molten salt method...

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Main Authors: Nurul Hikmah, Anton Prasetyo
Format: Article
Language:English
Published: Jurusan Fisika Fakultas Sains Dan Teknologi, Universitas Islam Negeri Maulana Malik Ibrahim Malang 2025-04-01
Series:Jurnal Neutrino: Jurnal Fisika dan Aplikasinya
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Online Access:https://ejournal.uin-malang.ac.id/index.php/NEUTRINO/article/view/31329
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author Nurul Hikmah
Anton Prasetyo
author_facet Nurul Hikmah
Anton Prasetyo
author_sort Nurul Hikmah
collection DOAJ
description The triple-layer Aurivillius compound Bi4Ti2.9Fe0.1O12 has been reported to exhibit both adsorption and photocatalytic properties and, therefore, can be used to remove organic waste such as antibiotic residues. In this study, the Bi4Ti2.9Fe0.1O12 compound was synthesized using the molten salt method. The diffractogram showed Bi4Ti2.9Fe0.1O12 compound was successfully synthesized with no impurity phases detected. Scanning electron microscopy (SEM) images revealed that the compound has a plate-like/sheet-agglomerated particle morphology, with sizes ranging from 2 to 6 μm. Band gap energy calculations showed that the Bi4Ti2.9Fe0.1O12 compound has a band gap of 2.74 eV (453 nm). Adsorption tests demonstrated that the compound could adsorb 54.47± 0.56% of ciprofloxacin. Adsorption-degradation tests over 30, 60, 90, and 120 minutes reduced ciprofloxacin c oncentration by 59.84±0.54, 64.05±0.056, 70.04±0.091, and 62.55±0.052%, respectively. It indicates that the adsorption mechanism is more dominant than the photocatalytic mechanism. This may be due to the large number of ciprofloxacin molecules adhering to the BIT surface, making it difficult for light to penetrate, thereby preventing the photocatalytic mechanism from operating at its maximum efficiency.
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id doaj-art-e55bdd8d33db4f388acb535009302f13
institution DOAJ
issn 1979-6374
2460-5999
language English
publishDate 2025-04-01
publisher Jurusan Fisika Fakultas Sains Dan Teknologi, Universitas Islam Negeri Maulana Malik Ibrahim Malang
record_format Article
series Jurnal Neutrino: Jurnal Fisika dan Aplikasinya
spelling doaj-art-e55bdd8d33db4f388acb535009302f132025-08-20T03:03:49ZengJurusan Fisika Fakultas Sains Dan Teknologi, Universitas Islam Negeri Maulana Malik Ibrahim MalangJurnal Neutrino: Jurnal Fisika dan Aplikasinya1979-63742460-59992025-04-01172818810.18860/neu.v17i2.313298734ADSORPTION-PHOTOCATALYSIS SYNERGY OF BI4TI2.9FE0.1O12 FOR CIPROFLOXACIN REMOVALNurul Hikmah0Anton Prasetyo1Department of Chemistry Universitas Islam Negeri Maulana Malik Ibrahim MalangDepartment of Chemistry Universitas Islam Negeri Maulana Malik Ibrahim MalangThe triple-layer Aurivillius compound Bi4Ti2.9Fe0.1O12 has been reported to exhibit both adsorption and photocatalytic properties and, therefore, can be used to remove organic waste such as antibiotic residues. In this study, the Bi4Ti2.9Fe0.1O12 compound was synthesized using the molten salt method. The diffractogram showed Bi4Ti2.9Fe0.1O12 compound was successfully synthesized with no impurity phases detected. Scanning electron microscopy (SEM) images revealed that the compound has a plate-like/sheet-agglomerated particle morphology, with sizes ranging from 2 to 6 μm. Band gap energy calculations showed that the Bi4Ti2.9Fe0.1O12 compound has a band gap of 2.74 eV (453 nm). Adsorption tests demonstrated that the compound could adsorb 54.47± 0.56% of ciprofloxacin. Adsorption-degradation tests over 30, 60, 90, and 120 minutes reduced ciprofloxacin c oncentration by 59.84±0.54, 64.05±0.056, 70.04±0.091, and 62.55±0.052%, respectively. It indicates that the adsorption mechanism is more dominant than the photocatalytic mechanism. This may be due to the large number of ciprofloxacin molecules adhering to the BIT surface, making it difficult for light to penetrate, thereby preventing the photocatalytic mechanism from operating at its maximum efficiency.https://ejournal.uin-malang.ac.id/index.php/NEUTRINO/article/view/31329bi4ti2.9fe0.1o12ciprofloxacinadsorption-photocatalyst
spellingShingle Nurul Hikmah
Anton Prasetyo
ADSORPTION-PHOTOCATALYSIS SYNERGY OF BI4TI2.9FE0.1O12 FOR CIPROFLOXACIN REMOVAL
Jurnal Neutrino: Jurnal Fisika dan Aplikasinya
bi4ti2.9fe0.1o12
ciprofloxacin
adsorption-photocatalyst
title ADSORPTION-PHOTOCATALYSIS SYNERGY OF BI4TI2.9FE0.1O12 FOR CIPROFLOXACIN REMOVAL
title_full ADSORPTION-PHOTOCATALYSIS SYNERGY OF BI4TI2.9FE0.1O12 FOR CIPROFLOXACIN REMOVAL
title_fullStr ADSORPTION-PHOTOCATALYSIS SYNERGY OF BI4TI2.9FE0.1O12 FOR CIPROFLOXACIN REMOVAL
title_full_unstemmed ADSORPTION-PHOTOCATALYSIS SYNERGY OF BI4TI2.9FE0.1O12 FOR CIPROFLOXACIN REMOVAL
title_short ADSORPTION-PHOTOCATALYSIS SYNERGY OF BI4TI2.9FE0.1O12 FOR CIPROFLOXACIN REMOVAL
title_sort adsorption photocatalysis synergy of bi4ti2 9fe0 1o12 for ciprofloxacin removal
topic bi4ti2.9fe0.1o12
ciprofloxacin
adsorption-photocatalyst
url https://ejournal.uin-malang.ac.id/index.php/NEUTRINO/article/view/31329
work_keys_str_mv AT nurulhikmah adsorptionphotocatalysissynergyofbi4ti29fe01o12forciprofloxacinremoval
AT antonprasetyo adsorptionphotocatalysissynergyofbi4ti29fe01o12forciprofloxacinremoval