Pulsed laser-tuned ruthenium@carbon interface for self-powered hydrogen production via zinc–hydrazine battery coupled hybrid electrolysis

Herein, we report the synthesis of selectively face-centered cubic structured ruthenium nanospheres covered in graphitic carbon (denoted as Ru@C) using an effective and innovative pulsed laser ablation in liquid strategy. The Ru@C‒200 catalyst exhibited a low overpotential of 48 ​mV for hydrogen evo...

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Main Authors: Huieun Ahn, Raja Arumugam Senthil, Sieon Jung, Anuj Kumar, Mohd Ubaidullah, Myong Yong Choi
Format: Article
Language:English
Published: KeAi Communications Co. Ltd. 2025-09-01
Series:eScience
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Online Access:http://www.sciencedirect.com/science/article/pii/S2667141725000382
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author Huieun Ahn
Raja Arumugam Senthil
Sieon Jung
Anuj Kumar
Mohd Ubaidullah
Myong Yong Choi
author_facet Huieun Ahn
Raja Arumugam Senthil
Sieon Jung
Anuj Kumar
Mohd Ubaidullah
Myong Yong Choi
author_sort Huieun Ahn
collection DOAJ
description Herein, we report the synthesis of selectively face-centered cubic structured ruthenium nanospheres covered in graphitic carbon (denoted as Ru@C) using an effective and innovative pulsed laser ablation in liquid strategy. The Ru@C‒200 catalyst exhibited a low overpotential of 48 ​mV for hydrogen evolution reaction (HER) and an ultralow oxidation potential of −8 ​mV (vs. reversible hydrogen electrode) for hydrazine oxidation reaction (HzOR) at 10 ​mA ​cm−2, maintaining long-term durability for over 100 ​h, demonstrating its dual-functional activity. This performance was attributed to the robust synergistic coupling between the Ru core and C shell, as confirmed by in situ electrochemical studies and density functional theory investigations. As a result, overall hydrazine splitting (OHzS) in the Ru@C‒200||Ru@C‒200 system requires only low cell voltages of 0.11 and 0.70 ​V at 10 and 100 ​mA ​cm−2, respectively. Moreover, a rechargeable zinc–hydrazine (Zn–Hz) battery, fabricated using the Ru@C‒200 catalyst as the cathode and Zn foil as the anode, exhibited a high energy efficiency of 90% and efficient H2 production, validating its remarkable ability for practical applications. Notably, coupling Zn–Hz battery with OHzS system encourages self-powered H2 production. This study provides potential guidance for engineering robust electrocatalysts for large-scale H2 production while purifying hydrazine-containing industrial sewage.
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institution Kabale University
issn 2667-1417
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publishDate 2025-09-01
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spelling doaj-art-e4fead9cb62b449ba3bf6ec657fa43922025-08-24T05:14:56ZengKeAi Communications Co. Ltd.eScience2667-14172025-09-015510040810.1016/j.esci.2025.100408Pulsed laser-tuned ruthenium@carbon interface for self-powered hydrogen production via zinc–hydrazine battery coupled hybrid electrolysisHuieun Ahn0Raja Arumugam Senthil1Sieon Jung2Anuj Kumar3Mohd Ubaidullah4Myong Yong Choi5Department of Chemistry (BK21 FOUR), Research Institute of Advanced Chemistry, Gyeongsang National University, Jinju 52828, Republic of KoreaDepartment of Chemistry (BK21 FOUR), Research Institute of Advanced Chemistry, Gyeongsang National University, Jinju 52828, Republic of KoreaDepartment of Chemistry (BK21 FOUR), Research Institute of Advanced Chemistry, Gyeongsang National University, Jinju 52828, Republic of KoreaNano-Technology Research Laboratory, Department of Chemistry, GLA University, Mathura, Uttar Pradesh 281406, IndiaDepartment of Chemistry, College of Science, King Saud University, Riyadh 11451, Saudi ArabiaDepartment