Membrane adsorbers with ultrahigh metal-organic framework loading for high flux separations

Abstract Metal-organic frameworks (MOFs) with high porosity and designable functionality make it possible to access the merits of high permeability and selectivity. However, scalable fabrication methods to produce mixed matrix membranes (MMMs) with good flexibility and ultrahigh MOF loading are urge...

Full description

Saved in:
Bibliographic Details
Main Authors: Hang Wang, Shuang Zhao, Yi Liu, Ruxin Yao, Xiaoqi Wang, Yuhua Cao, Dou Ma, Mingchu Zou, Anyuan Cao, Xiao Feng, Bo Wang
Format: Article
Language:English
Published: Nature Portfolio 2019-09-01
Series:Nature Communications
Online Access:https://doi.org/10.1038/s41467-019-12114-8
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1849433058297511936
author Hang Wang
Shuang Zhao
Yi Liu
Ruxin Yao
Xiaoqi Wang
Yuhua Cao
Dou Ma
Mingchu Zou
Anyuan Cao
Xiao Feng
Bo Wang
author_facet Hang Wang
Shuang Zhao
Yi Liu
Ruxin Yao
Xiaoqi Wang
Yuhua Cao
Dou Ma
Mingchu Zou
Anyuan Cao
Xiao Feng
Bo Wang
author_sort Hang Wang
collection DOAJ
description Abstract Metal-organic frameworks (MOFs) with high porosity and designable functionality make it possible to access the merits of high permeability and selectivity. However, scalable fabrication methods to produce mixed matrix membranes (MMMs) with good flexibility and ultrahigh MOF loading are urgently needed yet largely unmet. Herein, we report a thermally induced phase separation-hot pressing (TIPS-HoP) strategy to roll-to-roll produce 10 distinct MOF-membranes (loadings up to 86 wt%). Ultrahigh-molecular-weight polyethylene interweaving the MOF particles contributes to their mechanical strength. Rejections (99%) of organic dyes with a water flux of 125.7 L m–2 h–1 bar–1 under cross-flow filtration mode. The micron-sized channels between the MOF particles translate into fast water permeation, while the porous MOFs reject solutes through rapid adsorption. This strategy paves ways for developing high-performance membrane adsorbers for crucial separation processes. As a proof-of-concept, the abilities of the membrane adsorbers for separating racemates and proteins have been demonstrated.
format Article
id doaj-art-e489aa5255654e1f927c6c3e0a80fd01
institution Kabale University
issn 2041-1723
language English
publishDate 2019-09-01
publisher Nature Portfolio
record_format Article
series Nature Communications
spelling doaj-art-e489aa5255654e1f927c6c3e0a80fd012025-08-20T03:27:11ZengNature PortfolioNature Communications2041-17232019-09-011011910.1038/s41467-019-12114-8Membrane adsorbers with ultrahigh metal-organic framework loading for high flux separationsHang Wang0Shuang Zhao1Yi Liu2Ruxin Yao3Xiaoqi Wang4Yuhua Cao5Dou Ma6Mingchu Zou7Anyuan Cao8Xiao Feng9Bo Wang10Beijing Key Laboratory of Photoelectronic/Electrophotonic Conversion Materials, Key Laboratory of Cluster Science, Ministry of Education, School of Chemistry and Chemical Engineering, Beijing Institute of TechnologyBeijing Key Laboratory of Photoelectronic/Electrophotonic Conversion Materials, Key Laboratory of Cluster Science, Ministry of Education, School of Chemistry and Chemical Engineering, Beijing Institute of TechnologyBeijing Key Laboratory of Photoelectronic/Electrophotonic Conversion Materials, Key Laboratory of Cluster Science, Ministry of Education, School of Chemistry and Chemical Engineering, Beijing Institute of TechnologyBeijing Key Laboratory of Photoelectronic/Electrophotonic Conversion Materials, Key Laboratory of Cluster Science, Ministry of Education, School of Chemistry and Chemical Engineering, Beijing Institute of TechnologyBeijing Key Laboratory of Photoelectronic/Electrophotonic Conversion Materials, Key Laboratory of Cluster Science, Ministry of Education, School of Chemistry and Chemical Engineering, Beijing Institute of TechnologyBeijing Key Laboratory of Photoelectronic/Electrophotonic Conversion Materials, Key Laboratory of Cluster Science, Ministry of