Experimental Investigations on Repair and Permeability Reduction for Single Sandstone Fracture Using a Mixed CaCO<sub>3</sub> and Fe(OH)<sub>3</sub> Precipitate

In China, groundwater loss caused by underground coal mining is becoming increasingly serious. The key to groundwater restoration is to repair mining-induced water-conducting fractures (WCFs) in the overlying strata. In this study, the adsorption–consolidation sealing characteristics of chemical pre...

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Main Authors: Jinfeng Ju, Quansheng Li, Chenyu Wang, Yanan Fan
Format: Article
Language:English
Published: MDPI AG 2024-11-01
Series:Applied Sciences
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Online Access:https://www.mdpi.com/2076-3417/14/22/10617
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author Jinfeng Ju
Quansheng Li
Chenyu Wang
Yanan Fan
author_facet Jinfeng Ju
Quansheng Li
Chenyu Wang
Yanan Fan
author_sort Jinfeng Ju
collection DOAJ
description In China, groundwater loss caused by underground coal mining is becoming increasingly serious. The key to groundwater restoration is to repair mining-induced water-conducting fractures (WCFs) in the overlying strata. In this study, the adsorption–consolidation sealing characteristics of chemical precipitates were used to conduct permeability reduction (PR) experiments, including adding mixed CaCO<sub>3</sub> and Fe(OH)<sub>3</sub> to a sandstone specimen with a single fracture at room temperature. An aqueous solution of Na<sub>2</sub>CO<sub>3</sub> was used as the simulated groundwater, and a solution of mixed CaCl<sub>2</sub> and FeCl<sub>2</sub> was used as the repair reagent to simulate the water seepage conditions of a fractured rock mass. The two aqueous solutions were simultaneously injected into a single-fractured rock specimen at a constant flow rate. The experimental results show that the Fe(OH)<sub>3</sub> colloid encapsulated CaCO<sub>3</sub> crystals in a mixed precipitate, reducing the overall structural stability of the mixed precipitate and restricting repair and PR efficiency. However, the Fe(OH)<sub>3</sub> precipitate had better PR efficiency in the initial stage of the experiment. Therefore, a better scheme was put forward to repair the WCF, utilizing a mixed Fe(OH)<sub>3</sub> and CaCO<sub>3</sub> precipitate with a molar ratio close to 1:4 in the early stage and a single CaCO<sub>3</sub> precipitate in the later stage.
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spelling doaj-art-e43fe1d00d8e4758afe189fd905a024a2025-08-20T01:53:40ZengMDPI AGApplied Sciences2076-34172024-11-0114221061710.3390/app142210617Experimental Investigations on Repair and Permeability Reduction for Single Sandstone Fracture Using a Mixed CaCO<sub>3</sub> and Fe(OH)<sub>3</sub> PrecipitateJinfeng Ju0Quansheng Li1Chenyu Wang2Yanan Fan3The National and Local Joint Engineering Laboratory of Internet Application Technology on Mine, China University of Mining and Technology, Xuzhou 221008, ChinaState Key Laboratory of Water Resource Protection and Utilization in Coal Mining, Beijing 100011, ChinaState Key Laboratory for Fine Exploration and Intelligent Development of Coal Resources, China University of Mining and Technology, Xuzhou 221116, ChinaState Key Laboratory of Intelligent Construction and Healthy Operation and Maintenance of Deep Underground Engineering, China University of Mining and Technology, Xuzhou 221116, ChinaIn China, groundwater loss caused by underground coal mining is becoming increasingly serious. The key to groundwater restoration is to repair mining-induced water-conducting fractures (WCFs) in the overlying strata. In this study, the adsorption–consolidation sealing characteristics of chemical precipitates were used to conduct permeability reduction (PR) experiments, including adding mixed CaCO<sub>3</sub> and Fe(OH)<sub>3</sub> to a sandstone specimen with a single fracture at room temperature. An aqueous solution of Na<sub>2</sub>CO<sub>3</sub> was used as the simulated groundwater, and a solution of mixed CaCl<sub>2</sub> and FeCl<sub>2</sub> was used as the repair reagent to simulate the water seepage conditions of a fractured rock mass. The two aqueous solutions were simultaneously injected into a single-fractured rock specimen at a constant flow rate. The experimental results show that the Fe(OH)<sub>3</sub> colloid encapsulated CaCO<sub>3</sub> crystals in a mixed precipitate, reducing the overall structural stability of the mixed precipitate and restricting repair and PR efficiency. However, the Fe(OH)<sub>3</sub> precipitate had better PR efficiency in the initial stage of the experiment. Therefore, a better scheme was put forward to repair the WCF, utilizing a mixed Fe(OH)<sub>3</sub> and CaCO<sub>3</sub> precipitate with a molar ratio close to 1:4 in the early stage and a single CaCO<sub>3</sub> precipitate in the later stage.https://www.mdpi.com/2076-3417/14/22/10617water-conducting fracture (WCF)mixed precipitatepermeability reduction (PR)restoration of aquifer ecological functiongreen mining
spellingShingle Jinfeng Ju
Quansheng Li
Chenyu Wang
Yanan Fan
Experimental Investigations on Repair and Permeability Reduction for Single Sandstone Fracture Using a Mixed CaCO<sub>3</sub> and Fe(OH)<sub>3</sub> Precipitate
Applied Sciences
water-conducting fracture (WCF)
mixed precipitate
permeability reduction (PR)
restoration of aquifer ecological function
green mining
title Experimental Investigations on Repair and Permeability Reduction for Single Sandstone Fracture Using a Mixed CaCO<sub>3</sub> and Fe(OH)<sub>3</sub> Precipitate
title_full Experimental Investigations on Repair and Permeability Reduction for Single Sandstone Fracture Using a Mixed CaCO<sub>3</sub> and Fe(OH)<sub>3</sub> Precipitate
title_fullStr Experimental Investigations on Repair and Permeability Reduction for Single Sandstone Fracture Using a Mixed CaCO<sub>3</sub> and Fe(OH)<sub>3</sub> Precipitate
title_full_unstemmed Experimental Investigations on Repair and Permeability Reduction for Single Sandstone Fracture Using a Mixed CaCO<sub>3</sub> and Fe(OH)<sub>3</sub> Precipitate
title_short Experimental Investigations on Repair and Permeability Reduction for Single Sandstone Fracture Using a Mixed CaCO<sub>3</sub> and Fe(OH)<sub>3</sub> Precipitate
title_sort experimental investigations on repair and permeability reduction for single sandstone fracture using a mixed caco sub 3 sub and fe oh sub 3 sub precipitate
topic water-conducting fracture (WCF)
mixed precipitate
permeability reduction (PR)
restoration of aquifer ecological function
green mining
url https://www.mdpi.com/2076-3417/14/22/10617
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