of Chemistry (BK21 FOUR), Research Institute of Advanced Chemistry, Gyeongsang National University, Jinju 52828, Republic of Korea; Core-Facility Center for Photochemistry & Nanomaterials, Gyeongsang National University, Jinju 52828, Republic of Korea; Corresponding author.Herein, we report the synthesis of selectively face-centered cubic structured ruthenium nanospheres covered in graphitic carbon (denoted as Ru@C) using an effective and innovative pulsed laser ablation in liquid strategy. The Ru@C‒200 catalyst exhibited a low overpotential of 48 ​mV for hydrogen evolution reaction (HER) and an ultralow oxidation potential of −8 ​mV (vs. reversible hydrogen electrode) for hydrazine oxidation reaction (HzOR) at 10 ​mA ​cm−2, maintaining long-term durability for over 100 ​h, demonstrating its dual-functional activity. This performance was attributed to the robust synergistic coupling between the Ru core and C shell, as confirmed by in situ electrochemical studies and density functional theory investigations. As a result, overall hydrazine splitting (OHzS) in the Ru@C‒200||Ru@C‒200 system requires only low cell voltages of 0.11 and 0.70 ​V at 10 and 100 ​mA ​cm−2, respectively. Moreover, a rechargeable zinc–hydrazine (Zn–Hz) battery, fabricated using the Ru@C‒200 catalyst as the cathode and Zn foil as the anode, exhibited a high energy efficiency of 90% and efficient H2 production, validating its remarkable ability for practical applications. Notably, coupling Zn–Hz battery with OHzS system encourages self-powered H2 production. This study provides potential guidance for engineering robust electrocatalysts for large-scale H2 production while purifying hydrazine-containing industrial sewage.http://www.sciencedirect.com/science/article/pii/S2667141725000382Pulsed laser ablation in liquidRu@C electrocatalystZinc–hydrazine batteryHybrid water electrolysisEfficient H2 productionHydrazine degradation
spellingShingle Huieun Ahn
Raja Arumugam Senthil
Sieon Jung
Anuj Kumar
Mohd Ubaidullah
Myong Yong Choi
Pulsed laser-tuned ruthenium@carbon interface for self-powered hydrogen production via zinc–hydrazine battery coupled hybrid electrolysis
eScience
Pulsed laser ablation in liquid
Ru@C electrocatalyst
Zinc–hydrazine battery
Hybrid water electrolysis
Efficient H2 production
Hydrazine degradation
title Pulsed laser-tuned ruthenium@carbon interface for self-powered hydrogen production via zinc–hydrazine battery coupled hybrid electrolysis
title_full Pulsed laser-tuned ruthenium@carbon interface for self-powered hydrogen production via zinc–hydrazine battery coupled hybrid electrolysis
title_fullStr Pulsed laser-tuned ruthenium@carbon interface for self-powered hydrogen production via zinc–hydrazine battery coupled hybrid electrolysis
title_full_unstemmed Pulsed laser-tuned ruthenium@carbon interface for self-powered hydrogen production via zinc–hydrazine battery coupled hybrid electrolysis
title_short Pulsed laser-tuned ruthenium@carbon interface for self-powered hydrogen production via zinc–hydrazine battery coupled hybrid electrolysis
title_sort pulsed laser tuned ruthenium carbon interface for self powered hydrogen production via zinc hydrazine battery coupled hybrid electrolysis
topic Pulsed laser ablation in liquid
Ru@C electrocatalyst
Zinc–hydrazine battery
Hybrid water electrolysis
Efficient H2 production
Hydrazine degradation
url http://www.sciencedirect.com/science/article/pii/S2667141725000382
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AT anujkumar pulsedlasertunedrutheniumcarboninterfaceforselfpoweredhydrogenproductionviazinchydrazinebatterycoupledhybridelectrolysis
AT mohdubaidullah pulsedlasertunedrutheniumcarboninterfaceforselfpoweredhydrogenproductionviazinchydrazinebatterycoupledhybridelectrolysis
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