Education, School of Chemistry and Chemical Engineering, Beijing Institute of TechnologyBeijing Key Laboratory of Photoelectronic/Electrophotonic Conversion Materials, Key Laboratory of Cluster Science, Ministry of Education, School of Chemistry and Chemical Engineering, Beijing Institute of TechnologyDepartment of Materials Science and Engineering College of Engineering, Peking UniversityDepartment of Materials Science and Engineering College of Engineering, Peking UniversityBeijing Key Laboratory of Photoelectronic/Electrophotonic Conversion Materials, Key Laboratory of Cluster Science, Ministry of Education, School of Chemistry and Chemical Engineering, Beijing Institute of TechnologyBeijing Key Laboratory of Photoelectronic/Electrophotonic Conversion Materials, Key Laboratory of Cluster Science, Ministry of Education, School of Chemistry and Chemical Engineering, Beijing Institute of TechnologyAbstract Metal-organic frameworks (MOFs) with high porosity and designable functionality make it possible to access the merits of high permeability and selectivity. However, scalable fabrication methods to produce mixed matrix membranes (MMMs) with good flexibility and ultrahigh MOF loading are urgently needed yet largely unmet. Herein, we report a thermally induced phase separation-hot pressing (TIPS-HoP) strategy to roll-to-roll produce 10 distinct MOF-membranes (loadings up to 86 wt%). Ultrahigh-molecular-weight polyethylene interweaving the MOF particles contributes to their mechanical strength. Rejections (99%) of organic dyes with a water flux of 125.7 L m–2 h–1 bar–1 under cross-flow filtration mode. The micron-sized channels between the MOF particles translate into fast water permeation, while the porous MOFs reject solutes through rapid adsorption. This strategy paves ways for developing high-performance membrane adsorbers for crucial separation processes. As a proof-of-concept, the abilities of the membrane adsorbers for separating racemates and proteins have been demonstrated.https://doi.org/10.1038/s41467-019-12114-8
spellingShingle Hang Wang
Shuang Zhao
Yi Liu
Ruxin Yao
Xiaoqi Wang
Yuhua Cao
Dou Ma
Mingchu Zou
Anyuan Cao
Xiao Feng
Bo Wang
Membrane adsorbers with ultrahigh metal-organic framework loading for high flux separations
Nature Communications
title Membrane adsorbers with ultrahigh metal-organic framework loading for high flux separations
title_full Membrane adsorbers with ultrahigh metal-organic framework loading for high flux separations
title_fullStr Membrane adsorbers with ultrahigh metal-organic framework loading for high flux separations
title_full_unstemmed Membrane adsorbers with ultrahigh metal-organic framework loading for high flux separations
title_short Membrane adsorbers with ultrahigh metal-organic framework loading for high flux separations
title_sort membrane adsorbers with ultrahigh metal organic framework loading for high flux separations
url https://doi.org/10.1038/s41467-019-12114-8
work_keys_str_mv AT hangwang membraneadsorberswithultrahighmetalorganicframeworkloadingforhighfluxseparations
AT shuangzhao membraneadsorberswithultrahighmetalorganicframeworkloadingforhighfluxseparations
AT yiliu membraneadsorberswithultrahighmetalorganicframeworkloadingforhighfluxseparations
AT ruxinyao membraneadsorberswithultrahighmetalorganicframeworkloadingforhighfluxseparations
AT xiaoqiwang membraneadsorberswithultrahighmetalorganicframeworkloadingforhighfluxseparations
AT yuhuacao membraneadsorberswithultrahighmetalorganicframeworkloadingforhighfluxseparations
AT douma membraneadsorberswithultrahighmetalorganicframeworkloadingforhighfluxseparations
AT mingchuzou membraneadsorberswithultrahighmetalorganicframeworkloadingforhighfluxseparations
AT anyuancao membraneadsorberswithultrahighmetalorganicframeworkloadingforhighfluxseparations
AT xiaofeng membraneadsorberswithultrahighmetalorganicframeworkloadingforhighfluxseparations
AT bowang membraneadsorberswithultrahighmetalorganicframeworkloadingforhighfluxseparations